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US4692223A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for polishing silicon wafers

Assignee: Siltronic AG
•
Filing: 1986-05-05
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Granted: 1987-09-08
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Expires: 2006-05-05
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Abstract

Abstract A process for polishing silicon wafers includes the step of carrying out last polishing step in the polishing operation in such a way that a protective film of silicon dioxide is produced on the surface of the polished wafer. The film does not interfere with e.g., the subsequent oxidation processes. The protective film protects the wafer surface from the many effects arising in subsequent processes which may unfavorably influence the quality of the surface.

Inventors

  • 👤 Ingolf Lampert
  • 👤 Herbert Jacob

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 05:36
CPC Classifications
C; C30; C30B; C30B29/00; C30B29/02; C30B29/06; C25; C25D; C25D11/00; C25D11/02; C25D11/32; C30B33/00

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 73 words
In a process for polishing silicon wafer surfaces, the improvement comprising the steps of: initially polishing the wafer surface in a conventional manner under alkaline conditions until a high quality of said polished surface is achieved; and thereafter, without interruption of the polishing, continuing and completing the polishing operation under oxidizing conditions by adding an oxidizing agent or anodic oxidation, thereby producing a film of silicon dioxide on the polished silicon wafer surface.
Claim 2
Dependent Claim 73 words
In a process for polishing silicon wafer surfaces, the improvement comprising the steps of: initially polishing the wafer surface in a conventional manner under alkaline conditions until a high quality of said polished surface is achieved; and thereafter, without interruption of the polishing, continuing and completing the polishing operation under oxidizing conditions by adding an oxidizing agent or anodic oxidation, thereby producing a film of silicon dioxide on the polished silicon wafer surface.
Claim 3
Dependent Claim 21 words
The process according to claim 1, wherein the silicon dioxide film is produced with a thickness of at least 10 Å.
Claim 4
Dependent Claim 30 words
The process according to claim 1, wherein the silicon dioxide film is produced by anodic oxidation by means of a voltage source in a circuit with anodically poled silicon wafers.
Claim 5
Dependent Claim 34 words
The process according to claim 1, wherein the silicon dioxide film is produced with an oxidizer having a potential in alkaline solution in excess of approximately 0.52 volts measured against a standard hydrogen electrode.
Claim 6
Dependent Claim 28 words
The process according to claim 4, wherein the oxidizer is a member selected from the group consisting of permanganates, peroxodisulfates, hypobromites, hypochlorites, hydrogen peroxide, and a combination thereof.
Claim 7
Dependent Claim 29 words
The process according to claim 4, wherein the oxidizer is a member selected from the group consisting of sodium salts, potassium salts, stable ammonium salts, and a combination thereof.
Claim 8
Dependent Claim 17 words
The process according to claim 4, wherein the oxidizer is in the form of an aqueous solution.
Claim 9
Dependent Claim 35 words
The process according to claim 4, wherein the oxidizer is added to a polishing agent in an amount such that the oxidizer makes up from approximately 0.1 to 2.0% by volume of the polishing agent.
Claim 10
Dependent Claim 28 words
The process according to claim 8, wherein after the oxidizer is added to the polishing agent, polishing of the wafer continues for from approximately 0.5 to 5.0 minutes.
Claim 11
Dependent Claim 31 words
The process according to claim 3, wherein a polishing disk serves as a cathode and a closed circuit is formed by a polishing cloth impregnated with an ionically conductive polishing agent.
Claim 12
Dependent Claim 28 words
The process according to claim 10, wherein a voltage of from approximately -1 to +2 volts measured against a Calomel electrode is established between the anode and cathode.
Claim 13
Dependent Claim 25 words
The process according to claim 10, wherein a current density of from approximately 0.1 to 5 mA/cm 2 is established between the anode and cathode.
Claim 14
Dependent Claim 18 words
The process according to claim 1, wherein the silicon wafers have a diameter of at least 125 mm.

References Cited (Backward Citations)

US2875384A Cited
US3377258A Cited
US3429080A Cited
US3764491A Cited
GB1449702A Cited
US4070797A Cited
US4064660A Cited
US4092445A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-09-07 1991-03-09 1991-09-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-09-07 1995-03-09 1995-09-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-09-07 1999-03-09 1999-09-08 $7700.00 Window Closed / Lapsed

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