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US4606921A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for improving the flavor and aroma of instant coffee

Assignee: Nestec SA
•
Filing: 1982-03-22
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Granted: 1986-08-19
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Expires: 2002-03-22
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Abstract

Abstract A process for collecting volatile aromatics which are entrained with gases evolved during the wetting and extraction of fresh roasted and ground coffee beans and contained in part within the extract itself, and thereafter combining the collected volatile aromatics with processed coffee extract and/or soluble coffee to produce an instant coffee product having improved flavor and aroma is disclosed. The instant coffee product obtained by this process is also disclosed.

Inventors

  • 👤 Richard T. Liu

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 07:32
CPC Classifications
A; A23; A23F; A23F5/00; A23F5/24; A23F5/26; A23F5/46; A23F5/48; A23F5/50; A23F5/505

Claims Analysis

Total Claims: 26
Claim 1
Independent Claim 152 words
A process for separating volatile aromatics from roasted and ground coffee beans which comprises: (a) wetting and extracting the roasted and ground coffee beans with an aqueous extraction medium and withdrawing an extract at a temperature below 100° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the wetting step and the extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through at least two condensers wherein the first condenser condenses and removes water from the aromatics-laden gases and the last condenser is maintained at a temperature of from about 0° C. to 5° C. to condense volatile aromatics entrained with the aromatics-laden gases; and then (d) collecting the condensed volatile aromatics.
Claim 2
Dependent Claim 152 words
A process for separating volatile aromatics from roasted and ground coffee beans which comprises: (a) wetting and extracting the roasted and ground coffee beans with an aqueous extraction medium and withdrawing an extract at a temperature below 100° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the wetting step and the extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through at least two condensers wherein the first condenser condenses and removes water from the aromatics-laden gases and the last condenser is maintained at a temperature of from about 0° C. to 5° C. to condense volatile aromatics entrained with the aromatics-laden gases; and then (d) collecting the condensed volatile aromatics.
Claim 3
Dependent Claim 23 words
The process of claim 1, wherein the temperature of the withdrawn extract is in the range of about 80° C. to 98° C.
Claim 4
Dependent Claim 25 words
The process of claim 1, wherein inert gas is introduced into the extraction medium prior to the extraction medium contacting the roasted and ground coffee.
Claim 5
Dependent Claim 22 words
The process of claim 1, wherein prior to passing the extract through the separation chamber inert gas is introduced into the extract.
Claim 6
Dependent Claim 14 words
The process of claim 3 or 4, wherein the inert gas is carbon dioxide.
Claim 7
Dependent Claim 17 words
The process of claim 1, wherein the extract is heated prior to passing through the separation chamber.
Claim 8
Dependent Claim 24 words
The process of claim 1, wherein the first condenser is maintained at a temperature in the range of about 75° C. to 90° C.
Claim 9
Dependent Claim 89 words
The process of claim 7, wherein after the aromatics-laden gases have been passed through a first condenser maintained at a temperature in the range of about 75° C. to 90° C. and prior to subjecting the balance of the aromatics-laden gases to the last condenser maintained at a temperature in the range of about 0° C. to 5° C., the aromatics-laden gases are passed through a condenser maintained at a temperature in the range of about 55° C. to 70° C. to obtain yet another condensate of volatile aromatics.
Claim 10
Dependent Claim 206 words
A process for separating volatile aromatics from roast and ground coffee beans which comprises: (a) wetting and extracting the roasted and ground coffee with coffee extract obtained from a battery of serially connected percolators and withdrawing an extract at a temperature in the range of about 80° C. to 98° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the said wetting step and the withdrawn extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the withdrawn extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through a first condenser maintained at a temperature of about 75° C. to 90° C. to obtain a first condensate; (d) passing the balance of the aromatics-laden gases through a second condenser maintained at a temperature of about 55° C. to 70° C. to obtain a second condensate; (e) passing the balance of the aromatics-laden gases through a third condenser maintained at a temperature of about 0° C. to 5° C. to obtain a third condensate; and then (f) collecting the first, second and third condensates of volatile aromatics, respectively.
Claim 11
Dependent Claim 206 words
