Process for increasing filling capacity of tobacco

Claim 2

A process for increasing the filling capacity of tobacco which comprises contacting tobacco with an inert gaseous expansion agent at a pressure above about 4.5 Kg/cm 2 below the critical pressure of said expansion agent and at a temperature in the range of from about 20° C. below to about 42° C. above the critical temperature of said expansion agent and subsequently releasing the pressure within a time period of from one second to ten minutes, thereby causing the tobacco to expand.

Claim 3

The process of claim 1 wherein said contacting is effected at a temperature in the range of from the critical temperature of said expansion agent to about 42° C. above said critical temperature.

Claim 4

The process of claim 1 or 2 wherein said contacting is effected at a pressure above about 57 Kg/cm 2 .

Claim 5

The process of claim 1 or 2 wherein said contacting is effected at a pressure above about 57 Kg/cm 2 and said time period is from 3 to 300 seconds.

Claim 6

The process of claim 1 or 2 wherein said contacting is effected at a pressure above about 57 Kg/cm 2 , said time period is from 3 to 300 seconds and said expansion agent is selected from the class consisting of hydrocarbons and halocarbons having an atmospheric pressure boiling point in the range of -90° to 2° C.

Claim 7

A process for increasing the filling capacity of tobacco at least 50% which comprises, impregnating the tobacco with vapor of an inert expansion agent at supercritical pressure for said agent and thereafter reducing the pressure so as to cause the expansion agent to expand the cellular structure of the tobacco and to be expelled therefrom without the necessity of subjecting the tobacco to additional heat.

Claim 8

A process for increasing the filling capacity of tobacco at least 50% which comprises, impregnating the tobacco with vapor of an inert expansion agent at supercritical pressure for said agent and thereafter reducing the pressure so as to cause the expansion agent to expand the cellular structure of the tobacco and to be expelled therefrom without the necessity of subjecting the tobacco to additional heat.

Claim 9

A process for increasing the filling capacity of cut filler tobacco for cigarettes which comprises impregnating the tobacco with vapor of a low-boiling highly volatile inert expansion agent at supercritical conditions of pressure and temperature for said agent and thereafter reducing the pressure so as to cause the expansion agent to be expelled therefrom to expand the cellular structure of the tobacco by at least 50% and without subjecting the tobacco to additional heat.

Claim 10

A process for increasing the filling capacity of cut filler tobacco for cigarettes which comprises impregnating the tobacco with vapor of a low-boiling highly volatile inert expansion agent at supercritical conditions of pressure and temperature for said agent and thereafter reducing the pressure so as to cause the expansion agent to be expelled therefrom to expand the cellular structure of the tobacco by at least 50% and without subjecting the tobacco to additional heat.

Claim 11

A process for increasing the filling capacity of cigarette cut filler tobacco by expanding its cellular structure which comprises placing the tobacco in a pressure vessel, introducing a low-boiling highly volatile inert gaseous expansion agent having a critical temperature between 32° C. and 120° C. into the vessel in contact with the tobacco and increasing the pressure to above the critical pressure of the expansion agent to thoroughly permeate the cellular structure of the tobacco with the expansion agent in a highly condensed state, thereafter reducing the pressure to cause the expansion agent to change from its highly condensed state to an expanded vapor state, thereby expanding the cellular structure by at least 50% as the expansion agent is expelled therefrom.

Claim 12

A process for increasing the filling capacity of cigarette cut filler tobacco by expanding its cellular structure which comprises placing the tobacco in a pressure vessel, introducing a low-boiling highly volatile inert gaseous expansion agent having a critical temperature between 32° C. and 120° C. into the vessel in contact with the tobacco and increasing the pressure to above the critical pressure of the expansion agent to thoroughly permeate the cellular structure of the tobacco with the expansion agent in a highly condensed state, thereafter reducing the pressure to cause the expansion agent to change from its highly condensed state to an expanded vapor state, thereby expanding the cellular structure by at least 50% as the expansion agent is expelled therefrom.

Claim 13

A process for increasing the filling capacity of tobacco which comprises contacting tobacco with an inert gaseous expansion agent selected from the class consisting of hydrocarbons and halocarbons, at a pressure of at least 36 Kg/cm 2 and at a temperature in the range of from about 20° C. below to about 42° C. above the critical temperature of said expansion agent, and subsequently expelling said expansion agent from the tobacco by releasing the pressure within a time period of from one second to ten minutes, thereby expanding the cellular structure of the tobacco.

