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US4528043A Expired / Lapsed US ⏱️ 0.0 years remaining

Surface oxide layer treatment

Assignee: Rolls Royce PLC
•
Filing: 1983-05-13
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Granted: 1985-07-09
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Expires: 2003-05-13
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Abstract

Abstract In Titanium casting the surface of the casting is usually contaminated with a brittle oxide layer which has to be removed. Physical or chemical machining reduces the dimensions of the casting and adds to its cost. Chemical reagents may remove fine surface detail. In accordance with the invention the oxygen in the oxide layer is removed by contacting the surface of the casting with an oxide scavenge agent, notably Titanium, for a sufficient time and at a sufficient temperature to allow diffusion of the oxygen from the surface into the scavenge agent.

Inventors

  • 👤 David Mills

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 00:03
CPC Classifications
C; C23; C23G; C23G5/00; Y; Y10; Y10S; Y10S148/00; Y10S148/901; Y10T; Y10T428/00; Y10T428/12; Y10T428/12493; Y10T428/12736; Y10T428/12743

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 86 words
A method of treating a surface oxide layer on an article comprising the steps of contacting the surface oxide layer to be treated with a powdered oxygen scavenge agent and heat treating the article in an inert atmosphere for a sufficient time and at a sufficient temperature to cause the oxygen in the surface oxide layer to diffuse into the powdered oxygen scavenge agent so that a substantially unoxidized material of substantially the same dimensions as the surface oxide layer remains as part of the article.
Claim 2
Independent Claim 86 words
A method of treating a surface oxide layer on an article comprising the steps of contacting the surface oxide layer to be treated with a powdered oxygen scavenge agent and heat treating the article in an inert atmosphere for a sufficient time and at a sufficient temperature to cause the oxygen in the surface oxide layer to diffuse into the powdered oxygen scavenge agent so that a substantially unoxidized material of substantially the same dimensions as the surface oxide layer remains as part of the article.
Claim 3
Dependent Claim 14 words
A method according to claim 1 wherein the article is a cast titanium component.
Claim 4
Dependent Claim 14 words
A method according to claim 2 wherein the oxygen scavenge agent is titanium powder.
Claim 5
Dependent Claim 32 words
A method according to claim 1 wherein the powdered oxygen scavenge agent contains an enhancing agent which diffuses into the article during the heat treatment to enhance the properties of the article.
Claim 6
Dependent Claim 12 words
A method according to claim 4 wherein the enhancing agent is aluminium.

References Cited (Backward Citations)

CA573091A Cited
CA630874A Cited
US3000755A Cited
US3037883A Cited
GB1050409A Cited
US3556744A Cited
GB1205478A Cited
US3640778A Cited
US3958047A Cited
US3903338A Cited
DE2153218A1 Cited
SU691499A1 Cited
US4098450A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-07-08 1989-01-07 1989-07-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-07-08 1993-01-07 1993-07-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-07-08 1997-01-07 1997-07-09 $7700.00 Window Closed / Lapsed

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