A process for separating volatile aromatics from roast and ground coffee beans which comprises: (a) wetting and extracting the roasted and ground coffee with coffee extract obtained from a battery of serially connected percolators and withdrawing an extract at a temperature in the range of about 80° C. to 98° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the said wetting step and the withdrawn extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the withdrawn extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through a first condenser maintained at a temperature of about 75° C. to 90° C. to obtain a first condensate; (d) passing the balance of the aromatics-laden gases through a second condenser maintained at a temperature of about 55° C. to 70° C. to obtain a second condensate; (e) passing the balance of the aromatics-laden gases through a third condenser maintained at a temperature of about 0° C. to 5° C. to obtain a third condensate; and then (f) collecting the first, second and third condensates of volatile aromatics, respectively.
Claim 12
Dependent Claim 11 words
The process of claim 9, wherein the first condensate is discarded.
Claim 13
Dependent Claim 183 words
A process for making an instant coffee powder of improved flavor and aroma which comprises: (a) wetting and extracting roasted and ground coffee beans with an aqueous extraction medium and withdrawing an extract at a temperature below 100° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the wetting step and the extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through at least two condensers wherein the first condenser condenses and removes water from the aromatics-laden gases and the last condenser is maintained at a temperature in the range of from about 0° C. to 5° C. to condense volatile aromatics entrained with the aromatics-laden gases and collecting these volatile aromatics; (d) treating the separated extract to provide a dried instant coffee powder; and (e) adding collected volatile aromatics to the extract during or after the said treating step of the extract.
Claim 14
Dependent Claim 183 words
A process for making an instant coffee powder of improved flavor and aroma which comprises: (a) wetting and extracting roasted and ground coffee beans with an aqueous extraction medium and withdrawing an extract at a temperature below 100° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the wetting step and the extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through at least two condensers wherein the first condenser condenses and removes water from the aromatics-laden gases and the last condenser is maintained at a temperature in the range of from about 0° C. to 5° C. to condense volatile aromatics entrained with the aromatics-laden gases and collecting these volatile aromatics; (d) treating the separated extract to provide a dried instant coffee powder; and (e) adding collected volatile aromatics to the extract during or after the said treating step of the extract.
Claim 15
Dependent Claim 22 words
The process of claim 11, wherein the temperature the withdrawn extract is in the range of about 80° C. to 98° C.
Claim 16
Dependent Claim 25 words
The process of claim 11, wherein inert gas is introduced into the extraction medium prior to the extraction medium contacting the roasted and ground coffee.
Claim 17
Dependent Claim 22 words
The process of claim 11, wherein prior to passing the extract through the separation chamber inert gas is introduced into the extract.
Claim 18
Dependent Claim 14 words
The process of claims 13 or 14, wherein the inert gas is carbon dioxide.
Claim 19
Dependent Claim 17 words
The process of claim 11, wherein the extract is heated prior to passing through the separation chamber.
Claim 20
Dependent Claim 24 words
The process of claim 11, wherein the first condenser is maintained at a temperature in the range of about 75° C. to 90° C.
Claim 21
Dependent Claim 98 words
The process of claim 17, wherein after the aromatics-laden gases have been passed through a first condenser maintained at a temperature in the range of about 75° C. to 90° C. to obtain a first condensate, the balance of the aromatics-laden gases is then passed through a second condenser maintained at a temperature in the range of about 55° C. to 70° C. to obtain a second condensate of volatile aromatics and then passed through the last condenser maintained at a temperature of about 0° C. to 5° C. to obtain yet a third condensate of volatile aromatics.
Claim 22
Dependent Claim 24 words
The process of claim 17, wherein the first condensate obtained at a condensation temperature of from about 75° C. to 90° C. is discarded.
Claim 23
Dependent Claim 287 words