Claim 14

A process for increasing the filling capacity of tobacco which comprises contacting tobacco with an inert gaseous expansion agent selected from the class consisting of hydrocarbons and halocarbons, at a pressure of at least 36 Kg/cm 2 and at a temperature in the range of from about 20° C. below to about 42° C. above the critical temperature of said expansion agent, and subsequently expelling said expansion agent from the tobacco by releasing the pressure within a time period of from one second to ten minutes, thereby expanding the cellular structure of the tobacco.

Claim 15

The process of claim 9 wherein said time period is 3 to 300 seconds.

Claim 16

The process of claim 9 wherein said time period is 5 to 20 seconds.

Claim 17

The process of claim 9 wherein said contacting is effected at a pressure above about 70 Kg/cm 2 .

Claim 18

A process for increasing the filling capacity of tobacco by 50% or more which comprises contacting tobacco having a moisture content in the range of 10 to 30 wt.% with an inert normally-gaseous expansion agent selected from the class consisting of hydrocarbons and halocarbons having a critical temperature in the range of from 30° to 155° C., said contacting being effected at a pressure above about 36 Kg/cm 2 and at a temperature in the range of from 20° C. below to 42° C. above the critical temperature of said expansion agent to produce tobacco impregnated with said expansion agent, releasing said expansion agent from said impregnated tobacco at a rate such that the pressure is reduced to about atmospheric pressure within a time period of one second to ten minutes to expand the cellular structure of the tobacco in the absence of a separate heating step.

Claim 19

A process for increasing the filling capacity of tobacco by 50% or more which comprises contacting tobacco having a moisture content in the range of 10 to 30 wt.% with an inert normally-gaseous expansion agent selected from the class consisting of hydrocarbons and halocarbons having a critical temperature in the range of from 30° to 155° C., said contacting being effected at a pressure above about 36 Kg/cm 2 and at a temperature in the range of from 20° C. below to 42° C. above the critical temperature of said expansion agent to produce tobacco impregnated with said expansion agent, releasing said expansion agent from said impregnated tobacco at a rate such that the pressure is reduced to about atmospheric pressure within a time period of one second to ten minutes to expand the cellular structure of the tobacco in the absence of a separate heating step.

Claim 20

A process for expanding tobacco to increase the filling capacity thereof which comprises contacting tobacco with an inert vaporous expansion agent selected from the group consisting of hydrocarbons and halocarbons having a critical temperature in the range of from 30° to 155° C., said contacting being effected at a temperature equal to or greater than the critical temperature of said expansion agent and at a pressure above about 4.5 Kg/cm 2 below the critical pressure of said expansion agent to impregnate the tobacco, reducing the pressure causing at least a portion of said expansion agent to transfer to the liquid phase and condense in the tobacco, continuing to reduce the pressure until the pressure reaches about atmospheric pressure in less than about ten minutres, thereby causing the expansion agent to be vaporized and separated from the tobacco and the tobacco to be expanded.

Claim 21

A process for expanding tobacco to increase the filling capacity thereof which comprises contacting tobacco with an inert vaporous expansion agent selected from the group consisting of hydrocarbons and halocarbons having a critical temperature in the range of from 30° to 155° C., said contacting being effected at a temperature equal to or greater than the critical temperature of said expansion agent and at a pressure above about 4.5 Kg/cm 2 below the critical pressure of said expansion agent to impregnate the tobacco, reducing the pressure causing at least a portion of said expansion agent to transfer to the liquid phase and condense in the tobacco, continuing to reduce the pressure until the pressure reaches about atmospheric pressure in less than about ten minutres, thereby causing the expansion agent to be vaporized and separated from the tobacco and the tobacco to be expanded.

Claim 22

The process of claim 14 wherein said contacting is effected at a pressure of at least about 57 Kg/cm 2 .

