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US4643854A Expired / Lapsed US ⏱️ 0.0 years remaining

Shell forming system

Assignee: California Institute of Technology
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Filing: 1984-08-15
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Granted: 1987-02-17
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Expires: 2004-08-15
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Abstract

Abstract An apparatus is provided for forming gas-filled spheres of metal, glass or other material, which produces spheres (12) of uniform size and wall thickness in a relatively simple system. The system includes concentric nozzles, including an inner nozzle (18) through which gas flows and and an outer nozzle (20), which jointly define an annular passageway (50) through which a liquid flows. The flow rates are adjusted so that the gas flows at greater velocity than does the liquid, out of their respective nozzles, e.g. three times as great, in order to produce an extrusion (30) which undergoes axisymmetric oscillations resulting in the pinch off into hollow spheres with very uniform spacing. The system is useful not only where gas-filled spheres are required, but also is useful to accurately control the dispensing of solid, liquid, or gaseous materials.

Inventors

  • 👤 James M. Kendall, Jr.
  • 👤 Taylor G. Wang
  • 👤 Daniel D. Elleman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-30 06:33
CPC Classifications
B; B22; B22F; B22F9/00; B22F9/02; B22F9/06; B22F9/08; B22F9/082; B01; B01J; B01J13/00; B01J13/02; B01J13/04; B22D; B22D25/00; B22D25/02; B22F1/00; B22F1/06; B22F1/065; B22F1/0655; B29; B29C; B29C49/00; B29C49/0042; C; C03; C03B; C03B19/00; C03B19/10; B22F2009/088

