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US4587225A Expired / Lapsed US ⏱️ 0.0 years remaining

High-strength zirconia type sintered body

Assignee: Tosoh Corp
•
Filing: 1984-10-17
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Granted: 1986-05-06
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Expires: 2004-10-17
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Abstract

Abstract A zirconia type sintered body consisting essentially of 50 to 98% by weight of zirconia (ZrO2) containing 1.5 to 5 mole % of yttria (Y2O3) and 50 to 2% by weight of alumina (Al2O3), spinal (MgAl2O4) or mullite (3Al2O3.2SiO2), and having a three-point bending strength of at least 1700 MPa is provided. This sintered body is prepared by a process wherein a powdery composition consisting essentially of 50 to 98% by weight of (a1) a powder of zirconia containing 1.5 to 5 mole % of yttria or (a2) a mixture comprising 1.5 to 5 mole % of a yttria powder and 95 to 98.5 mole % of a zirconia powder and 2 to 50% by weight of (b) a powder of an alumina type oxide selected from alumina, an alumina-magnesia type oxide, an alumina-silica type oxide, a mixture of alumina and magnesia and a mixture of alumina and silica is subjected to a hot isotactic pressing treatment under a pressure of at lesast 50 MPa at temperature of 1300 DEG C. to 1700 DEG C. or a monoazially compression-sintering treatment under a pressure of at least 20 MPa at a temperature of 1400 DEG C. to 1700 DEG C.

Inventors

  • 👤 Koji Tsukuma
  • 👤 Kuniyoshi Ueda
  • 👤 Takaaki Tsukidate

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 00:48
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/48; C04B35/622; C04B35/64; C04B35/645; C04B35/6455; C04B35/10; C04B35/44; C04B35/486; C04B35/488; C04B35/4885

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 159 words
A hot isostatically pressed zirconia type sintered body consisting essentially of 50 to 98% by weight of ziroconia (ZrO 2 ) containing 1.5 to 5 mole % of yttria (Y 2 O 3 ) and 50 to 2% by weight of alumina (Al 2 O 3 ), spinel (MgAl 2 O 4 ) or mullite (3Al 2 O 3 ·2SiO 2 ), said hot isostatically pressed sintered body having a three-point bending strength of at least 1700 MPa, the crystal phase of zirconia constituting the sintered body being substantially composed of a tetragonal crystal or a mixture of at least 50% of a tetragonal crystal and up to 50% of a cubic crystal, said sintered body having having a bulk density of at least 99.5% of the theoretical density and devoid of pores having a size of 30 μm or more, and the crystal of said sintered body having an average grain size of not larger than 2 μm.
Claim 2
Dependent Claim 159 words
A hot isostatically pressed zirconia type sintered body consisting essentially of 50 to 98% by weight of ziroconia (ZrO 2 ) containing 1.5 to 5 mole % of yttria (Y 2 O 3 ) and 50 to 2% by weight of alumina (Al 2 O 3 ), spinel (MgAl 2 O 4 ) or mullite (3Al 2 O 3 ·2SiO 2 ), said hot isostatically pressed sintered body having a three-point bending strength of at least 1700 MPa, the crystal phase of zirconia constituting the sintered body being substantially composed of a tetragonal crystal or a mixture of at least 50% of a tetragonal crystal and up to 50% of a cubic crystal, said sintered body having having a bulk density of at least 99.5% of the theoretical density and devoid of pores having a size of 30 μm or more, and the crystal of said sintered body having an average grain size of not larger than 2 μm.
Claim 3
Dependent Claim 23 words
A hot isostatically pressed zirconia type sintered body according to claim 1, wherein said sintered body consists essentially of yttria-containing zirconia and alumina.

References Cited (Backward Citations)

DE2810134A1 Cited
US4221650A Cited
US4314827A Cited
US4518397A Cited
US4518398A Cited
US4336339A Cited
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US4506024A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-05-05 1989-11-04 1990-05-06 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-05-05 1993-11-04 1994-05-06 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-05-05 1997-11-04 1998-05-06 $7700.00 Window Closed / Lapsed

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