US4560526A
Expired / Lapsed
US
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Process for preparing molded silicon carbide product
Assignee: Nippon Soda Co Ltd
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Filing: 1984-03-12
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Granted: 1985-12-24
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Expires: 2004-03-12
Abstract
Abstract A process for preparing a molded silicon carbide product, by molding a mixture of silicon carbide powder, an organosilicon compound and one or more lubricants to form a compact and sintering the thus-formed compact, is described.
Inventors
- 👤 Masatoshi Okumura
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 18:39
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/56; C04B35/565; C04B35/571; C04B35/622; C04B35/626; C04B35/63; C04B35/6303; C04B35/6316; C04B35/71; C04B35/78; C04B35/80
Claims Analysis
Total Claims: 29
Claim 1
Independent Claim
280 words
A process for preparing a molded silicon carbide product, which process comprises molding a mixture of silicon carbide powder, an organosilicon compound and a lubricant selected from the group consisting of higher fatty acids, higher fatty acid esters, higher fatty acid amides, higher alcohols and paraffin wax into a compact and sintering the compact wherein the lubricant has the following properties: (a) it does not substantially evaporate during such operations as mixing, drying, molding, etc.; (b) it is in liquid or solid form, and when it is a solid, it has a melting point of 40° C. or higher; (c) it exhibits low viscosity in a melt of a mixture of the lubricant and organosilicon compound; and, (d) it undergoes almost complete evaporation at or below a temperature at which the organosilicon compound is pyrolyzed, i.e., at temperatures up to 500° C.; wherein the organosilicon compound is one or more compounds selected from those in which (1) silicon atoms are bonded only to carbon atoms; (2) besides the bonds between silicon atoms and carbon atoms, silicon atoms are bonded to hydrogen atoms; (3) besides the bonds between silicon atoms and carbon atoms, there are bonds formed between silicon atoms and halogen atoms; (4) in addition to the bonds between silicon atoms and carbon atoms, there are bonds established between silicon atoms per se; and (5) there are two or more types of bonds out of the above-mentioned bonds (2) through (4), or a polycondensation product, obtained by polycondensation of these compounds, containing silicon-carbon bonds as its principal backbone structure; and wherein the ratio of lubricant to organosilicon compound is in the range of 0.2 to 1 to 2.0 to 1.
Claim 2
Dependent Claim
280 words
A process for preparing a molded silicon carbide product, which process comprises molding a mixture of silicon carbide powder, an organosilicon compound and a lubricant selected from the group consisting of higher fatty acids, higher fatty acid esters, higher fatty acid amides, higher alcohols and paraffin wax into a compact and sintering the compact wherein the lubricant has the following properties: (a) it does not substantially evaporate during such operations as mixing, drying, molding, etc.; (b) it is in liquid or solid form, and when it is a solid, it has a melting point of 40° C. or higher; (c) it exhibits low viscosity in a melt of a mixture of the lubricant and organosilicon compound; and, (d) it undergoes almost complete evaporation at or below a temperature at which the organosilicon compound is pyrolyzed, i.e., at temperatures up to 500° C.; wherein the organosilicon compound is one or more compounds selected from those in which (1) silicon atoms are bonded only to carbon atoms; (2) besides the bonds between silicon atoms and carbon atoms, silicon atoms are bonded to hydrogen atoms; (3) besides the bonds between silicon atoms and carbon atoms, there are bonds formed between silicon atoms and halogen atoms; (4) in addition to the bonds between silicon atoms and carbon atoms, there are bonds established between silicon atoms per se; and (5) there are two or more types of bonds out of the above-mentioned bonds (2) through (4), or a polycondensation product, obtained by polycondensation of these compounds, containing silicon-carbon bonds as its principal backbone structure; and wherein the ratio of lubricant to organosilicon compound is in the range of 0.2 to 1 to 2.0 to 1.
Claim 3
Dependent Claim
17 words
A process as claimed in claim 1, wherein said higher fatty acids are used as a lubricant.
Claim 4
Dependent Claim
18 words
A process as claimed in claim 1, wherein said higher fatty acid esters are used as a lubricant.
Claim 5
Dependent Claim
18 words
A process as claimed in claim 1, wherein said higher fatty acid amides are used as a lubricant.
Claim 6
Dependent Claim
16 words
A process as claimed in claim 1, wherein said higher alcohols are used as a lubricant.
Claim 7
Dependent Claim
16 words
A process as claimed in claim 1, wherein said paraffin wax is used as a lubricant.
Claim 8
Dependent Claim
41 words
A process as claimed in claim 1, wherein two or more materials selected from the group consisting of higher fatty acids, higher fatty acid esters, higher fatty acid amides, higher alcohols and paraffin wax are used in combination as the lubricant.
Claim 9
Dependent Claim
20 words
A process as claimed in claim 1, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 10
Dependent Claim
15 words
A process as claimed in claim 1, wherein said molding is carried out by injection.
Claim 11
Dependent Claim
20 words
A process as claimed in claim 2, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 12
Dependent Claim
15 words
A process as claimed in claim 2, wherein said molding is carried out by injection.
Claim 13
Dependent Claim
20 words
A process as claimed in claim 3, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 14
Dependent Claim
15 words
A process as claimed in claim 3, wherein said molding is carried out by injection.
Claim 15
Dependent Claim
20 words
A process as defined in claim 4, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 16
Dependent Claim
15 words
A process as claimed in claim 4, wherein said molding is carried out by injection.
Claim 17
Dependent Claim
20 words
A process as claimed in claim 5, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 18
Dependent Claim
15 words
A process as claimed in claim 5, wherein said molding is carried out by injection.
Claim 19
Dependent Claim
20 words
A process as claimed in claim 6, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 20
Dependent Claim
15 words
A process as claimed in claim 6, wherein said molding is carried out by injection.
Claim 21
Dependent Claim
20 words
A process as claimed in claim 7, wherein a part of the silicon carbide powder consists of silicon carbide whiskers.
Claim 22
Dependent Claim
15 words
A process as claimed in claim 7, wherein said molding is carried out by injection.
Claim 23
Dependent Claim
15 words
A process as claimed in claim 8, wherein said molding is carried out by injection.
Claim 24
Dependent Claim
15 words
A process as claimed in claim 10, wherein said molding is carried out by injection.
Claim 25
Dependent Claim
15 words
A process as claimed in claim 12, wherein said molding is carried out by injection.
Claim 26
Dependent Claim
15 words
A process as claimed in claim 14, wherein said molding is carried out by injection.
Claim 27
Dependent Claim
15 words
A process as claimed in claim 16, wherein said molding is carried out by injection.
Claim 28
Dependent Claim
15 words
A process as claimed in claim 18, wherein said molding is carried out by injection.
Claim 29
Dependent Claim
15 words
A process as claimed in claim 20, wherein said molding is carried out by injection.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-12-23 | 1989-06-24 | 1989-12-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-12-23 | 1993-06-24 | 1993-12-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-12-23 | 1997-06-24 | 1997-12-24 | $7700.00 | Window Closed / Lapsed |