US4699849A
Expired / Lapsed
US
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Metal matrix composites and method of manufacture
Assignee: Boeing Co
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Filing: 1985-07-17
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Granted: 1987-10-13
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Expires: 2005-07-17
Abstract
Abstract A metal matrix composite is produced by plastically deforming a metal powder, either before or after blending the powder with ceramic fibers, and compacting the mixture at elevated temperatures to achieve substantially full density. Imparting strain energy to the metal allows reduction of the compaction temperature to eliminate reaction between the fibers and the metal or degradation of the fibers. Silicon nitride fibers are thermodynamically superior for use in aluminum or titanium metal matrix composites, since silicon nitride fibers are more stable at the temperatures required for full compaction. Secondary phase reactions are avoided.
Inventors
- 👤 K. Bhagwan Das
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 23:37
CPC Classifications
C; C22; C22C; C22C47/00; C22C47/14; C22C49/00; C22C49/02; C22C49/04; C22C49/10; C22C49/11; Y; Y10; Y10S; Y10S428/00; Y10S428/902; Y10T; Y10T428/00; Y10T428/29; Y10T428/2913; Y10T428/2933; Y10T428/294; Y10T428/2951; Y10T428/2953; Y10T428/2956; Y10T428/2958
Claims Analysis
Total Claims: 20
Claim 1
Independent Claim
66 words
A metal matrix composite comprising: a matrix metal selected from the group of alloys consisting of titanium and aluminum alloys, the metal having been compacted to near full theoretical density at elevated temperatures and pressure; and silicon nitride fibers uniformly dispersed throughout the matrix metal, the composite being further characterized by the absence of substantially any evidence of interfacial reaction between the metal and the fibers.
Claim 2
Dependent Claim
66 words
A metal matrix composite comprising: a matrix metal selected from the group of alloys consisting of titanium and aluminum alloys, the metal having been compacted to near full theoretical density at elevated temperatures and pressure; and silicon nitride fibers uniformly dispersed throughout the matrix metal, the composite being further characterized by the absence of substantially any evidence of interfacial reaction between the metal and the fibers.
Claim 3
Dependent Claim
18 words
The composite of claim 1 wherein the fibers comprise about 10 to 20% by volume of the composite.
Claim 4
Dependent Claim
12 words
The composite of claim 2 wherein the metal is a titanium alloy.
Claim 5
Dependent Claim
12 words
The composite of claim 2 wherein the metal is an aluminum alloy.
Claim 6
Dependent Claim
10 words
The composite of claim 2 wherein the fibers are uncoated.
Claim 7
Dependent Claim
10 words
The composite of claim 1, wherein the fibers are whiskers.
Claim 8
Dependent Claim
59 words
A metal matrix composite comprising an aluminum alloy or titanium alloy and ceramic fiber whiskers formed by compacting a substantially uniform dispersion of matrix metal and fibers to substantially full theoretical density at an elevated temperature and pressure, the composite being characterized by having essentially no evidence of secondary phase reaction at the interface between the metal and fibers.
Claim 9
Dependent Claim
59 words
A metal matrix composite comprising an aluminum alloy or titanium alloy and ceramic fiber whiskers formed by compacting a substantially uniform dispersion of matrix metal and fibers to substantially full theoretical density at an elevated temperature and pressure, the composite being characterized by having essentially no evidence of secondary phase reaction at the interface between the metal and fibers.
Claim 10
Dependent Claim
11 words
The composite of claim 7 wherein the whiskers are silicon nitride.
Claim 11
Dependent Claim
12 words
The composite of claim 8 wherein the alloy is an aluminum alloy.
Claim 12
Dependent Claim
28 words
The composite of claim 8 wherein the alloy is a titanium alloy, and wherein the alloy is plastically deformed prior to compacting to reduce the compacting processing temperature.
Claim 13
Dependent Claim
16 words
The composite of claim 7 wherein the fibers comprise about 10-20 volume % of the composite.
Claim 14
Dependent Claim
10 words
The composite of claim 10 wherein the fibers are uncoated.
Claim 15
Dependent Claim
10 words
The composite of claim 7 wherein the fibers are uncoated.
Claim 16
Dependent Claim
46 words
A metal matrix composite comprising a substantially full density compact including Ti-10-2-3 alloy and about 10-20 volume % silicon nitride fibers substantially uniformly dispersed throughout the titanium alloy, the composite being further characterized by having essentially no evidence of secondary phase reaction at the fiber/metal interface.
Claim 17
Dependent Claim
46 words
A metal matrix composite comprising a substantially full density compact including Ti-10-2-3 alloy and about 10-20 volume % silicon nitride fibers substantially uniformly dispersed throughout the titanium alloy, the composite being further characterized by having essentially no evidence of secondary phase reaction at the fiber/metal interface.
Claim 18
Dependent Claim
18 words
The composite of claim 14 wherein the fibers are discontinuous whiskers having an aspect ratio of about 20-200.
Claim 19
Dependent Claim
57 words
A metal matrix composite consisting essentially of a titanium alloy matrix metal and Si 3 N 4 whiskers, the titanium alloy matrix metal being plastically deformed prior to compaction with the whiskers, the composite being characterized by essentially no secondary phase reaction at the interface between the metal and whiskers and being of substantially full theoretical density.
Claim 20
Dependent Claim
57 words
A metal matrix composite consisting essentially of a titanium alloy matrix metal and Si 3 N 4 whiskers, the titanium alloy matrix metal being plastically deformed prior to compaction with the whiskers, the composite being characterized by essentially no secondary phase reaction at the interface between the metal and whiskers and being of substantially full theoretical density.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-10-12 | 1991-04-13 | 1991-10-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-10-12 | 1995-04-13 | 1995-10-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-10-12 | 1999-04-13 | 1999-10-13 | $7700.00 | Window Closed / Lapsed |