A process for making an instant coffee powder of improved flavor and aroma which comprises: (a) wetting and extracting roasted and ground coffee beans with coffee extract obtained from a battery of serially connected percolators and withdrawing an extract at a temperature in the range of about 80° C. to 98° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the said wetting step and the withdrawn extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the withdrawn extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through a first condenser maintained at a temperature of about 75° C. to 90° C. to obtain a first condensate which is discarded; (d) passing the balance of the aromatics-laden gases through a second condenser maintained at a temperature of about 55° C. to 70° C. to obtain a second condensate of volatile aromatics; (e) passing the balance of the aromatics-laden gases through a third condenser maintained at a temperature of about 0° C. to 5° C. to obtain a third condensate of volatile aromatics; (f) cooling the separated extract obtained from the separation chamber; (g) removing aromatic constituents contained within the extract; (h) concentrating the extract; (i) returning the removed aromatic constituents to the concentrated extract and adding volatile aromatics from the second condensate to the concentrated extract; (j) drying the concentrated extract to produce an instant coffee powder; and then (k) mixing a liquid edible oil with condensed volatile aromatics from the third condensate to form an emulsion and plating the emulsion onto the dried instant coffee powder.
Claim 24
Dependent Claim 287 words
A process for making an instant coffee powder of improved flavor and aroma which comprises: (a) wetting and extracting roasted and ground coffee beans with coffee extract obtained from a battery of serially connected percolators and withdrawing an extract at a temperature in the range of about 80° C. to 98° C. at essentially atmospheric pressure; (b) passing aromatics-laden gases evolved by the said wetting step and the withdrawn extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the withdrawn extract are separated from the extract while maintaining the extract at a temperature below 100° C. and at essentially atmospheric pressure; (c) passing the separated aromatics-laden gases through a first condenser maintained at a temperature of about 75° C. to 90° C. to obtain a first condensate which is discarded; (d) passing the balance of the aromatics-laden gases through a second condenser maintained at a temperature of about 55° C. to 70° C. to obtain a second condensate of volatile aromatics; (e) passing the balance of the aromatics-laden gases through a third condenser maintained at a temperature of about 0° C. to 5° C. to obtain a third condensate of volatile aromatics; (f) cooling the separated extract obtained from the separation chamber; (g) removing aromatic constituents contained within the extract; (h) concentrating the extract; (i) returning the removed aromatic constituents to the concentrated extract and adding volatile aromatics from the second condensate to the concentrated extract; (j) drying the concentrated extract to produce an instant coffee powder; and then (k) mixing a liquid edible oil with condensed volatile aromatics from the third condensate to form an emulsion and plating the emulsion onto the dried instant coffee powder.
Claim 25
Dependent Claim 145 words
A process for separating volatile aromatics from roasted and ground coffee beans which comprises: (a) wetting and extracting the roasted and ground coffee beans with an aqueous extraction medium and withdrawing an extract at a temperature below its boiling point; (b) passing aromatics-laden gases evolved by the wetting step and the extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the extract are separated from the extract while maintaining the extract at a temperature below its boiling point; (c) passing the separated aromatics-laden gases through at least two condensers wherein the first condenser condenses and removes water from the aromatics-laden gases and the last condenser is maintained at a temperature of from about 0° C. to 5° C. to condense volatile aromatics entrained with the aromatics-laden gases; and then (d) collecting the condensed volatile aromatics.
Claim 26
Dependent Claim 145 words
A process for separating volatile aromatics from roasted and ground coffee beans which comprises: (a) wetting and extracting the roasted and ground coffee beans with an aqueous extraction medium and withdrawing an extract at a temperature below its boiling point; (b) passing aromatics-laden gases evolved by the wetting step and the extract through a separation chamber wherein the aromatics-laden gases evolved by the wetting step and aromatics-laden gases entrained within the extract are separated from the extract while maintaining the extract at a temperature below its boiling point; (c) passing the separated aromatics-laden gases through at least two condensers wherein the first condenser condenses and removes water from the aromatics-laden gases and the last condenser is maintained at a temperature of from about 0° C. to 5° C. to condense volatile aromatics entrained with the aromatics-laden gases; and then (d) collecting the condensed volatile aromatics.

References Cited (Backward Citations)

US2432759A Cited
US3148070A Cited
US3244532A Cited
CA1001476A Cited
US4072761A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-08-18 1990-02-17 1990-08-19 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-08-18 1994-02-17 1994-08-19 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-08-18 1998-02-17 1998-08-19 $7700.00 Window Closed / Lapsed

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