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US4668263A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for producing glass preform for optical fiber

Assignee: Sumitomo Electric Industries Ltd
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Filing: 1985-11-04
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Granted: 1987-05-26
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Expires: 2005-11-04
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Abstract

Abstract A rod-in-tube method for producing a glass preform for use in the fabrication of an optical fiber, which comprises steps of inserting a glass rod as a core material in a glass tube as a cladding material, fusing and closing one end of the cladding material, filling a gap between the core and cladding materials with an atmosphere containing at least one gaseous halogen-containing compound and then heating the core and cladding materials at a temperature not lower than 1,900° C. to collapse the gap between them and to fuse them together, from which glass preform, an optical fiber with low attenuation of light transmission is fabricated.

Inventors

  • 👤 Hiroshi Yokota
  • 👤 Gotaro Tanaka
  • 👤 Hiroo Kanamori
  • 👤 Futoshi Mizutani
  • 👤 Toshio Danzuka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 22:44
CPC Classifications
C; C03; C03B; C03B37/00; C03B37/01; C03B37/012; C03B37/01205; C03B37/01211; Y; Y10; Y10S; Y10S65/00; Y10S65/15; Y10S65/16; Y10S65/90

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 182 words
A rod-in-tube method of producing a glass preform suitable for use in the fabrication of an optical fiber, said method comprising the steps of: (a) inserting a core-material glass rod in a cladding-material glass tube; (b) fusing and closing the end portion of one end of the cladding-material glass tube while filling a gap between the core-material glass rod and the cladding-material glass tube with a vapor containing at least one gaseous halogen-containing compound; (c) immediately prior to fusing the entire circumference of said end portion of the cladding-material glass tube with the core-material glass rod, opening a valve connected to a feed system for performing said filling and to an exhaust system and adjusting the flow of the gaseous halogen-containing compound by exhausting some of the vapor being fed toward the gap any further increase of the pressure in the gap; and (d) heating the core-material glass rod and the cladding-material glass tube at a temperature not lower than 1,900° C. in order to collapse the gap between the core-material glass rod and the cladding-material glass tube and fuse them together.
Claim 2
Dependent Claim 182 words
A rod-in-tube method of producing a glass preform suitable for use in the fabrication of an optical fiber, said method comprising the steps of: (a) inserting a core-material glass rod in a cladding-material glass tube; (b) fusing and closing the end portion of one end of the cladding-material glass tube while filling a gap between the core-material glass rod and the cladding-material glass tube with a vapor containing at least one gaseous halogen-containing compound; (c) immediately prior to fusing the entire circumference of said end portion of the cladding-material glass tube with the core-material glass rod, opening a valve connected to a feed system for performing said filling and to an exhaust system and adjusting the flow of the gaseous halogen-containing compound by exhausting some of the vapor being fed toward the gap any further increase of the pressure in the gap; and (d) heating the core-material glass rod and the cladding-material glass tube at a temperature not lower than 1,900° C. in order to collapse the gap between the core-material glass rod and the cladding-material glass tube and fuse them together.
Claim 3
Dependent Claim 42 words
The rod-in-tube method according to claim 1, wherein the halogen-containing compound is at least one of SF 6 , CCl 2 F 2 , CF 4 , SiF 4 , NF 3 , F 2 , Cl 2 and SOCl 2 .
Claim 4
Dependent Claim 35 words
The rod-in-tube method according to claim 1, wherein an inner surface of the cladding material glass tube is etched with a gas comprising a fluorine-containing compound prior to the insertion of the core-material glass rod.
Claim 5
Dependent Claim 16 words
The rod-in-tube method according to claim 3, wherein the etching gas further comprises a chlorine-containing compound.
Claim 6
Dependent Claim 31 words
The rod-in-tube method according to claim 1, wherein the core-material glass rod is inserted in the cladding-material glass tube while the gaseous halogen-containing compound is injected in the cladding-material glass tube.
Claim 7
Dependent Claim 15 words
The rod-in-tube method according to claim 5, wherein the halogen-containing compound is a chlorine-containing compound.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-05-25 1990-11-24 1991-05-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-05-25 1994-11-24 1995-05-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-05-25 1998-11-24 1999-05-26 $7700.00 Window Closed / Lapsed

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