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 76 words
A method for forming hollow shells, comprising: emitting gas through a nozzle; and emitting liquid through an annular area surrounding said nozzle to form a hollow extrusion; said steps of emitting including moving said gas out of said nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through said annular area, whereby to enable spontaneous pinch-off of said hollow extrusion into said hollow shells.
Claim 2
Independent Claim 76 words
A method for forming hollow shells, comprising: emitting gas through a nozzle; and emitting liquid through an annular area surrounding said nozzle to form a hollow extrusion; said steps of emitting including moving said gas out of said nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through said annular area, whereby to enable spontaneous pinch-off of said hollow extrusion into said hollow shells.
Claim 3
Dependent Claim 36 words
The method described in claim 1 wherein: the velocity V in centimeters of the liquid through said annular area is at least equal to 11/√D where D is the thickness of said annular area in centimeters.
Claim 4
Independent Claim 130 words
A method for dispensing droplets of initially liquid material, of uniform mass, comprising: emitting a gas through an inner nozzle; and emitting said liquid material through an annular space that lies between said inner nozzle and an outer nozzle that surrounds said inner nozzle to form a hollow extrusion; said steps of emitting including moving said gas through the downstream end of said inner nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through the downstream end of said annular space, and controlling the environment in front of said nozzles so it is substantially free of winds that would deflect the emitted gas and liquid sidewardly, whereby to enable spontaneous pinch-off of said hollow extrusion into hollow spheres.
Claim 5
Independent Claim 130 words
A method for dispensing droplets of initially liquid material, of uniform mass, comprising: emitting a gas through an inner nozzle; and emitting said liquid material through an annular space that lies between said inner nozzle and an outer nozzle that surrounds said inner nozzle to form a hollow extrusion; said steps of emitting including moving said gas through the downstream end of said inner nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through the downstream end of said annular space, and controlling the environment in front of said nozzles so it is substantially free of winds that would deflect the emitted gas and liquid sidewardly, whereby to enable spontaneous pinch-off of said hollow extrusion into hollow spheres.
Claim 6
Dependent Claim 41 words
The method described in claim 3 wherein: said step of emitting said gas includes emitting said gas from the tip of the inner nozzle into the surrounding environment at a location forward of the location where said liquid material is emitted.
Claim 7
Independent Claim 175 words
A method for dispensing droplets of initially liquid material, of uniform mass, comprising: emitting a gas through an inner nozzle; and emitting said liquid material through an annular space that lies between said inner nozzle and an outer nozzle that surrounds said inner nozzle; said steps of emitting including moving said gas through the downstream end of said inner nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through the downstream end of said annular space, and controlling the environment in front of said nozzles so it is substantially free of winds that would deflect that emitted gas and liquid sidewardly; the velocity of said liquid is at least about as great as the velocity V given by the following equation: V=[2S/RD]1/2 where V is the velocity in cm/sec, S is the surface tension of the liquid in dynes/cm, R is the density of the liquid in gm/cm 3 , and D is the clearance between said inner and outer nozzles in cm.
Claim 8
Independent Claim 175 words
A method for dispensing droplets of initially liquid material, of uniform mass, comprising: emitting a gas through an inner nozzle; and emitting said liquid material through an annular space that lies between said inner nozzle and an outer nozzle that surrounds said inner nozzle; said steps of emitting including moving said gas through the downstream end of said inner nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through the downstream end of said annular space, and controlling the environment in front of said nozzles so it is substantially free of winds that would deflect that emitted gas and liquid sidewardly; the velocity of said liquid is at least about as great as the velocity V given by the following equation: V=[2S/RD]1/2 where V is the velocity in cm/sec, S is the surface tension of the liquid in dynes/cm, R is the density of the liquid in gm/cm 3 , and D is the clearance between said inner and outer nozzles in cm.
Claim 9
Independent Claim 128 words
A method for forming hollow shells, comprising: emitting gas through an inner nozzle; and emitting liquid through an annular area between an outer nozzle that surrounds said inner nozzle and said inner nozzle to form a hollow extrusion; said steps of emitting including moving said gas out of said inner nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through said annular area; said outer nozzle has an inside diameter on the order of 4 millimeters, the clearance between said nozzles is on the order of three-quarters millimeter, and the velocity of the liquid is on the order of one meter per second, whereby to enable spontaneous pinch-off of said hollow extrusion into said hollow shells.
Claim 10
Independent Claim 128 words
A method for forming hollow shells, comprising: emitting gas through an inner nozzle; and emitting liquid through an annular area between an outer nozzle that surrounds said inner nozzle and said inner nozzle to form a hollow extrusion; said steps of emitting including moving said gas out of said inner nozzle at a velocity which is between about 1.3 and 10 times greater than the velocity of emission of said liquid through said annular area; said outer nozzle has an inside diameter on the order of 4 millimeters, the clearance between said nozzles is on the order of three-quarters millimeter, and the velocity of the liquid is on the order of one meter per second, whereby to enable spontaneous pinch-off of said hollow extrusion into said hollow shells.
Claim 11
Independent Claim 109 words
A method for forming hollow shells, comprising: emitting gas through a nozzle; and emitting liquid through an annular area surrounding said nozzle to form a hollow extrusion; said steps of emitting including moving said gas out of said nozzle at a velocity which is between 1.3 and 10 times greater than the velocity of emission of said liquid through said annular area; the velocity of said liquid which is emitted from said annular area being greater than the velocity of surface tension waves in the liquid material which surrounds the gas in the gas-filled liquid extrusion, whereby to enable spontaneous pinch-off of said hollow extrusion into said hollow shells.
Claim 12
Independent Claim 109 words
A method for forming hollow shells, comprising: emitting gas through a nozzle; and emitting liquid through an annular area surrounding said nozzle to form a hollow extrusion; said steps of emitting including moving said gas out of said nozzle at a velocity which is between 1.3 and 10 times greater than the velocity of emission of said liquid through said annular area; the velocity of said liquid which is emitted from said annular area being greater than the velocity of surface tension waves in the liquid material which surrounds the gas in the gas-filled liquid extrusion, whereby to enable spontaneous pinch-off of said hollow extrusion into said hollow shells.
Claim 13
Dependent Claim 74 words
The method described in claim 7 wherein: the velocity V of said liquid which is emitted from said annular area is at least about as great as that given by the following equation: V=[2S/RD]1/2 where V is the liquid velocity in cm/sec, S is the surface tension of the liquid in dynes/cm, R is the density of the liquid in gm/cm 3 , and D is the thickness of said annular area in cm.
Claim 14
Dependent Claim 34 words
The method described in claim 7 wherein: said steps of emitting include moving said gas out of said nozzle at a velocity about three times the velocity of the liquid through the annular space.

References Cited (Backward Citations)

US4166084A Cited
US4344787A Cited
US4303431A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1990-02-16 1990-08-18 1991-02-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1994-02-16 1994-08-18 1995-02-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1998-02-16 1998-08-18 1999-02-17 $7700.00 Window Closed / Lapsed

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