← Back to Patent Explorer
US4604147A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of manufacturing permanent magnets

Assignee: Thyssen Stahl AG
•
Filing: 1984-09-17
•
Granted: 1986-08-05
•
Expires: 2004-09-17
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract An alloy is proposed for use in making permanent magnets. The alloy has the following composition by weight: ______________________________________ Chromium 22.5 to 25.5% Cobalt 15.0 to 17.5% Molybdenum 2.0 to 4.0% Silicon 0.1 to 0.8% Oxygen less than 0.10% Effective carbon less than 0.06% Remainder iron and unavoidable impurities, ______________________________________ where effective carbon is defined as carbon content plus 0.86 times nitrogen content. In a method of manufacturing permanent magnets, a workpiece is made of the alloy, for example by suction or extrusion casting, and the workpiece is subjected to a heat treatment comprising: (a) a homogenizing annealing for 15 minutes to 3 hours at 1230° C. to 1280° C., followed by quenching in water or oil; and (b) a thermo-magnetic treatment for 10 to 30 minutes at 720° C. to 740° C., followed by the application for 10 to 120 minutes in a preferred axial direction of a magnetic field of 80 to 240 kA/m at a temperature of 630° C. to 650° C., followed by cooling in air. The workpiece is then optionally age-hardened in the following three stages: i maintaining the workpiece at 590° C. to 625° C. for 0.25 to 10 hours ii maintaining the workpiece at 555° C. to 585° C. for 0.5 to 30 hours, and iii maintaining the workpiece at 500° C. to 540° C. for 0 to 50 hours.

Inventors

  • 👤 Helmut Brandis
  • 👤 Wolfgang Spyra

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 04:50
CPC Classifications
C; C22; C22C; C22C38/00; C22C38/18; C22C38/30; H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/032; H01F1/04

