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US4582629A Expired / Lapsed US ⏱️ 0.0 years remaining

Use of microwave radiation in separating emulsions and dispersions of hydrocarbons and water

Assignee: THERMAL WAVE INTERNATIONAL
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Filing: 1983-12-29
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Granted: 1986-04-15
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Expires: 2003-12-29
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Abstract

Abstract Oil and water emulsions can be more rapidly separated when exposed to electromagnetic radiation in the range of from 1 to 300 millimeters, commonly called microwaves. The microwave treatment can be in conjunction with other separating and heating devices such as skimmers, gun barrel treaters, heater treaters, and the like.

Inventors

  • 👤 Nicholas O. Wolf

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 10:45
CPC Classifications
C; C10; C10G; C10G33/00; C10G33/02; B; B01; B01D; B01D17/00; B01D17/02; B01D17/04

Claims Analysis

Total Claims: 14
Claim 1
Independent Claim 53 words
A method for enhancing the separation of hydrocarbon and water from an emulsion or dispersion thereof comprising the steps of subjecting said emulsion or dispersion to microwave radiation in the range of one millimeter to 30 centimeters and heating the microwave irradiated emulsion or dispersion to a separating temperature using conventional heating means.
Claim 2
Independent Claim 53 words
A method for enhancing the separation of hydrocarbon and water from an emulsion or dispersion thereof comprising the steps of subjecting said emulsion or dispersion to microwave radiation in the range of one millimeter to 30 centimeters and heating the microwave irradiated emulsion or dispersion to a separating temperature using conventional heating means.
Claim 3
Dependent Claim 21 words
A method as described in claim 1 when used at a power level of from about 300 to about 50,000 watts.
Claim 4
Dependent Claim 15 words
A method as described in claim 2 when used in oil external emulsions and dispersions.
Claim 5
Dependent Claim 35 words
A method as described in claim 3 wherein the oil external emulsion or dispersion contains from about 50% to greater than 99% oil by weight based on the total weight of the emulsion or dispersion.
Claim 6
Dependent Claim 33 words
A method as described in claim 4 wherein the emulsion or dispersion is treated at a power level of from about 1 watt to about 500 watts per gallon of emulsion or dispersion.
Claim 7
Dependent Claim 15 words
A method as described in claim 2 when used in water external emulsions and dispersions.
Claim 8
Dependent Claim 34 words
A method as described in claim 6 wherein the water external emulsion or dispersion contains from about 1% to about 50% oil by weight based on the total weight of the emulsion or dispersion.
Claim 9
Dependent Claim 38 words
A method as described in claim 7 wherein the emulsion or dispersion is treated at a power level of about 1 watt to about 500 watts per gallon of emulsion or dispersion in the presence of chemical deemulsifiers.
Claim 10
Dependent Claim 29 words
A method as described in claim 8 wherein chemical deemulsifiers are present at concentrations up to one percent by weight based on the weight of the dispersion or emulsion.
Claim 11
Dependent Claim 22 words
A method as described in claim 9 where the deemulsifier is selected from the group consisting of non-ionic surfactants and cationic surfactants.
Claim 12
Dependent Claim 30 words
The method as described in claim 1 wherein said step of heating to a separating temperature comprises heating to a temperature of from about 45° C. to about 115° C.
Claim 13
Independent Claim 50 words
A method for enhancing the separation of hydrocarbon and water from dispersion or emulsion thereof in the presence of chemical deemulsifiers comprising the steps of contacting the dispersion or emulsion and chemical deemulsifiers with microwave energy before heating the emulsion or dispersion to a separating temperature using conventional heating means.
Claim 14
Independent Claim 50 words
A method for enhancing the separation of hydrocarbon and water from dispersion or emulsion thereof in the presence of chemical deemulsifiers comprising the steps of contacting the dispersion or emulsion and chemical deemulsifiers with microwave energy before heating the emulsion or dispersion to a separating temperature using conventional heating means.

References Cited (Backward Citations)

US2446557A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-04-14 1989-10-14 1990-04-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-04-14 1993-10-14 1994-04-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-04-14 1997-10-14 1998-04-15 $7700.00 Window Closed / Lapsed

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