US4502901A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Manufacture of gypsum board from FGD gypsum
Assignee: National Gypsum Properties LLC
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Filing: 1983-10-19
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Granted: 1985-03-05
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Expires: 2003-10-19
Abstract
Abstract By-product gypsum, which is formed during a flue gas desulfurization process, (FGD gypsum) is carefully formed as an aqueous slurry of crystals having a mean particle diameter of between about 35 microns and 80 microns and filtered, which filter cake is substantially completely dried before calcination, without any substantial grinding action, the crystals are then flash calcined to a hemihydrate, then ground, to reduce consistency, and then formed into an aqueous slurry from which a paper-covered gypsum board is formed of superior core quality.
Inventors
- 👤 Edward A. Burkard
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 19:35
CPC Classifications
C; C04; C04B; C04B11/00; C04B11/26; C04B11/262; C04B11/264
Claims Analysis
Total Claims: 19
Claim 1
Independent Claim
167 words
The method of making gypsum wallboard comprising the steps of removing substantially all of the free moisture from an about 94% to 98% pure gypsum filter cake of about 35 to 80 micron average particle diameter FGD dihydrate gypsum while avoiding any substantial reduction of particle size of said gypsum other than the breaking up of agglomerates of particles, flash calcining said dried FGD gypsum to about 25% of the water of hydration producing FGD hemihydrate gypsum, grinding at least about 25% of said calcined gypsum to produce a Fisher surface area of material of at least about 2500 cm 2 /gm, said surface area being measured on the product as ground if 100% of the calcined gypsum is ground and on a blend of the ground product with the unground portion if less than 100% of the calcined gypsum is ground, mixing said post-ground calcined gypsum with water and a lightweight aggregate, and forming the resultant aqueous slurry into board form between opposed paper face sheets.
Claim 2
Independent Claim
167 words
The method of making gypsum wallboard comprising the steps of removing substantially all of the free moisture from an about 94% to 98% pure gypsum filter cake of about 35 to 80 micron average particle diameter FGD dihydrate gypsum while avoiding any substantial reduction of particle size of said gypsum other than the breaking up of agglomerates of particles, flash calcining said dried FGD gypsum to about 25% of the water of hydration producing FGD hemihydrate gypsum, grinding at least about 25% of said calcined gypsum to produce a Fisher surface area of material of at least about 2500 cm 2 /gm, said surface area being measured on the product as ground if 100% of the calcined gypsum is ground and on a blend of the ground product with the unground portion if less than 100% of the calcined gypsum is ground, mixing said post-ground calcined gypsum with water and a lightweight aggregate, and forming the resultant aqueous slurry into board form between opposed paper face sheets.
Claim 3
Dependent Claim
31 words
The method of claim 1 wherein about 25% to 50% of said calcined gypsum is ground to an increased surface area for mixture with 75% to 50% of unground calcined gypsum.
Claim 4
Dependent Claim
18 words
The method of claim 1 wherein said grinding of calcined gypsum is carried out in an impact mill.
Claim 5
Dependent Claim
14 words
The method of claim 3 wherein said impact mill is a centrifugal impact mill.
Claim 6
Dependent Claim
18 words
The method of claim 4 wherein said centrifugal impact mill is rotated at about 1100 to 2000 rpm.
Claim 7
Dependent Claim
29 words
The method of claim 4 wherein said centrifugal impact mill comprises a plurality of metal pins on a rotor and a plurality of metal pins on a fixed housing.
Claim 8
Dependent Claim
55 words
The method of claim 1 wherein said flash calcining comprises continuously feeding said dried FGD dihydrate gypsum to a peripherally confined cylindrical heating zone by means of a moist heated gas stream moving tangentially into the upper part of said heating zone, whereby said FGD gypsum being calcined is conveyed spirally through said heating zone.
Claim 9
Dependent Claim
42 words
The method of claim 7 wherein said moist heated gas stream is repeatedly replenished by additional heated gas streams entering said heating zone through a plurality of entry orifices arranged substantially tangential to and along said cylindrical periphery of said heating zone.
Claim 10
Dependent Claim
31 words
The method of claim 8 wherein about 25% to 50% of said calcined gypsum is ground to an increased surface area for mixture with 75% to 50% of unground calcined gypsum.
Claim 11
Dependent Claim
18 words
The method of claim 8 wherein said grinding of calcined gypsum is carried out in an impact mill.
Claim 12
Dependent Claim
14 words
The method of claim 10 wherein said impact mill is a centrifugal impact mill.
Claim 13
Dependent Claim
18 words
The method of claim 11 wherein said centrifugal impact mill is rotated at about 1100 to 2000 rpm.
Claim 14
Dependent Claim
19 words
The method of claim 1 wherein said average particle diameter is from about 60 microns to about 70 microns.
Claim 15
Dependent Claim
17 words
The method of claim 1 wherein said filter cake has from about 10% to 15% free water.
Claim 16
Dependent Claim
21 words
The method of claim 1 wherein said free moisture in said FGD dihydrate is removed in a cage mill flash dryer.
Claim 17
Dependent Claim
18 words
The method of claim 15 wherein said FGD dihydrate is continuously fed to said cage mill flash dryer.
Claim 18
Dependent Claim
17 words
The method of claim 1 wherein said formed board is dried in a high temperature drying oven.
Claim 19
Dependent Claim
18 words
The method of claim 17 wherein the dried board has a weight of about 1600 lbs/MSF/1/2 in. thickness.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-03-04 | 1988-09-03 | 1989-03-05 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-03-04 | 1992-09-03 | 1993-03-05 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-03-04 | 1996-09-03 | 1997-03-05 | $7700.00 | Window Closed / Lapsed |