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US4598765A Expired / Lapsed US ⏱️ 0.0 years remaining

Sample cell temperature stabilizer

Assignee: PerkinElmer Instruments LLC
•
Filing: 1984-02-03
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Granted: 1986-07-08
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Expires: 2004-02-03
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Abstract

Abstract An apparatus for modifying the temperature of the effluent of a fluid stream entering a flow cell which includes a counterflow heat exchange between the outlet fluid and the inlet fluid and a thermally equilibrating the flow cell with the inlet fluid after it has passed through the counterflow heat exchange and before it enters the flow cell.

Inventors

  • 👤 John Atwood
  • 👤 Charles Helms
  • 👤 Raymond P. W. Scott

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 06:35
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/01; G01N21/03; G01N21/0332; G01N21/05

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 165 words
In a liquid chromatograph a thermal equilibrating apparatus for equilibrating the temperature of liquid as it passes through a flow cell comprising, in combination: a flow cell housing having an inlet port and an outlet port through which liquid can pass from said inlet port to said outlet port; an outlet conduit in fluid communication with said outlet port for conducting away fluid exiting from said outlet port; an inlet conduit coupled to said inlet port and of a smaller diameter than said outlet conduit for conducting fluid into said inlet port, said inlet conduit being coiled around and in thermal transfer relationship with said outlet conduit along a portion of the length thereof; and means in direct thermal transfer relationship with said flow cell housing around which said inlet conduit is coiled in a thermal transfer relationship therewith and disposed between the point of separation of said inlet conduit from said outlet conduit and the connection of said inlet conduit to said inlet port.
Claim 2
Dependent Claim 165 words
In a liquid chromatograph a thermal equilibrating apparatus for equilibrating the temperature of liquid as it passes through a flow cell comprising, in combination: a flow cell housing having an inlet port and an outlet port through which liquid can pass from said inlet port to said outlet port; an outlet conduit in fluid communication with said outlet port for conducting away fluid exiting from said outlet port; an inlet conduit coupled to said inlet port and of a smaller diameter than said outlet conduit for conducting fluid into said inlet port, said inlet conduit being coiled around and in thermal transfer relationship with said outlet conduit along a portion of the length thereof; and means in direct thermal transfer relationship with said flow cell housing around which said inlet conduit is coiled in a thermal transfer relationship therewith and disposed between the point of separation of said inlet conduit from said outlet conduit and the connection of said inlet conduit to said inlet port.
Claim 3
Dependent Claim 34 words
Apparatus as claimed in claim 1 wherein said thermal transfer effecting means includes a member having one end thereof within said housing and another end thereof external said housing and distal said flow cell.
Claim 4
Dependent Claim 14 words
Apparatus as claimed in claim 2 wherein said member is a rigid copper rod.
Claim 5
Dependent Claim 42 words
Apparatus as claimed in claim 1 wherein said helically coiled portion of said inlet conduit about said thermal transfer means has a lead angle in the range of 60 to 70 degrees with respect to the axis of said thermal transfer means.
Claim 6
Dependent Claim 21 words
Apparatus as claimed in claim 1 wherein said inlet conduit is helically wrapped around and in contact with said outlet conduit.
Claim 7
Dependent Claim 45 words
Apparatus as claimed in claim 5 wherein said inlet conduit is helically coiled about said outlet conduit, said coiling lead angle is in the range of 60 to 70 degrees with respect to the axis of said outlet conduit whereby thermal transfer is effected therebetween.

References Cited (Backward Citations)

US2201056A Cited
US3273356A Cited
US3799250A Cited
US4248259A Cited
US4296738A Cited
US4479727A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-07-07 1990-01-06 1990-07-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-07-07 1994-01-06 1994-07-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-07-07 1998-01-06 1998-07-08 $7700.00 Window Closed / Lapsed

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