Method of making a thermally stable composite honeycomb panel

Claim 1

A method for forming a thermally stable honeycomb panel comprised of a core member, a faceplate member, and a backplate member with each of said members being constructed of one or more thermally stable composite planks comprised of about 50% graphite fibers and of about 50% borosilicate glass and formed by hot pressing in vacuum, said method comprising first constructing a core member by a process A which comprises completing the steps (i-vii) of said process A as follows: (i) providing a plurality of said thermally stable composite planks having a predetermined length of l, predetermined width of w, and predetermined thickness of t; (ii) notching said planks individually along said length of l to form a series of equally spaced notches with a depth equal to 1/2w and a width equal to t; (iii) applying to each of said notched surfaces, a wet frit paste which additionally contains a volatile carrier to adjust fludity, said wet frit paste comprised of a borosilicate glass suspended in an organic binder designed to boil out completely below the glass melting temperature of said thermally stable planks, said borosilicate glass having a thermal expansion of from about 67 to about 46×10 -7 inch/inch/°C. over the temperature range from 0° C.-300° C. and a glass melting temperature of about 450° C. to about 600° C.; (iv) assembling said plurality of notched planks to form a series of square honeycomb cells and then allowing the assembled plurality of notched planks to dry at room temperature for a predetermined time period to allow the volatile carrier to evaporate; (v) completing a bonding process for the dried assembly which comprises placing the dried assembly in an oven in an air atmosphere and heating to a predetermined temperature which is melting point of the glass contained in said frit; (vi) maintaining the predetermined temperature long enough to ensure that the entire dried assembly has reached the proper temperature to achieve bonding; (vii) turning the oven off and allowing the dried assembly to cool to room temperature to yield a thermally stable core member; and said method further comprising completing process B set forth hereinbelow for forming said thermally stable honeycomb panel having said core member with a faceplate member and a backplace member bonded at the respective top and bottom outer surfaces thereof of said core member, said process B comprising completing the additional steps (viii-xi) of said process B as follows: (viii) providing a pair of said thermally stable composite planks of a predetermined length, width, and thickness to serve as a faceplate member and backplate member of said core member when bonded thereto; (ix) applying a wet frit paste, as defined in step (iii) of process A hereinabove, to the joining surface of said faceplate member and said backplate member and to said core member; (x) placing said backplate member on a flat surface, placing said core member with applied wet frit paste on top and bottom of exposed thermally stable plank edges, placing said faceplate member on top of said core member, and then allowing said core member, faceplate member, and backplate member to dry at room temperature for a predetermined time period to allow volatile carrier to evaporate; and (xi) completing an equivalent bonding process for the dried honeycomb panel comprised of said core member, said backplate member, and said faceplate member as defined in steps (v-vii) of process A hereinabove and additionally applying a small load on top of said faceplate member to ensure contact between the parts being bonded during said bonding process to thereby complete the forming of a thermally stable honeycomb panel.

Claim 2

A method for forming a thermally stable honeycomb panel comprised of a core member, a faceplate member, and a backplate member with each of said members being constructed of one or more thermally stable composite planks comprised of about 50% graphite fibers and of about 50% borosilicate glass and formed by hot pressing in vacuum, said method comprising first constructing a core member by a process A which comprises completing the steps (i-vii) of said process A as follows: (i) providing a plurality of said thermally stable composite planks having a predetermined length of l, predetermined width of w, and predetermined thickness of t; (ii) notching said planks individually along said length of l to form a series of equally spaced notches with a depth equal to 1/2w and a width equal to t; (iii) applying to each of said notched surfaces, a wet frit paste which additionally contains a volatile carrier to adjust fludity, said wet frit paste comprised of a borosilicate glass suspended in an organic binder designed to boil out completely below the glass melting temperature of said thermally stable planks, said borosilicate glass having a thermal expansion of from about 67 to about 46×10 -7 inch/inch/°C. over the temperature range from 0° C.-300° C. and a glass melting temperature of about 450° C. to about 600° C.; (iv) assembling said plurality of notched planks to form a series of square honeycomb cells and then allowing the assembled plurality of notched planks to dry at room temperature for a predetermined time period to allow the volatile carrier to evaporate; (v) completing a bonding process for the dried assembly which comprises placing the dried assembly in an oven in an air atmosphere and heating to a predetermined temperature which is melting point of the glass contained in said frit; (vi) maintaining the predetermined temperature long enough to ensure that the entire dried assembly has reached the proper temperature to achieve bonding; (vii) turning the oven off and allowing the dried assembly to cool to room temperature to yield a thermally stable core member; and said method further comprising completing process B set forth hereinbelow for forming said thermally stable honeycomb panel having said core member with a faceplate member and a backplace member bonded at the respective top and bottom outer surfaces thereof of said core member, said process B comprising completing the additional steps (viii-xi) of said process B as follows: (viii) providing a pair of said thermally stable composite planks of a predetermined length, width, and thickness to serve as a faceplate member and backplate member of said core member when bonded thereto; (ix) applying a wet frit paste, as defined in step (iii) of process A hereinabove, to the joining surface of said faceplate member and said backplate member and to said core member; (x) placing said backplate member on a flat surface, placing said core member with applied wet frit paste on top and bottom of exposed thermally stable plank edges, placing said faceplate member on top of said core member, and then allowing said core member, faceplate member, and backplate member to dry at room temperature for a predetermined time period to allow volatile carrier to evaporate; and (xi) completing an equivalent bonding process for the dried honeycomb panel comprised of said core member, said backplate member, and said faceplate member as defined in steps (v-vii) of process A hereinabove and additionally applying a small load on top of said faceplate member to ensure contact between the parts being bonded during said bonding process to thereby complete the forming of a thermally stable honeycomb panel.