US4588413A
Expired / Lapsed
US
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Process for producing dyeings with reactive dyestuffs
Assignee: Sanofi Aventis Deutschland GmbH
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Filing: 1984-07-19
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Granted: 1986-05-13
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Expires: 2004-07-19
Abstract
Abstract Improvements in the fastness properties of substrates dyed with reactive dyestuffs are achieved by a dyeing after-treatment with an agent which is the reaction product polyethyleneimine and a bifunctional alkylating agent.
Inventors
- 👤 Karl-Heinz Keil
- 👤 Fritz Engelhardt
- 👤 Ulrich Greiner
- 👤 Klaus Sternberger
- 👤 Manfred Pelster
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 14:06
CPC Classifications
D; D06; D06P; D06P5/00; D06P5/02; D06P5/04; D06P5/08; C; C08; C08G; C08G73/00; C08G73/02; C08G73/0206; C08G73/0213; C08G73/022; D06P1/00; D06P1/44; D06P1/52; D06P1/5264; D06P1/5278; Y; Y10; Y10S; Y10S8/00; Y10S8/916; Y10S8/918
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
68 words
In the process for dyeing textile materials, yarns, threads or fibers dyeable with reactive dyestuffs by contact and treatment with reactive dyestuff, the improvement comprises improving the fastness of the dyed substrate by aftertreating the dyed substrate with 0.5 to 5% by weight of substrate of an aftertreatment agent which is the reaction product of polyethyleneimine and an alkylating agent having two alkylating groups in an aqueous solution.
Claim 2
Dependent Claim
68 words
In the process for dyeing textile materials, yarns, threads or fibers dyeable with reactive dyestuffs by contact and treatment with reactive dyestuff, the improvement comprises improving the fastness of the dyed substrate by aftertreating the dyed substrate with 0.5 to 5% by weight of substrate of an aftertreatment agent which is the reaction product of polyethyleneimine and an alkylating agent having two alkylating groups in an aqueous solution.
Claim 3
Dependent Claim
24 words
The process according to claim 1 wherein the dyed substrate is aftertreated with 1 to 3% by weight of substrate of said aftertreatment agent.
Claim 4
Dependent Claim
143 words
The process according to claim 1 wherein the aftertreatment agent is the reaction product of polyethyleneimine of the formula H--CH.sub.2 CH.sub.2 NH).sub.a --CH.sub.2 CH.sub.2 NX).sub.b H with an alkylating agent of the formula Y--CH.sub.2 --Z--CH.sub.2 --Y wherein X is ##STR14## a and b independently are each a number from 0 to 600 and the sum of a and b is 50 to 600; c is a number from 0 to 50; Z is a direct bond, --C n H 2n --, or --C m H 2m --D--C m H 2m --, wherein n is a number from 1 to 4, m is either 1 or 2 and D is --O--, --S--, --NH--, --CO--, --SO--, --SO 2 -- or phenylene; and Y is a substituent which can be eliminated as an anion and comprises chloro, bromo, iodo, hydroxyl, sulphato, sulphonyloxy, phenylsulphonyloxy, tolylsulphonyloxy or ##STR15##
Claim 5
Dependent Claim
37 words
The process according to claim 1 wherein said bifunctional alkylating agent is epichlorohydrin, glycidol, 1,3-dichloropropan-2-ol, β,β'-dichlorodiethyl ether, ββ'-dichlorodiethylamine, β,β'-dichlorodiethyl sulphide, β,β'-dichlorodiethyl sulphoxide, β,β'-dichlorodiethyl sulphone, β,β'-disulphatoethylether, β,β'-diphenylsulphonyloxyethyl ether, meta- or para-diepoxyethylbenzene, meta- or para-diepoxypropylbenzene, diepoxybutane, diepoxy-2-methylbutane or diepoxypropylamine.
Claim 6
Dependent Claim
23 words
The process according to claim 1 wherein the aftertreatment agent is the reaction product of polyethyleneimine with epichlorohydrin, 1,3-dichloropropane-2-ol or a mixture thereof.
Claim 7
Dependent Claim
29 words
The process according to claim 1 wherein the aftertreatment agent is the reaction product of polyethyleneimine with a bifunctional alkylating agent in a weight ratio of 100:0.01 to 100:2.
Claim 8
Dependent Claim
29 words
The process according to claim 6 wherein the aftertreatment agent is the reaction product of polyethyleneimine with a bifunctional alkylating agent in a weight ratio of 100:0.1 to 100:1.
Claim 9
Dependent Claim
16 words
The process according to claim 1 wherein the aftertreatment temperature is about 40°° to 100° C.
Claim 10
Dependent Claim
31 words
The process according to claim 1 wherein the aftertreatment is at about 60° to 100° C. at a pH of about 9-10 for a period of about 2 to 6 hours.
Claim 11
Dependent Claim
22 words
A dyed substrate of textile material, yarns, threads or fibers having an improved fastness prepared by the process according to claim 1.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-05-12 | 1989-11-11 | 1990-05-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-05-12 | 1993-11-11 | 1994-05-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-05-12 | 1997-11-11 | 1998-05-13 | $7700.00 | Window Closed / Lapsed |