Claim 23

A process for increasing the filing capacity of tobacco which comprises contacting tobacco with an inert vaporous expansion agent selected from the group consisting of ethane, propane, propylene, dichlorodifluoromethane, monochlorodifluoromethane, isobutane, n-butane, and mixtures thereof, at a temperature from 20° C. below up to 42° C. above the critical temperature of said expansion agent and at a pressure above about 4.5 Kg/cm 2 below the critical pressure of said expansion agent to impregnate the tobacco, and reducing the pressure until the expansion agent pressure on the tobacco reaches substantially atmospheric pressure within a period of one second to about ten minutes, thereby causing the expansion agent to be expelled from the tobacco and the tobacco to expand.

Claim 24

A process for increasing the filing capacity of tobacco which comprises contacting tobacco with an inert vaporous expansion agent selected from the group consisting of ethane, propane, propylene, dichlorodifluoromethane, monochlorodifluoromethane, isobutane, n-butane, and mixtures thereof, at a temperature from 20° C. below up to 42° C. above the critical temperature of said expansion agent and at a pressure above about 4.5 Kg/cm 2 below the critical pressure of said expansion agent to impregnate the tobacco, and reducing the pressure until the expansion agent pressure on the tobacco reaches substantially atmospheric pressure within a period of one second to about ten minutes, thereby causing the expansion agent to be expelled from the tobacco and the tobacco to expand.

Claim 25

A process for increasing the filling capacity of tobacco which comprises confining tobacco within a pressure vessel, introducing an inert gaseous expansion agent selected from the class consisting of hydrocarbons and halogenated hydrocarbons having a critical temperature in the range of from 30° to 155° C. into said vessel into contact with said tobacco in an amount sufficient to raise the pressure within said vessel to above about 70 Kg/cm 2 while maintaining said expansion agent substantially in the vapor phase, releasing the gaseous expansion agent from said vessel at a controlled rate to reduce the pressure in said vessel to substantially atmospheric pressure within a time period of from one second to ten minutes, thereby expanding the tobacco without adding heat.

Claim 26

A process for increasing the filling capacity of tobacco which comprises confining tobacco within a pressure vessel, introducing an inert gaseous expansion agent selected from the class consisting of hydrocarbons and halogenated hydrocarbons having a critical temperature in the range of from 30° to 155° C. into said vessel into contact with said tobacco in an amount sufficient to raise the pressure within said vessel to above about 70 Kg/cm 2 while maintaining said expansion agent substantially in the vapor phase, releasing the gaseous expansion agent from said vessel at a controlled rate to reduce the pressure in said vessel to substantially atmospheric pressure within a time period of from one second to ten minutes, thereby expanding the tobacco without adding heat.

Claim 27

The process of claim 17 wherein said time period is from 3 to 300 seconds.

Claim 28

The process of claim 17 wherein said expansion agent is selected from the group consisting of ethane, propane, propylene, Refrigerant 12, Refrigerant 22, isobutane, n-butane, and mixtures thereof.

Claim 29

The process of claim 19 wherein said time period is from 5 to 20 seconds.

Claim 30

Tobacco treated in accordance with the process of claim 17.

Claim 31

The process of claim 1, wherein the expansion agent is a material which has a critical temperature within the range of about 32° C. to 120° C.

Claim 32

The process of claim 22, wherein the expansion agent is a light hydrocarbon, a halogenated hydrocarbon or a mixture thereof.

Claim 33

The process of claim 25, wherein the expansion agent comprises ethane, propane, propylene, n-butane, isobutane, dichlorodifluoromethane or monochlorodifluoromethane or a mixture thereof.

Claim 34

The process of claim 24, wherein the expansion is effected without an additional heating step.

Claim 35

The process of claim 1, wherein the expansion agent comprises a mixture of materials, and wherein the filling capacity of the tobacco is increased by at least 50%.

Claim 36

The process of claim 1, wherein the expansion agent is a material having an atmospheric boiling point of about -90° to about 2° C.

Claim 37

The process of claim 1, wherein the pressure at which the tobacco is contacted with the expansion agent is below about 142 Kg/cm 2 .

Claim 38

The process of claim 6, 7, 9, 13, 14 or 16 wherein the expansion agent comprises a hydrocarbon or halogenated hydrocarbon having a critical temperature within the range of 32° C.-120° C.

Claim 39

The process of claim 29, wherein the tobacco is contacted with the expansion agent at a pressure above about 4.5 Kg/cm 2 below the critical pressure of the expansion agent.