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US4577646A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for improving the fillability of tobacco

Assignee: Reemtsma Cigarettenfabriken GmbH
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Filing: 1984-04-20
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Granted: 1986-03-25
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Expires: 2004-04-20
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Abstract

Abstract Process for improving the fillability of tobacco, such as cut tobacco leaves or ribs and tobacco additives by treating the tobacco in an autoclave with a containing nitrogen and/or argon at pressures up to 1000 bar, with subsequent decompression and a gas heat treatment. The tobacco or the treatment gas supplied to the reactor and/or the decompression step are carried out in such a way that the discharged tobacco which is thereafter supplied to a subsequent heat treatment has a temperature, at introduction to the heat treatment step, below 0 DEG C. This is achieved by precooling the treatment gas prior to supplying it to the autoclave or cooling the treatment gas while supplying it to the autoclave and/or additionally cooling the autoclave and/or precooling the tobacco and/or injecting subcooled or liquefied treatment gas into the autoclave. The process includes multistage treatment gas whereby supply and decompression steps are carried out in a cascade-like manner.

Inventors

  • 👤 Klaus-Dieter Ziehn

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 16:13
CPC Classifications
A; A24; A24B; A24B3/00; A24B3/18; A24B3/182

Claims Analysis

Total Claims: 19
Claim 1
Independent Claim 97 words
In a process for improving the fillability of tobacco by treatment with a treatment gas containing at least one of the following: nitrogen gas, argon gas or a mixture thereof at pressures up to 1000 bar in an autoclave, decompressing the tobacco, and subjecting the tobacco to a heat treatment, the improvement comprising: supplying the autoclave with both tobacco and treatment gas and decompressing the treated tobacco in such manner that the decompressed tobacco supplied to the subsequent heat treatment has an inlet temperature for the heat treatment of below 0° C., said treatment gas being non-polar.
Claim 2
Dependent Claim 97 words
In a process for improving the fillability of tobacco by treatment with a treatment gas containing at least one of the following: nitrogen gas, argon gas or a mixture thereof at pressures up to 1000 bar in an autoclave, decompressing the tobacco, and subjecting the tobacco to a heat treatment, the improvement comprising: supplying the autoclave with both tobacco and treatment gas and decompressing the treated tobacco in such manner that the decompressed tobacco supplied to the subsequent heat treatment has an inlet temperature for the heat treatment of below 0° C., said treatment gas being non-polar.
Claim 3
Dependent Claim 21 words
A process according to claim 1, comprising cooling the treatment gas not later than when it is supplied to the autoclave.
Claim 4
Dependent Claim 20 words
A process according to claim 2, comprising cooling the autoclave in which the tobacco is treated with the treatment gas.
Claim 5
Dependent Claim 20 words
A process according to claim 1 comprising cooling the autoclave in which the tobacco is treated with the treatment gas.
Claim 6
Dependent Claim 17 words
A process according to claim 1, comprising cooling the tobacco prior to its introduction into the autoclave.
Claim 7
Dependent Claim 17 words
A process according to claim 4, comprising cooling the tobacco prior to its introduction into the autoclave.
Claim 8
Dependent Claim 26 words
A process according to claim 1, comprising injecting subcooled or liquefied treatment gas into the autoclave during the treatment of the tobacco with the treatment gas.
Claim 9
Dependent Claim 61 words
A process according to claim 1, said process further comprising providing a plurality of autoclaves; cascading said autoclaves wherein treatment gas from one autoclave under a high pressure is introduced into at least one other autoclave, said other autoclave being at an initial pressure less than said one autoclave, whereby said one autoclave is decompressed while said other autoclave is pressurized.
Claim 10
Dependent Claim 44 words
A process according to claim 8, said process further comprising: carrying out the pressurization and the decompression in a stepwise manner, the pressurization including forcing additional treatment gas into a said other autoclave during the final compression stage to obtain the desired final pressure.
Claim 11
Dependent Claim 32 words
A process according to claim 9, said process further comprising: additionally cooling the treatment gas supplied from a said one autoclave during the transfer of said gas to a said other autoclave.
Claim 12
Dependent Claim 35 words
A process according to claim 8, said process further comprising: additionally cooling the treatment gas supplied from a said one autoclave during the transfer to a said other autoclave which is at a lower pressure.
Claim 13
Dependent Claim 26 words
A process according to claim 8, said process further comprising: charging the autoclave during the final stage of the compression with subcooled or liquified treatment gas.
Claim 14
Dependent Claim 27 words
A process according to claim 1 comprising subjecting the tobacco to low temperature insulation after decompression and up to the subsequent heat treatment to prevent premature heating.
Claim 15
Dependent Claim 50 words
A process according to claim 1, comprising carrying out the subsequent heat treatment either with (1) water vapour in the form of saturated steam or (2) with water vapour having a density of 0.5 to 10 kg/m 3 or (3) with hot air having a temperature up to 440° C.
Claim 16
Dependent Claim 40 words
A process according to claim 14 wherein the subsequent heat treatment is carried out either with (1) water vapour in the form of saturated steam or (2) with water vapour having a density of 0.5 to 10 kg/m 3 .
Claim 17
Dependent Claim 20 words
A process according to claim 1, comprising introducing the treating gas into the autoclave from below or from the side.
Claim 18
Dependent Claim 23 words
A process according to claim 1, comprising decompressing the autoclave via the top or through the bottom after the final pressure is reached.
Claim 19
Dependent Claim 53 words
A process according to claim 1, comprising introducing the treating gas into an annular space within the autoclave, said annular space being defined in its outer configuration by the inner wall of the autoclave and in its inner configuration by a cylindrical wall having openings leading into the inner part of the autoclave.

References Cited (Backward Citations)

US4340073A Cited
US4235250A Cited
US4289148A Cited
US4461310A Cited
GB2115677A Cited
US4460000A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-03-24 1989-09-23 1990-03-25 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-03-24 1993-09-23 1994-03-25 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-03-24 1997-09-23 1998-03-25 $7700.00 Window Closed / Lapsed

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