US4608356A
Expired / Lapsed
US
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Preparation of a reforming catalyst
Assignee: Chevron USA Inc
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Filing: 1984-12-20
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Granted: 1986-08-26
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Expires: 2004-12-20
Abstract
Abstract A method of preparing a reforming catalyst is disclosed wherein a large-pore zeolite is impregnated with an aqueous solution of platinum and the zeolite is only allowed to soak in the solution for less than three hours to form a catalyst. After the catalyst is dried, it is calcined in an atmosphere containing steam.
Inventors
- 👤 Waldeen C. Buss
- 👤 Charles R. Wilson
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 14:56
CPC Classifications
C; C10; C10G; C10G35/00; C10G35/04; C10G35/06; C10G35/095; B; B01; B01J; B01J29/00; B01J29/04; B01J29/06; B01J29/064
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
58 words
A method of preparing a reforming catalyst comprising the steps of: (a) impregnating a large-pore zeolite with an aqueous solution of a Group VIII metal and allowing said zeolite to soak in said solution for less than three hours to form a catalyst; (b) drying said catalyst; and (c) calcining said dried catalyst in an atmosphere containing steam.
Claim 2
Independent Claim
58 words
A method of preparing a reforming catalyst comprising the steps of: (a) impregnating a large-pore zeolite with an aqueous solution of a Group VIII metal and allowing said zeolite to soak in said solution for less than three hours to form a catalyst; (b) drying said catalyst; and (c) calcining said dried catalyst in an atmosphere containing steam.
Claim 3
Independent Claim
83 words
A method of preparing a reforming catalyst comprising the steps of: (a) mixing a large-pore zeolite with an inorganic oxide binder; (b) extruding said mixture to form an extrudate; (c) drying and calcining said extrudate; (d) impregnating said calcined extrudate with an aqueous solution of a Group VIII metal and allowing said calcined extrudate to soak in said solution for less than three hours to form a catalyst; (e) drying said catalyst; and (f) calcining said dried catalyst in an atmosphere contaning steam.
Claim 4
Independent Claim
83 words
A method of preparing a reforming catalyst comprising the steps of: (a) mixing a large-pore zeolite with an inorganic oxide binder; (b) extruding said mixture to form an extrudate; (c) drying and calcining said extrudate; (d) impregnating said calcined extrudate with an aqueous solution of a Group VIII metal and allowing said calcined extrudate to soak in said solution for less than three hours to form a catalyst; (e) drying said catalyst; and (f) calcining said dried catalyst in an atmosphere contaning steam.
Claim 5
Dependent Claim
26 words
A method of preparing a reforming catalyst according to claim 2 wherein said large-pore zeolite has an apparent pore size of from 7 to 9 Angstroms.
Claim 6
Dependent Claim
30 words
A method of preparing a reforming catalyst according to claim 3 wherein said large-pore zeolite is selected from the group consisting of zeolite X, zeolite Y, and type L zeolite.
Claim 7
Dependent Claim
20 words
A method of preparing a reforming catalyst according to claim 4 wherein said large-pore zeolite is a type L zeolite.
Claim 8
Independent Claim
139 words
A method of preparing a reforming catalyst comprising the steps of: (a) mixing a type L zeolite with an inorganic oxide binder, wherein said inorganic oxide is selected from the group consisting of silica, alumina, and aluminosilicates; (b) extruding said mixture to form an extrudate; (c) drying and calcining said extrudate; (d) ion exchanging said calcined extrudate with an aqueous solution of an alkaline earth metal selected from the group consisting of barium, strontium, and calcium; (e) drying and calcining said ion exchanged extrudate; (f) impregnating said calcined extrudate with an aqueous solution of a Group VIII metal and allowing said calcined extrudate to soak in said solution for less than three hours to form a catalyst; (g) drying said catalyst; and (h) calcining said dried catalyst with steam in air, wherein said air has at least 3% steam.
Claim 9
Independent Claim
139 words
A method of preparing a reforming catalyst comprising the steps of: (a) mixing a type L zeolite with an inorganic oxide binder, wherein said inorganic oxide is selected from the group consisting of silica, alumina, and aluminosilicates; (b) extruding said mixture to form an extrudate; (c) drying and calcining said extrudate; (d) ion exchanging said calcined extrudate with an aqueous solution of an alkaline earth metal selected from the group consisting of barium, strontium, and calcium; (e) drying and calcining said ion exchanged extrudate; (f) impregnating said calcined extrudate with an aqueous solution of a Group VIII metal and allowing said calcined extrudate to soak in said solution for less than three hours to form a catalyst; (g) drying said catalyst; and (h) calcining said dried catalyst with steam in air, wherein said air has at least 3% steam.
Claim 10
Dependent Claim
26 words
A method of preparing a reforming catalyst according to claim 6 wherein said alkaline earth metal is barium and wherein said Group VIII metal is platinum.
Claim 11
Dependent Claim
30 words
A method of preparing a reforming catalyst according to claim 7 wherein said catalyst has from 5% to 10% by weight barium and from 0.2% to 1.0% by weight platinum.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-08-25 | 1990-02-24 | 1990-08-26 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-08-25 | 1994-02-24 | 1994-08-26 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-08-25 | 1998-02-24 | 1998-08-26 | $7700.00 | Window Closed / Lapsed |