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US4585827A Expired / Lapsed US ⏱️ 0.0 years remaining

Low formaldehyde release reactant

Assignee: FREEDOM TEXTILE CHEMICALS Co
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Filing: 1984-07-13
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Granted: 1986-04-29
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Expires: 2004-07-13
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Abstract

Abstract Textile treating agent for imparting crease resistance is made by mixing 1 mol glyoxal, 2 mols formaldehyde, 1 mol urea and 1.5 mol ethylene glycol and reacting the mixture first at pH 6 to 7 at 60° C. and then at pH 3 at 60°. The product is found to have more stable formaldehyde release properties in textile treating baths as pH of the bath is varied in the range from about 3.0 to about 4.5.

Inventors

  • 👤 Kenneth H. Remley

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 08:11
CPC Classifications
D; D06; D06M; D06M11/00; C; C08; C08G; C08G12/00; C08G12/02; C08G12/40; C08G12/42; C08G12/421; C08G12/422

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 115 words
An improved method for making textile finishing agent comprising the steps of mixing glyoxal, formaldehyde, urea and a glycol and reacting the mixture at temperature in the range from about 40° C. to about 80° C. and at pH in the range from 6 to 7 for time sufficient to complete the reaction and then changing the pH of the product mixture and further reacting at temperature in the range from about 40° C. to about 80° C. and at pH in the range from 3.5 to about 1.0 for time sufficient to complete the reaction and then adjusting the pH of the product mixture to pH in the range from pH 4.5 to 5.5.
Claim 2
Dependent Claim 115 words
An improved method for making textile finishing agent comprising the steps of mixing glyoxal, formaldehyde, urea and a glycol and reacting the mixture at temperature in the range from about 40° C. to about 80° C. and at pH in the range from 6 to 7 for time sufficient to complete the reaction and then changing the pH of the product mixture and further reacting at temperature in the range from about 40° C. to about 80° C. and at pH in the range from 3.5 to about 1.0 for time sufficient to complete the reaction and then adjusting the pH of the product mixture to pH in the range from pH 4.5 to 5.5.
Claim 3
Dependent Claim 15 words
A textile finishing agent comprising a product made by the process described in claim 1.
Claim 4
Dependent Claim 29 words
An aqueous solution of a textile finishing agent defined by claim 2 further comprising a catalyst in said solution for the cross-linking reaction of the product with textile fabric.

References Cited (Backward Citations)

US4396391A Cited
US4396391B1 Cited
US4396391B2 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-04-28 1989-10-28 1990-04-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-04-28 1993-10-28 1994-04-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-04-28 1997-10-28 1998-04-29 $7700.00 Window Closed / Lapsed

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