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US4690776A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of manufacture of a toothpaste composition

Assignee: ROBELL RESEARCH Inc
•
Filing: 1986-01-08
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Granted: 1987-09-01
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Expires: 2006-01-08
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Abstract

Abstract A method of preparing a toothpaste composition by the steps of adding calcium phosphate in an amount of 0.5 to 5% by weight of the composition and sodium perborate in an amount of 0.5 to 5% by weight of the composition to hot water to form a first mixture and agitating the first mixture, adding to the first mixture sorbitol in an amount of 1 to 50% by weight of the composition, cornstarch in an amount of 0.5 to 10% by weight of the composition and aluminum hydroxide in an amount of 0.01 to 1% by weight of the composition to form a second mixture and agitating the second mixture, adding to the second mixture dicalcium phosphate in an amount of 1 to 50% by weight of the composition and sodium monofluoride phosphate in an amount of 0.7 to 0.8% by weight of the composition to form a third mixture and agitating the third mixture, adding to the third mixture sodium bicarbonate, in an amount of 1 to 50% by weight of the composition, gradually adding increments of a flavoring material in an amount of 0.05 to 2% to control any foaming and to facilitate release of gases to form a fourth mixture, and adding to the fourth mixture sodium lauryl sulfoacetate in an amount of 0.1 to 5% and gum in an amount of 0.5 to 5% and agitating the fourth mixture until a homogeneous paste composition is obtained.

Inventors

  • 👤 Irwin E. Smigel

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 09:57
CPC Classifications
A; A61; A61K; A61K8/00; A61K8/18; A61K8/19; A61K8/24; A61K8/22; A61K8/29; A61Q; A61Q11/00

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 237 words
A method of preparing a toothpaste composition comprising adding calcium phosphate in an amount of 0.5 to 5% by weight of the composition and sodium perborate in an amount of 0.5 to 5% by weight of the composition to hot water to form a first mixture and agitating the first mixture, adding to said first mixture sorbitol in an amount of 1 to 50% by weight of the composition, cornstarch in an amount of 0.5 to 10% by weight of the composition and aluminum hydroxide in an amount of 0.01 to 1% by weight of the composition to form a second mixture and agitating the second mixture, adding to said second mixture dicalcium phosphate in an amount of 1 to 50% by weight of the composition and sodium monofluoride phosphate in an amount of 0.7 to 0.8% by weight of the composition to form a third mixture and agitating the third mixture, adding to the third mixture sodium bicarbonate, in an amount of 1 to 50% by weight of the composition, gradually adding increments of a flavoring material in an amount of 0.05 to 2% to control any foaming and to facilitate release of gases to form a fourth mixture, and adding to the fourth mixture sodium lauryl sulfoacetate in an amount of 0.1 to 5% and gum in an amount of 0.5 to 5% and agitating the fourth mixture until a homogeneous paste composition is obtained.
Claim 2
Independent Claim 237 words
A method of preparing a toothpaste composition comprising adding calcium phosphate in an amount of 0.5 to 5% by weight of the composition and sodium perborate in an amount of 0.5 to 5% by weight of the composition to hot water to form a first mixture and agitating the first mixture, adding to said first mixture sorbitol in an amount of 1 to 50% by weight of the composition, cornstarch in an amount of 0.5 to 10% by weight of the composition and aluminum hydroxide in an amount of 0.01 to 1% by weight of the composition to form a second mixture and agitating the second mixture, adding to said second mixture dicalcium phosphate in an amount of 1 to 50% by weight of the composition and sodium monofluoride phosphate in an amount of 0.7 to 0.8% by weight of the composition to form a third mixture and agitating the third mixture, adding to the third mixture sodium bicarbonate, in an amount of 1 to 50% by weight of the composition, gradually adding increments of a flavoring material in an amount of 0.05 to 2% to control any foaming and to facilitate release of gases to form a fourth mixture, and adding to the fourth mixture sodium lauryl sulfoacetate in an amount of 0.1 to 5% and gum in an amount of 0.5 to 5% and agitating the fourth mixture until a homogeneous paste composition is obtained.
Claim 3
Dependent Claim 16 words
A method as claimed in claim 1 wherein the water is initially heated to 150° F.
Claim 4
Dependent Claim 20 words
A method as claimed in claim 2 wherein the first, second and third mixtures are each agitated for ten minutes.
Claim 5
Dependent Claim 30 words
A method as claimed in claim 2 comprising adding an alkylparaben in an amount of 0.05 to 1.0% by weight of the composition to the second mixture before agitation thereof.
Claim 6
Dependent Claim 45 words
A method as claimed in claim 2 comprising adding calcium carbonate in an amount of 1 to 50% by weight of the composition and magnesium carbonate in an amount of 1 to 25% by weight of the composition to the third mixture before agitation thereof.
Claim 7
Dependent Claim 58 words
A method as claimed in claim 2 comprising adding to the fourth mixture titanium dioxide as a whitening agent in an amount of 0.1 to 10% by weight of the composition and saccharinate in an amount of from 0.05 to 2% by weight of the composition and the resulting mixture is agitated for at least one half hour.
Claim 8
Dependent Claim 31 words
A method as claimed in claim 2 comprising adding a cellulose gum in an amount of 0.5 to 5% by weight of the composition to the fourth mixture before agitation thereof.

References Cited (Backward Citations)

US2751328A Cited
US4066745A Cited
US4029760A Cited
US4353890A Cited
US4405599A Cited
US4603045A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-08-31 1991-03-02 1991-09-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-08-31 1995-03-02 1995-09-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-08-31 1999-03-02 1999-09-01 $7700.00 Window Closed / Lapsed

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