US4526673A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Coating method
Assignee: Spire Corp
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Filing: 1983-12-19
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Granted: 1985-07-02
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Expires: 2003-12-19
Abstract
Abstract A coating apparatus and method for coating industrial cutting and turning tools of any desired shape and configuration and the like significantly to improve the tools' working properties. The coating is formed of cubic boron nitride, with a preferred thickness not exceeding ten microns. The coating apparatus includes an rf excited plasma source chamber having a gas feed ring for ionizing a gas admitted into the chamber via the ring. The preferred feedgas is a borazine and benzene vapor mixture. A coating chamber is mounted adjacent to and contiguous with the plasma source chamber via a neck portion. The coating chamber includes a vacuum interlock to permit the entry and removal of a tool transport. At least one vacuum pump is operatively connected to the chamber. Preferably, a plurality of permanent magnets and electron supply filaments are arranged circumferentially about the plasma source chamber. Preferably, the tool transport is rotatable during coating. Preferably, the apparatus is microprocessor controlled.
Inventors
- 👤 Roger G. Little
- 👤 Stanley R. Shanfield
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-27 20:38
CPC Classifications
H; H01; H01J; H01J37/00; H01J37/32; H01J37/32431; C; C04; C04B; C04B35/00; C04B35/515; C04B35/58; C04B35/583; C04B35/5831; C23; C23C; C23C16/00; C23C16/22; C23C16/30; C23C16/34; C23C16/342; C23C16/44; C23C16/50; C23C16/505; C23C16/509; H01J37/02; H01J37/04; H01J37/08
Claims Analysis
Total Claims: 14
Claim 1
Independent Claim
143 words
A process of coating parts comprising: (a) positioning a plurality of parts on a work transport; (b) introducing said plurality of parts with said work transport into a coating chamber maintained under vacuum; (c) subjecting said plurality of parts to cleaning by ion beam milling in an inert gas environment; (d) providing a negative bias to said plurality of parts in said coating chamber; (e) exposing said plurality of negatively biased parts within said coating chamber to a beam of ions extracted from an rf excited plasma acting on a feed as introduced into a second chamber adjacent and contiguous with said coating chamber for a time period not exceeding sixty minutes; and (f) progressively increasing the beam energy of said beam of ions from about 300 electron-volts to about 1200 electron-volts while said plurality of negatively biased parts are being exposed thereto.
Claim 2
Dependent Claim
143 words
A process of coating parts comprising: (a) positioning a plurality of parts on a work transport; (b) introducing said plurality of parts with said work transport into a coating chamber maintained under vacuum; (c) subjecting said plurality of parts to cleaning by ion beam milling in an inert gas environment; (d) providing a negative bias to said plurality of parts in said coating chamber; (e) exposing said plurality of negatively biased parts within said coating chamber to a beam of ions extracted from an rf excited plasma acting on a feed as introduced into a second chamber adjacent and contiguous with said coating chamber for a time period not exceeding sixty minutes; and (f) progressively increasing the beam energy of said beam of ions from about 300 electron-volts to about 1200 electron-volts while said plurality of negatively biased parts are being exposed thereto.
Claim 3
Dependent Claim
18 words
The process of claim 1 wherein said parts to be coated are of any desired shape and configuration.
Claim 4
Dependent Claim
38 words
The process of claim 1 wherein said parts are formed of any one of the group including: steels, tungsten carbides, ceramics, plastics, quartz, carbon tool sheets, titanium-nickel or titanium-carbide or aluminum-oxide coated metals, diamond-like carbon, and semiconductor materials.
Claim 5
Dependent Claim
37 words
The process of claim 1 wherein said parts include industrial cutting and turning tools, such as tool bits, drill bits, machining bits, grinding wheels, chisels, saw blades, razor blades, surgical tools, ball bearings, abrasives and the like.
Claim 6
Dependent Claim
25 words
The process of claim 1 wherein the pressure of said coating chamber maintained under vacuum is from about 10 -8 to about 10 -2 torr.
Claim 7
Dependent Claim
17 words
The process of claim 1 wherein said negative bias is from about -1 to about -1000 VDC.
Claim 8
Dependent Claim
42 words
The process of claim 1 wherein said ion beam has a diameter of from about 20 to about 50 cm, a beam energy of up to 2000 electron-volts, a beam current density of from about 0.5 to about 5 mA/cm 2 .
Claim 9
Dependent Claim
28 words
The process of claim 1 wherein said feedgas is a mixture of borazine vapor and benzene vapor, and the resultant coating on said parts is cubic boron nitride.
Claim 10
Dependent Claim
11 words
The process of claim 8 wherein said feedgas also contains hydrogen.
Claim 11
Dependent Claim
11 words
The process of claim 8 wherein said feedgas also contains helium.
Claim 12
Dependent Claim
40 words
The process of claim 1 wherein said second chamber also is maintained under vacuum at a pressure from about 10 -5 to about 10 1 torr, and wherein the outside of said second chamber is cooled to below 550° C.
Claim 13
Dependent Claim
25 words
The process of claim 1 wherein said negatively biased parts within said coating chamber also are rotated while being exposed to said beam of ions.
Claim 14
Dependent Claim
34 words
The process of claim 1 wherein said plurality of negatively biased parts within said coating chamber also are heated to a temperature of at least about 25° C. but not exceeding about 1000° C.
References Cited (Backward Citations)
No citation records indexed.
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-07-01 | 1988-12-31 | 1989-07-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-07-01 | 1992-12-31 | 1993-07-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-07-01 | 1996-12-31 | 1997-07-02 | $7700.00 | Window Closed / Lapsed |