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US4540444A Expired / Lapsed US ⏱️ 0.0 years remaining

Aluminum cleaner and system

Assignee: Henkel Corp
•
Filing: 1982-08-12
•
Granted: 1985-09-10
•
Expires: 2002-08-12
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Abstract

Abstract Processes and alkaline cleaning compositions for cleaning aluminum containers to prevent off-flavor and off-taste in liquid comestible products with which the containers are filled. The processes involve the use of an aqueous alkaline cleaning solution having the following compositions: ______________________________________ Ingredient Quantity, g/l ______________________________________ 1. Alkali metal or ammonium carbonate 0.1-0.9 2. Alkali metal or ammonium tripoly- 0.6-7.6 phosphate (anhydrous) 3. Alkali metal or ammonium tetraborate 0.5-6.3 (pentahydrate) 4. Alkali metal or ammonium metasilicate 0.1-0.8 (anhydrous) 5. Tri(alkali metal or ammonium)phosphate 0.4-5.4 (anhydrous) 6. Alkali metal or ammonium gluconate or 0.1-1.3 glucoheptonate 7. Surfactant 0.02-0.27 ______________________________________

Inventors

  • 👤 Timm L. Kelly

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 16:21
CPC Classifications
C; C23; C23G; C23G1/00; C23G1/14; C23G1/22

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 210 words
In a method for cleaning aluminum or aluminum alloy beverage containers comprising the use of an acid cleaning bath, the improvement comprising treating the containers subsequent to the acid cleaning bath with an alkaline cleaning solution for from about 5 seconds to about 1 minute at a temperature in the range of from about 90° F. to about 130° F. to remove trace impurities including C 7 -C 9 aldehydes that cause off-flavor in beverages, wherein said alkaline cleaning solution consists essentially of: (a) from about 0.2 to about 0.6 g/l of at least one alkali metal or ammonium carbonate; (b) from about 2.0 to about 5.1 g/l of at least one alkali metal or ammonium tripolyphosphate; (c) from about 1.7 to about 4.2 g/l of at least one alkali metal or ammonium tetraborate pentahydrate; (d) from about 0.2 to about 0.5 g/l of at least one alkali metal or ammonium metasilicate; (e) from about 1.4 to about 3.6 g/l of at least one tri(alkali metal or ammonium) phosphate; (f) from about 0.3 to about 0.9 g/l of at least one alkali metal or ammonium gluconate or glucoheptonate; and (g) from about 0.02 to about 0.27 g/l of at least one surfactant which is stable in the aqueous alkaline solution.
Claim 2
Dependent Claim 210 words
In a method for cleaning aluminum or aluminum alloy beverage containers comprising the use of an acid cleaning bath, the improvement comprising treating the containers subsequent to the acid cleaning bath with an alkaline cleaning solution for from about 5 seconds to about 1 minute at a temperature in the range of from about 90° F. to about 130° F. to remove trace impurities including C 7 -C 9 aldehydes that cause off-flavor in beverages, wherein said alkaline cleaning solution consists essentially of: (a) from about 0.2 to about 0.6 g/l of at least one alkali metal or ammonium carbonate; (b) from about 2.0 to about 5.1 g/l of at least one alkali metal or ammonium tripolyphosphate; (c) from about 1.7 to about 4.2 g/l of at least one alkali metal or ammonium tetraborate pentahydrate; (d) from about 0.2 to about 0.5 g/l of at least one alkali metal or ammonium metasilicate; (e) from about 1.4 to about 3.6 g/l of at least one tri(alkali metal or ammonium) phosphate; (f) from about 0.3 to about 0.9 g/l of at least one alkali metal or ammonium gluconate or glucoheptonate; and (g) from about 0.02 to about 0.27 g/l of at least one surfactant which is stable in the aqueous alkaline solution.
Claim 3
Dependent Claim 22 words
A method according to claim 1 wherein the temperature is in the range of from about 100° F. to about 115° F.
Claim 4
Dependent Claim 19 words
A method in accordance with claim 1 wherein said time is from about 10 seconds to about 30 seconds.
Claim 5
Independent Claim 28 words
A method in accordance with any one of claims 1, 2, or 3 wherein the containers are treated by spraying the alkaline cleaning solution onto the surfaces thereof.
Claim 6
Dependent Claim 18 words
A method in accordance with claim 1 wherein the surfactant (g) is at least one low foaming surfactant.
Claim 7
Dependent Claim 229 words
In a method for cleaning aluminum or aluminum alloy beverage containers comprising the steps of prerinse; acid prewash; acid clean; rinse; and deionized water rinse, the improvement comprising adding the following steps between the rinse and deionized water rinse steps to remove trace impurities including C 7 -C 9 aldehydes that cause off-flavor in beverages: A. spraying said containers with an alkaline cleaning solution for from about 5 seconds to about 1 minute at a temperature in the range of from about 90° F. to about 130° F., wherein the alkaline solution consists essentially of (a) from about 0.2 to about 0.6 g/l of at least one alkali metal or ammonium carbonate; (b) from about 2.0 to about 5.1 g/l of at least one alkali metal or ammonium tripolyphosphate; (c) from about 1.7 to about 4.2 g/l of at least one alkali metal or ammonium tetraborate pentahydrate; (d) from about 0.2 to about 0.5 g/l of at least one alkali metal or ammonium metasilicate; (e) from about 1.4 to about 3.6 g/l of at least one tri(alkali metal or ammonium) phosphate; (f) from about 0.3 to about 0.9 g/l of at least one alkali metal or ammonium gluconate or glucoheptonate; and (g) from about 0.02 to about 0.27 g/l of at least one surfactant which is stable in the aqueous alkaline solution; and B. rinsing the containers with water.
Claim 8
Dependent Claim 229 words
In a method for cleaning aluminum or aluminum alloy beverage containers comprising the steps of prerinse; acid prewash; acid clean; rinse; and deionized water rinse, the improvement comprising adding the following steps between the rinse and deionized water rinse steps to remove trace impurities including C 7 -C 9 aldehydes that cause off-flavor in beverages: A. spraying said containers with an alkaline cleaning solution for from about 5 seconds to about 1 minute at a temperature in the range of from about 90° F. to about 130° F., wherein the alkaline solution consists essentially of (a) from about 0.2 to about 0.6 g/l of at least one alkali metal or ammonium carbonate; (b) from about 2.0 to about 5.1 g/l of at least one alkali metal or ammonium tripolyphosphate; (c) from about 1.7 to about 4.2 g/l of at least one alkali metal or ammonium tetraborate pentahydrate; (d) from about 0.2 to about 0.5 g/l of at least one alkali metal or ammonium metasilicate; (e) from about 1.4 to about 3.6 g/l of at least one tri(alkali metal or ammonium) phosphate; (f) from about 0.3 to about 0.9 g/l of at least one alkali metal or ammonium gluconate or glucoheptonate; and (g) from about 0.02 to about 0.27 g/l of at least one surfactant which is stable in the aqueous alkaline solution; and B. rinsing the containers with water.

References Cited (Backward Citations)

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US3039970A Cited
US3524817A Cited
US3669893A Cited
US3888783A Cited
US4116853A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-09-09 1989-03-11 1989-09-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-09-09 1993-03-11 1993-09-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-09-09 1997-03-11 1997-09-10 $7700.00 Window Closed / Lapsed

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