US4557765A
Expired / Lapsed
US
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Method for amorphization of a metal crystal
Assignee: The University of Osaka
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Filing: 1984-03-02
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Granted: 1985-12-10
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Expires: 2004-03-02
Abstract
Abstract A desired shape of amorphous region is formed at a predetermined position in a metal crystal by introducing the desired shape of lattice defect at the predetermined position in the metal crystal, and then irradiating the lattice defect with an electron beam to form the desired shape of amorphous region at the predetermined position in the metal crystal.
Inventors
- 👤 Hirotaro Mori
- 👤 Hiroshi Fujita
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 09:16
CPC Classifications
C; C22; C22F; C22F3/00
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
168 words
A method of forming an amorphous metal region at a predetermined position within an intermetallic compound comprising the steps of: (a) introducing a lattice defect having a given shape at said predetermined position within said intermetallic compound by adjusting the arrangement of the lattice defects, said defect being selected from the group consisting of a dislocation line, stacking fault, crystal grain boundary and foreign interface; (b) irradiating said intermetallic compound with an electron beam having a flux density not exceeding approximately 1×10 24 e/m 2 . sec, the energy of said electron beam being sufficient to introduce damage to said intermetallic compound, particularly in the vicinity of said lattice defect, in addition to that produced in step (a); (c) heating said intermetallic compound to a temperature not exceeding approximately 273° K.; and (d) maintain said electron beam irradiation for a time not exceeding approximately 1300 seconds to cause amorphorization along said lattice defect, said intermetallic compound being selected from the group consisting of NiTi and Co 2 Ti.
Claim 2
Independent Claim
168 words
A method of forming an amorphous metal region at a predetermined position within an intermetallic compound comprising the steps of: (a) introducing a lattice defect having a given shape at said predetermined position within said intermetallic compound by adjusting the arrangement of the lattice defects, said defect being selected from the group consisting of a dislocation line, stacking fault, crystal grain boundary and foreign interface; (b) irradiating said intermetallic compound with an electron beam having a flux density not exceeding approximately 1×10 24 e/m 2 . sec, the energy of said electron beam being sufficient to introduce damage to said intermetallic compound, particularly in the vicinity of said lattice defect, in addition to that produced in step (a); (c) heating said intermetallic compound to a temperature not exceeding approximately 273° K.; and (d) maintain said electron beam irradiation for a time not exceeding approximately 1300 seconds to cause amorphorization along said lattice defect, said intermetallic compound being selected from the group consisting of NiTi and Co 2 Ti.
Claim 3
Dependent Claim
57 words
The method as claimed in claim 1, wherein the intermetallic compound is NiTi, the lattice defect is introduced in step (a) by rolling said intermetallic compound at room temperature, the heating of step (c) is conducted at a temperature in the range of 255° to 273° K. and the electron beam is maintained for approximately 1300 seconds.
Claim 4
Dependent Claim
58 words
The method as claimed in claim 1, wherein the intermetallic compound is NiTi, the lattice defect is introduced in step (a) by annealing said intermetallic compound at approximately 1,173° K. for about 12 KS, the heating of step (c) is conducted at a temperature of approximately 260° K. and the electron beam is maintained for approximately 1300 seconds.
Claim 5
Dependent Claim
87 words
The method as claimed in claim 1, wherein the intermetallic compound is Co 2 Ti, the lattice defect is introduced in step (a) by annealing said intermetallic compound at approximately 1273° K. for about 160 KS, the irradiating of said intermetallic compound in step (a) is conducted with an electron beam having a flux density of approximately 1×10 24 e/m 2 . sec, the heating of step (c) is conducted at a temperature of approximately 160° K. and the electron beam is maintained for approximately 120 seconds.
Claim 6
Dependent Claim
43 words
The method as claimed in claim 1, wherein said lattice defect is introduced in step (a) into said intermetallic compound at said predetermined position by a method selected from the group consisting of plastic deformation, heat treatment and irradiation with a particle ray.
References Cited (Backward Citations)
US3926682A
Cited
US4122240A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-12-09 | 1989-06-10 | 1989-12-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-12-09 | 1993-06-10 | 1993-12-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-12-09 | 1997-06-10 | 1997-12-10 | $7700.00 | Window Closed / Lapsed |