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US4649165A Expired / Lapsed US ⏱️ 0.0 years remaining

Dental filling material comprising polymerizable (meth)acrylic compound, X-ray opaque fillers and microfiller

Assignee: Blendax GmbH
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Filing: 1985-01-26
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Granted: 1987-03-10
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Expires: 2005-01-26
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Abstract

Abstract Dental filling material on the basis of polymerizable compounds and an inorganic filler mixture with improved properties, particularly excellent X-ray opacity and polishability, where the filler mixture essentially consists of an X-ray opaque filler with a particle size distribution of between 0,5 and 40 μm, an X-ray opaque filler with a particle size distribution of between 0,2 and 15 μm and a microfiller, particularly colloidal silica, with a particle size distribution of between 5 and 150 nm.

Inventors

  • 👤 Werner Kuhlmann

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 22:34
CPC Classifications
A; A61; A61K; A61K6/00; A61K6/80; A61K6/884; A61K6/887

Claims Analysis

Total Claims: 10
Claim 1
Independent Claim 142 words
Dental filling material comprising (i) one or more polymerizable (meth) acrylic compounds, (ii) polymerization accelerators, polymerization initiators or mixtures thereof and about 60 to 90% by weight, based on the total composition, of an inorganic filler mixture of at least two X-ray opaque fillers with different particle size distribution which comprises: (a) about 5 to 20% by weight, based on the total filler mixture, of at least one X-ray opaque filler with a particle size distribution of between 0.5 to 40 micrometers, (b) about 20 to 40% by weight, based on the total filler mixture, of at least one X-ray opaque filler with a particle size distribution of between 0.2 and 15 micrometers, and (c) about 40 to 75% by weight, based on the total filler mixture, of at least one microfiller with a particle size distribution between 5 and 150 nanometers.
Claim 2
Dependent Claim 142 words
Dental filling material comprising (i) one or more polymerizable (meth) acrylic compounds, (ii) polymerization accelerators, polymerization initiators or mixtures thereof and about 60 to 90% by weight, based on the total composition, of an inorganic filler mixture of at least two X-ray opaque fillers with different particle size distribution which comprises: (a) about 5 to 20% by weight, based on the total filler mixture, of at least one X-ray opaque filler with a particle size distribution of between 0.5 to 40 micrometers, (b) about 20 to 40% by weight, based on the total filler mixture, of at least one X-ray opaque filler with a particle size distribution of between 0.2 and 15 micrometers, and (c) about 40 to 75% by weight, based on the total filler mixture, of at least one microfiller with a particle size distribution between 5 and 150 nanometers.
Claim 3
Dependent Claim 23 words
Dental filling material according to claim 1 containing about 10 to 15% by weight, based on the total filler mixture, of filler (a).
Claim 4
Dependent Claim 23 words
Dental filling material according to claim 1 containing about 25 to 35% by weight, based on the total filler mixture, of filler (b).
Claim 5
Dependent Claim 23 words
Dental filling material according to claim 1 containing about 55 to 65% by weight, based on the total filler mixture, of microfiller (c).
Claim 6
Dependent Claim 13 words
Dental filling material according to claim 1 wherein the microfiller is colloidal silica.
Claim 7
Dependent Claim 22 words
Dental filling material according to claim 1 wherein the microfiller (c) has an average particle size of about 30 to 60 nanometers.
Claim 8
Dependent Claim 42 words
Dental filling material according to claim 1 wherein filler (a) has the following particle size distribution: ______________________________________ about 5% 0.5-1 micrometers, about 10% 1-2 micrometers, about 20% 2-5 micrometers, about 20% 5-10 micrometers, about 30% 10-20 micrometers, about 15% 20-40 micrometers, ______________________________________
Claim 9
Dependent Claim 42 words
Dental filling material according to claim 1 wherein filler (b) has the following particle size distribution: ______________________________________ about 5% 0.2-0.5 micrometers, about 10% 0.5-1 micrometers, about 15% 1-2 micrometers, about 45% 2-5 micrometers, about 20% 5-10 micrometers, about 5% 10-15 micrometers. ______________________________________
Claim 10
Dependent Claim 21 words
Dental filling material according to claim 1 wherein at least one of filler (a), filler (b) and microfiller (c) is silanized.

References Cited (Backward Citations)

US4394465A Cited
US4389497A Cited
US4297266A Cited
US4407984A Cited
US4427799A Cited
US4388069A Cited
US4544359A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-03-09 1990-09-08 1991-03-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-03-09 1994-09-08 1995-03-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-03-09 1998-09-08 1999-03-10 $7700.00 Window Closed / Lapsed

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