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 249 words
A method of manufacturing a permanent magnet comprising forming a workpiece of an alloy having the following composition by weight: ______________________________________ Chromium 22.5 to 25.5% Cobalt 15.0 to 17.5% Molybdenum 2.0 to 4.0% Silicon 0.1 to 0.8% Oxygen less than 0.10% Effective carbon less than 0.06% Remainder iron and unavoidable impurities, ______________________________________ where effective carbon is defined as carbon content plus 0.86 times nitrogen content, and subjecting the workpiece to: (a) a homogenising annealing for 15 minutes to 3 hours at 1230° C. to 1280° C., followed by quenching in liquid; then to (b) a treatment comprising treating the workpiece for 10 to 30 minutes at 720° C. to 740° C., followed by the application for 10 to 120 minutes in a preferred axial direction of a magnetic field of 80 to 240 kA/m at a temperature of 630° C. to 650° C., followed by cooling in air; and subsequently to (c) an age-hardening treatment in the following stages: (ci) maintaining the workpiece at 590° C. to 625° C. for 0.25 to 10 hours (cii) maintaining the workpiece at 555° C. to 585° C. for 0.5 to 30 hours, and (ciii) maintaining the workpiece at 500° C. to 540° C. for 0 to 50 hours; thereby to form a permanent magnet which has the following properties, measured in the direction of magnetisation; coercive field strength B H C at least 50 kA/m; remanence Br at least 1.2 T; and energy value (BH) max at least 39 kJ/m 3 .
Claim 2
Independent Claim 249 words
A method of manufacturing a permanent magnet comprising forming a workpiece of an alloy having the following composition by weight: ______________________________________ Chromium 22.5 to 25.5% Cobalt 15.0 to 17.5% Molybdenum 2.0 to 4.0% Silicon 0.1 to 0.8% Oxygen less than 0.10% Effective carbon less than 0.06% Remainder iron and unavoidable impurities, ______________________________________ where effective carbon is defined as carbon content plus 0.86 times nitrogen content, and subjecting the workpiece to: (a) a homogenising annealing for 15 minutes to 3 hours at 1230° C. to 1280° C., followed by quenching in liquid; then to (b) a treatment comprising treating the workpiece for 10 to 30 minutes at 720° C. to 740° C., followed by the application for 10 to 120 minutes in a preferred axial direction of a magnetic field of 80 to 240 kA/m at a temperature of 630° C. to 650° C., followed by cooling in air; and subsequently to (c) an age-hardening treatment in the following stages: (ci) maintaining the workpiece at 590° C. to 625° C. for 0.25 to 10 hours (cii) maintaining the workpiece at 555° C. to 585° C. for 0.5 to 30 hours, and (ciii) maintaining the workpiece at 500° C. to 540° C. for 0 to 50 hours; thereby to form a permanent magnet which has the following properties, measured in the direction of magnetisation; coercive field strength B H C at least 50 kA/m; remanence Br at least 1.2 T; and energy value (BH) max at least 39 kJ/m 3 .
Claim 3
Independent Claim 249 words
A method of manufacturing a permanent magnet comprising forming a workpiece of an alloy having the following composition by weight: ______________________________________ Chromium 23.0 to 24.7% Cobalt 15.5 to 17.0% Molybdenum 2.0 to 3.5% Silicon 0.2 to 0.6% Oxygen less than 0.08% Effective carbon less than 0.06% Remainder iron and unavoidable impurities, ______________________________________ where effective carbon is defined as carbon content plus 0.86 times nitrogen content, and subjecting the workpiece to: (a) a homogenising annealing treatment for 30 to 60 minutes at 1250° C. to 1270° C., followed by quenching in liquid; then to (b) a treatment comprising maintaining the workpiece at 725° C. to 735° C. for 10 to 20 minutes, followed by applying to it for 20 to 80 minutes in a preferred axial direction, a magnetic field of 120 to 200 kA/m at a temperature of 635° C. to 645° C., followed by cooling in air; and subsequently to (c) an age-hardening treatment in the following stages: (ci) maintaining the workpiece at 595° C. to 605° C. for 0.5 to 1 hour (cii) maintaining the workpiece at 560° C. to 570° C. for 1 to 20 hours, and (ciii) maintaining the workpiece at 500° C. to 530° C. for 0 to 30 hours; thereby to form a permanent magnet which has the following properties, measured in the direction of magnetisation; coercive field strength B H C at least 50 kA/m; remanence Br at least 1.2 T; and energy value (BH) max at least 39 kJ/m 3 .
Claim 4
Independent Claim 249 words
A method of manufacturing a permanent magnet comprising forming a workpiece of an alloy having the following composition by weight: ______________________________________ Chromium 23.0 to 24.7% Cobalt 15.5 to 17.0% Molybdenum 2.0 to 3.5% Silicon 0.2 to 0.6% Oxygen less than 0.08% Effective carbon less than 0.06% Remainder iron and unavoidable impurities, ______________________________________ where effective carbon is defined as carbon content plus 0.86 times nitrogen content, and subjecting the workpiece to: (a) a homogenising annealing treatment for 30 to 60 minutes at 1250° C. to 1270° C., followed by quenching in liquid; then to (b) a treatment comprising maintaining the workpiece at 725° C. to 735° C. for 10 to 20 minutes, followed by applying to it for 20 to 80 minutes in a preferred axial direction, a magnetic field of 120 to 200 kA/m at a temperature of 635° C. to 645° C., followed by cooling in air; and subsequently to (c) an age-hardening treatment in the following stages: (ci) maintaining the workpiece at 595° C. to 605° C. for 0.5 to 1 hour (cii) maintaining the workpiece at 560° C. to 570° C. for 1 to 20 hours, and (ciii) maintaining the workpiece at 500° C. to 530° C. for 0 to 30 hours; thereby to form a permanent magnet which has the following properties, measured in the direction of magnetisation; coercive field strength B H C at least 50 kA/m; remanence Br at least 1.2 T; and energy value (BH) max at least 39 kJ/m 3 .

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-08-04 1990-02-03 1990-08-05 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-08-04 1994-02-03 1994-08-05 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-08-04 1998-02-03 1998-08-05 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag