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US4645749A Expired / Lapsed US ⏱️ 0.0 years remaining

Water soluble compositions for preparing analytical solutions

Assignee: Nortel Networks Ltd
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Filing: 1985-06-26
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Granted: 1987-02-24
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Expires: 2005-06-26
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Abstract

Abstract Low concentration standard aqueous solution for analytical purposes is prepared from a water soluble glass body containing the standardizing material. The glasses are phosphorus pentoxide based glasses and provide release rates, e.g. of Na ++ , of 0.01 to 100 micrograms per cm 2 per hour.

Inventors

  • 👤 Cyril F. Drake

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 09:58
CPC Classifications
C; C03; C03C; C03C4/00; C03C4/0035; C03C3/00; C03C3/12; C03C3/16

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 123 words
A water soluble body for the preparation of an aqueous analytical solution of a trace concentration of a metallic ion by dissolution of the body at a substantially constant predetermined rate, wherein said body consists of a water soluble glass composition incorporating phosphorus pentoxide as a glass forming oxide, wherein the glass incorporates glass modifying oxides including an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hour.
Claim 2
Dependent Claim 123 words
A water soluble body for the preparation of an aqueous analytical solution of a trace concentration of a metallic ion by dissolution of the body at a substantially constant predetermined rate, wherein said body consists of a water soluble glass composition incorporating phosphorus pentoxide as a glass forming oxide, wherein the glass incorporates glass modifying oxides including an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hour.
Claim 3
Dependent Claim 36 words
A body as claimed in claim 1, wheein the metallic ion is sodium, and wherein the sodium is provided in the form of sodium oxide at a concentration of 2.6 mole percent to 27.8 mole percent.
Claim 4
Dependent Claim 16 words
A body as claimed in claim 2 or 1 and in the form of a tube.
Claim 5
Dependent Claim 33 words
A body as claimed in claim 2 or 1 and comprising a plurality of platelets, wherein the ratio of the largest diameter to the thickness of said platelets is not less than 10:1.
Claim 6
Dependent Claim 159 words
A cartridge for the preparation of an analytical solution of a trace concentration of a metallic ion, the cartridge comprising an inert housing having an inlet and an outlet for the passage of water therethrough, a water soluble glass body disposed in the housing and adapted to release the metallic ion at a substantially constant predetermined rate on dissolution, and means for retaining the body in the housing, wherein said body consists of a water soluble glass composition incorporating phosphorous pentoxide as a glass forming oxide, wherein said glass incorporates an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when the glass is contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hours.
Claim 7
Dependent Claim 159 words
A cartridge for the preparation of an analytical solution of a trace concentration of a metallic ion, the cartridge comprising an inert housing having an inlet and an outlet for the passage of water therethrough, a water soluble glass body disposed in the housing and adapted to release the metallic ion at a substantially constant predetermined rate on dissolution, and means for retaining the body in the housing, wherein said body consists of a water soluble glass composition incorporating phosphorous pentoxide as a glass forming oxide, wherein said glass incorporates an oxide of said metal and calcium oxide, wherein the concentration of phosphorus pentoxide in the glass is between 38.5 mole percent and 45.9 mole percent, and wherein the calcium oxide concentration is between 33.7 mole percent and 51.5 mole percent such that, when the glass is contacted with pure water, the metallic ion is released at a rate of 0.01 to 100 micrograms per cm 2 per hours.
Claim 8
Dependent Claim 35 words
A cartridge as claimed in claim 5, wherein said glass consists essentially of 2.6 to 27.8 mole % sodium oxide, 33.7 to 51.5 mole % calcium oxide and 38.5 to 45.9 mole % phosphorus pentoxide.
Claim 9
Dependent Claim 30 words
A standard analytical solution of a trace quantity of a cation prepared from a glass body as claimed in claim 1 or from a cartridge as claimed in claim 5.

References Cited (Backward Citations)

US2370472A Cited
US3272588A Cited
GB1078765A Cited
GB1155113A Cited
GB1149274A Cited
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US4482541A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-02-23 1990-08-25 1991-02-24 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-02-23 1994-08-25 1995-02-24 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-02-23 1998-08-25 1999-02-24 $7700.00 Window Closed / Lapsed

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