US4636336A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for drying a chelating agent
Assignee: Boeing North American Inc
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Filing: 1984-11-02
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Granted: 1987-01-13
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Expires: 2004-11-02
Abstract
Abstract A process is described for reducing the volume of a liquid waste containing an organic amine chelating agent in which a finely atomized spray of the liquid waste is contacted with a gas stream having a temperature in excess of the thermal decomposition temperature of the chelating agent. The proportions of the hot gas stream and liquid waste are controlled to rapidly evaporate water from the liquid waste and cool the gas to a temperature below the decomposition temperature of the chelating agent in a time of less than about 6 seconds to produce a dry, flowable powder product including the chelating agent.
Inventors
- 👤 Richard L. Gay
- 👤 LeRoy F. Grantham
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 21:59
CPC Classifications
G; G21; G21F; G21F9/00; G21F9/04; G21F9/06; G21F9/14; Y; Y10; Y10S; Y10S159/00; Y10S159/12
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
171 words
A process for reducing the volume of a low-level radioactive liquid waste containing an organic amine chelating agent comprising: burning a fuel and an oxygen-containing gas to produce a hot gas stream having a temperature in excess of the thermal decomposition temperature of the chelating agent; introducing the hot gas stream into a spray drying zone; introducing a finely atomized spray of said liquid waste into said spray drying zone and into intimate contact with said hot gas stream; controlling the proportions of said hot gas stream and said liquid waste to rapidly evaporate water from said liquid waste and cool said hot gas to a temperature below the decomposition temperature of said chelating agent in a time of less than six seconds to produce (a) a dry, flowable powder product including said chelating agent, and (b) a product gas substantially free of any gaseous products of said chelating agent and volatile fission products of the radioactive constituents of said liquid waste; and separating said powder product from said product gas.
Claim 2
Dependent Claim
171 words
A process for reducing the volume of a low-level radioactive liquid waste containing an organic amine chelating agent comprising: burning a fuel and an oxygen-containing gas to produce a hot gas stream having a temperature in excess of the thermal decomposition temperature of the chelating agent; introducing the hot gas stream into a spray drying zone; introducing a finely atomized spray of said liquid waste into said spray drying zone and into intimate contact with said hot gas stream; controlling the proportions of said hot gas stream and said liquid waste to rapidly evaporate water from said liquid waste and cool said hot gas to a temperature below the decomposition temperature of said chelating agent in a time of less than six seconds to produce (a) a dry, flowable powder product including said chelating agent, and (b) a product gas substantially free of any gaseous products of said chelating agent and volatile fission products of the radioactive constituents of said liquid waste; and separating said powder product from said product gas.
Claim 3
Dependent Claim
15 words
The process of claim 1 wherein said chelating agent is an organic amine acid compound.
Claim 4
Dependent Claim
21 words
The process of claim 2 wherein said chelating agent is selected from the group consisting of EDTA, DTPA, HEDTA and NTA.
Claim 5
Dependent Claim
21 words
The process of claim 3 wherein said hot gas stream has a temperature within the range of 250° to 400° C.
Claim 6
Dependent Claim
34 words
The process of claim 4 wherein said hot gas is cooled to a temperature of from about 150° to 200° C. in a time within the range of from about 1 to 6 seconds.
Claim 7
Dependent Claim
19 words
The process of claim 5 wherein said time is within the range of from about 1.5 to 3 seconds.
Claim 8
Dependent Claim
11 words
The process of claim 6 wherein said chelating agent is EDTA.
Claim 9
Dependent Claim
30 words
The process of claim 5 wherein the gas is further cooled to a temperature of less than about 90° C. prior to separating said powder product from said product gas.
References Cited (Backward Citations)
US3008904A
Cited
US3101258A
Cited
US3922974A
Cited
US4235738A
Cited
US4053432A
Cited
US4145396A
Cited
US4285830A
Cited
DE2907984A1
Cited
JPS5594199A
Cited
US4499833A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-01-12 | 1990-07-14 | 1991-01-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-01-12 | 1994-07-14 | 1995-01-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-01-12 | 1998-07-14 | 1999-01-13 | $7700.00 | Window Closed / Lapsed |