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US4552776A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparation of tea color concentrate and product

Assignee: Procter and Gamble Co
•
Filing: 1984-12-21
•
Granted: 1985-11-12
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Expires: 2004-12-21
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Abstract

Abstract The present invention comprises a process for preparation of tea concentrate with enhanced natural color and the products prepared thereby. Tea is employed as a catalyst to reactions generating color formation. The resulting enhanced color of the tea concentrate and the tea products and beverages prepared therefrom is storage-stable. The process comprises heating a solution of sugar and acid to effect caramelization reactions, followed by adding tea solids and heating to a higher temperature to catalyze Maillard reactions.

Inventors

  • 👤 Hing-Cheung Tse

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 14:56
CPC Classifications
A; A23; A23F; A23F3/00; A23F3/16; A23F3/163; A23F3/30

Claims Analysis

Total Claims: 19
Claim 1
Independent Claim 174 words
A process for preparation of a tea concentrate of enhanced color and having a pH of about 1.5 to about 3.0 comprising: (a) heating a solution of one or more reducing sugars and acid to a temperature of from about 220° F. (104° C.) to about 300° F. (149° C.) for about 15 minutes, the ratio of acid to reducing sugar is from about 1:0.5 to about 1:5; (b) adding soluble tea solids to the solution and heating the resulting mixture to a temperature of from about 280° F. (138° C.) to about 360° F. (182° C.) for about 30 minutes, the ratio of tea solids to reducing sugars is from about 1:6 to about 1:75; (c) adding water to the mixture and maintaining the resulting mixture at a temperature of from about 170° F. (77° C.) to about 210° F. (99° C.) for about 45 minutes, the ratio of water to reducing sugars is from about 1:3 to about 3:1; and (d) separating any insolubles to yield a tea concentrate of enhanced color.
Claim 2
Dependent Claim 174 words
A process for preparation of a tea concentrate of enhanced color and having a pH of about 1.5 to about 3.0 comprising: (a) heating a solution of one or more reducing sugars and acid to a temperature of from about 220° F. (104° C.) to about 300° F. (149° C.) for about 15 minutes, the ratio of acid to reducing sugar is from about 1:0.5 to about 1:5; (b) adding soluble tea solids to the solution and heating the resulting mixture to a temperature of from about 280° F. (138° C.) to about 360° F. (182° C.) for about 30 minutes, the ratio of tea solids to reducing sugars is from about 1:6 to about 1:75; (c) adding water to the mixture and maintaining the resulting mixture at a temperature of from about 170° F. (77° C.) to about 210° F. (99° C.) for about 45 minutes, the ratio of water to reducing sugars is from about 1:3 to about 3:1; and (d) separating any insolubles to yield a tea concentrate of enhanced color.
Claim 3
Dependent Claim 14 words
The process of claim 1 wherein the acid comprises citric acid or phosphoric acid.
Claim 4
Dependent Claim 14 words
The process of claim 1 wherein the reducing sugars comprise high fructose corn syrup.
Claim 5
Dependent Claim 35 words
The process of claim 1 further comprising cooling the solution of step (a) to a temperature of from about 210° F. (99° C.) to about 250° F. (121° C.) prior to adding the tea solids.
Claim 6
Dependent Claim 13 words
The process of claim 1 wherein the water comprises distilled or deionized water.
Claim 7
Dependent Claim 34 words
The process of claim 1 further comprising cooling the mixture of step (b) to a temperature of from about 210° F. (99° C.) to about 250° F. (121° C.) prior to adding the water.
Claim 8
Dependent Claim 13 words
The process of claim 1 wherein the separation is by means of filtration.
Claim 9
Dependent Claim 20 words
The process of claim 1 wherein the tea concentrate has a tinctorial power of from about 0.10 to about 0.50.
Claim 10
Dependent Claim 20 words
The process of claim 1 wherein the tea concentrate has a hue index of from about 3.0 to about 9.0.
Claim 11
Dependent Claim 44 words
The process of claim 1 wherein the tea concentrate has a Hunter "L" value of from about 75 to about 85, a Hunter "a" value of from about 0.2 to about 2.0, and a Hunter "b" value of from about 25 to about 35.
Claim 12
Dependent Claim 233 words
A process for enhancing tea color comprising: (a) heating a solution of high fructose corn syrup and edible acid in a ratio of from about 1:0.5 to about 1:5 to a temperature of from about 220° F. (104° C.) to about 300° F. (149° C.) for about 15 minutes; (b) cooling the solution of step (a) to a temperature of from about 210° F. (99° C.) to about 250° F. (121° C.) for about 15 minutes; (c) adding soluble tea solids to the solution in a ratio to the reducing sugars of from about 1:6 to about 1:75 heating the resulting mixture to a temperature of from about 280° F. (138° C.) to about 360° F. (182° C.) for about 30 minutes; (d) cooling the mixture of step (b) to a temperature of from about 210° F. (99° C.) to about 250° F. (121° C.); (e) adding water to the mixture in a ratio to the reducing sugars of from about 1:3 to about 3:1, and maintining the resulting mixture at a temperature of from about 170° F. (77° C.) to about 210° F. (99° C.) with agitation for about 45 minutes; and (f) separating any insolubles to yield a tea concentrate having a pH of from about 1.5 to about 3.0, a hue index of from about 3.0 to about 9.0, and a tinctorial power of from about 0.10 to about 0.50.
Claim 13
Dependent Claim 233 words
A process for enhancing tea color comprising: (a) heating a solution of high fructose corn syrup and edible acid in a ratio of from about 1:0.5 to about 1:5 to a temperature of from about 220° F. (104° C.) to about 300° F. (149° C.) for about 15 minutes; (b) cooling the solution of step (a) to a temperature of from about 210° F. (99° C.) to about 250° F. (121° C.) for about 15 minutes; (c) adding soluble tea solids to the solution in a ratio to the reducing sugars of from about 1:6 to about 1:75 heating the resulting mixture to a temperature of from about 280° F. (138° C.) to about 360° F. (182° C.) for about 30 minutes; (d) cooling the mixture of step (b) to a temperature of from about 210° F. (99° C.) to about 250° F. (121° C.); (e) adding water to the mixture in a ratio to the reducing sugars of from about 1:3 to about 3:1, and maintining the resulting mixture at a temperature of from about 170° F. (77° C.) to about 210° F. (99° C.) with agitation for about 45 minutes; and (f) separating any insolubles to yield a tea concentrate having a pH of from about 1.5 to about 3.0, a hue index of from about 3.0 to about 9.0, and a tinctorial power of from about 0.10 to about 0.50.
Claim 14
Dependent Claim 23 words
The process of claim 1 wherein the tea concentrate of step (d) is dried and pulverized prior to addition to the tea mix.
Claim 15
Dependent Claim 29 words
The process of claim 1 wherein the tea concentrate of step (d) is diluted with water to yield a liquid tea product suitable for preparation of a tea beverage.
Claim 16
Dependent Claim 7 words
The product prepared according to claim 1.
Claim 17
Dependent Claim 7 words
The product prepared according to claim 11.
Claim 18
Dependent Claim 7 words
The product prepared according to claim 12.
Claim 19
Dependent Claim 7 words
The product prepared according to claim 13.

References Cited (Backward Citations)

US4440796A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-11-11 1989-05-13 1989-11-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-11-11 1993-05-13 1993-11-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-11-11 1997-05-13 1997-11-12 $7700.00 Window Closed / Lapsed

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