US4645749A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Water soluble compositions for preparing analytical solutions
Assignee: Nortel Networks Ltd
•
Filing: 1985-06-26
•
Granted: 1987-02-24
•
Expires: 2005-06-26
Abstract
Abstract Low concentration standard aqueous solution for analytical purposes is prepared from a water soluble glass body containing the standardizing material. The glasses are phosphorus pentoxide based glasses and provide release rates, e.g. of Na ++ , of 0.01 to 100 micrograms per cm 2 per hour.
Inventors
- 👤 Cyril F. Drake
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 09:58
CPC Classifications
C; C03; C03C; C03C4/00; C03C4/0035; C03C3/00; C03C3/12; C03C3/16
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
123 words
A water soluble body for the preparation of an aqueous analytical solution of a trace concentration of a metallic ion by dissolution of the body at a substantially constant predetermined rate, wherein said body consists of a water soluble glass composition incorporating phosphorus pentoxide as a glass forming oxide, wherein the glass incorporates glass modifying oxides including an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hour.
Claim 2
Dependent Claim
123 words
A water soluble body for the preparation of an aqueous analytical solution of a trace concentration of a metallic ion by dissolution of the body at a substantially constant predetermined rate, wherein said body consists of a water soluble glass composition incorporating phosphorus pentoxide as a glass forming oxide, wherein the glass incorporates glass modifying oxides including an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hour.
Claim 3
Dependent Claim
36 words
A body as claimed in claim 1, wheein the metallic ion is sodium, and wherein the sodium is provided in the form of sodium oxide at a concentration of 2.6 mole percent to 27.8 mole percent.
Claim 4
Dependent Claim
16 words
A body as claimed in claim 2 or 1 and in the form of a tube.
Claim 5
Dependent Claim
33 words
A body as claimed in claim 2 or 1 and comprising a plurality of platelets, wherein the ratio of the largest diameter to the thickness of said platelets is not less than 10:1.
Claim 6
Dependent Claim
159 words
A cartridge for the preparation of an analytical solution of a trace concentration of a metallic ion, the cartridge comprising an inert housing having an inlet and an outlet for the passage of water therethrough, a water soluble glass body disposed in the housing and adapted to release the metallic ion at a substantially constant predetermined rate on dissolution, and means for retaining the body in the housing, wherein said body consists of a water soluble glass composition incorporating phosphorous pentoxide as a glass forming oxide, wherein said glass incorporates an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when the glass is contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hours.
Claim 7
Dependent Claim
159 words
A cartridge for the preparation of an analytical solution of a trace concentration of a metallic ion, the cartridge comprising an inert housing having an inlet and an outlet for the passage of water therethrough, a water soluble glass body disposed in the housing and adapted to release the metallic ion at a substantially constant predetermined rate on dissolution, and means for retaining the body in the housing, wherein said body consists of a water soluble glass composition incorporating phosphorous pentoxide as a glass forming oxide, wherein said glass incorporates an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when the glass is contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hours.
Claim 8
Dependent Claim
35 words
A cartridge as claimed in claim 5, wherein said glass consists essentially of 2.6 to 27.8 mole % sodium oxide, 33.7 to 51.5 mole % calcium oxide and 38.5 to 45.9 mole % phosphorus pentoxide.
Claim 9
Dependent Claim
30 words
A standard analytical solution of a trace quantity of a cation prepared from a glass body as claimed in claim 1 or from a cartridge as claimed in claim 5.
References Cited (Backward Citations)
US2370472A
Cited
US3272588A
Cited
GB1078765A
Cited
GB1155113A
Cited
GB1149274A
Cited
US3640827A
Cited
GB1298605A
Cited
GB2057420A
Cited
GB2073732A
Cited
US4449981A
Cited
US4482541A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-02-23 | 1990-08-25 | 1991-02-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-02-23 | 1994-08-25 | 1995-02-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-02-23 | 1998-08-25 | 1999-02-24 | $7700.00 | Window Closed / Lapsed |