US4493854A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Production of defatted soybean products by supercritical fluid extraction
Assignee: United States Department of Agriculture
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Filing: 1983-09-20
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Granted: 1985-01-15
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Expires: 2003-09-20
Abstract
Abstract The raw grassy and bitter principles in soybeans are reduced to acceptable levels for purposes of human consumption without significant degradation of the nutritional properties. This result is achieved by a lipid extraction process in which raw soybean material is treated with carbon dioxide under carefully controlled supercritical conditions. Of particular importance are the moisture content of the bean material as well as the pressure, temperature, and contact time of the carbon dioxide extractant.
Inventors
- 👤 John P. Friedrich
- 👤 Arthur C. Eldridge
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 08:31
CPC Classifications
A; A23; A23L; A23L11/00; A23L11/30; A23L11/32
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
130 words
A method for preparing a flavorful, defatted soybean protein product from raw soybean material comprising the steps of: a. contacting said soybean material at a moisture content above 6.5% dry weight basis with a carbon dioxide solvent under supercritical conditions such that the characteristic raw grassy flavor is reduced without a substantial reduction in the protein solubility, wherein said conditions include a pressure of at least 690 bar and a temperature of at least 81° C., and thereby extracting the lipids from said soybean material; b. separating the lipid-containing carbon dioxide solvent resulting from step (a) from a substantially lipid-free soybean residue; and c. recovering said residue as a nutritious, organoleptically acceptable product characterized by a substantially reduced raw grassy flavor as compared to that of the raw soybean material.
Claim 2
Independent Claim
130 words
A method for preparing a flavorful, defatted soybean protein product from raw soybean material comprising the steps of: a. contacting said soybean material at a moisture content above 6.5% dry weight basis with a carbon dioxide solvent under supercritical conditions such that the characteristic raw grassy flavor is reduced without a substantial reduction in the protein solubility, wherein said conditions include a pressure of at least 690 bar and a temperature of at least 81° C., and thereby extracting the lipids from said soybean material; b. separating the lipid-containing carbon dioxide solvent resulting from step (a) from a substantially lipid-free soybean residue; and c. recovering said residue as a nutritious, organoleptically acceptable product characterized by a substantially reduced raw grassy flavor as compared to that of the raw soybean material.
Claim 3
Dependent Claim
15 words
The method as described in claim 1 wherein said soybean material is in flaked form.
Claim 4
Dependent Claim
17 words
The method as described in claim 1 and further comprising milling said recovered residue into a flour.
Claim 5
Dependent Claim
17 words
The method as described in claim 1 wherein said moisture content is in the range of 9-12%.
Claim 6
Dependent Claim
17 words
The method as described in claim 4 wherein the pressure is in the range of 793-855 bar.
Claim 7
Dependent Claim
17 words
The method as described in claim 4 wherein the temperature is in the range of 81°-100° C.
Claim 8
Dependent Claim
39 words
The method as described in claim 1 wherein the moisture content is in the range of about 10-12%, the pressure is in the range of about 827-855 bar, and the temperature is in the range of about 81°-84° C.
Claim 9
Dependent Claim
38 words
A method as described in claim 1 wherein the moisture content is not more than about 15%, the pressure is in the range of about 755-860 bar, and the temperature is in the range of about 81°-100° C.
Claim 10
Dependent Claim
29 words
A product produced by the process of claim 1 wherein said product is characterized by a nitrogen solubility index of at least 60 and a lipoxygenase activity near zero
Claim 11
Dependent Claim
29 words
A product produced by the process of claim 3 wherein said product is characterized by a nitrogen solubility index of at least 60 and a lipoxygenase activity near zero.
Claim 12
Dependent Claim
29 words
A product produced by the process of claim 7 wherein said product is characterized by a nitrogen solubility index of at least 60 and a lipoxygenase activity near zero.
Claim 13
Dependent Claim
29 words
A product produced by the process of claim 8 wherein said product is characterized by a nitrogen solubility index of at least 60 and a lipoxygenase activity near zero.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-01-15 | 1988-07-16 | 1989-01-15 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-01-15 | 1992-07-16 | 1993-01-15 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-01-15 | 1996-07-16 | 1997-01-15 | $7700.00 | Window Closed / Lapsed |