Patent US4116053A successfully refreshed from Google Patents.
US4490403A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for producing an agglomerated powdery milk product
Assignee: Niro Holding AS
•
Filing: 1983-06-13
•
Granted: 1984-12-25
•
Expires: 2003-06-13
Abstract
Abstract An agglomerated powdery milk product is prepared by spraying a concentrate of milk or a fraction thereof into a stream of drying gas directed against the surface of a fluidized layer of already spray dried particles in a conical chamber, thereby obtaining a favorable interaction. Special parameters including temperatures, rates of streams of drying air and residence time are adjusted to obtain an extensively agglomerated product, high production capacity, improved heat economy, low heat damage of the product, and to make possible an easy spray drying of materials, which have hitherto been regarded as unsuitable for spray drying.
Inventors
- 👤 Jan Pisecky
- 👤 Jens Krag
- 👤 Ib H. Sorensen
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 08:51
CPC Classifications
A; A23; A23C; A23C1/00; A23C1/04; A23C1/05; B; B01; B01D; B01D1/00; B01D1/16; B01D1/18; Y; Y10; Y10S; Y10S159/00; Y10S159/03
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
328 words
A process for producing an agglomerated powdery milk product, comprising the steps of (a) atomizing a liquid derived from milk, in the upper part of a conical downward tapering drying chamber by means of a nozzle into a central downward stream of drying gas at 200°-400° C. to produce particles, (b) maintaining in the lower part of said drying chamber a layer of particles fluidized in an upward stream of gas having a velocity of 0.3-1.5 m/sec, whereby the temperature of said upward stream of gas is adjusted between 10° and 150° C. to maintain the temperature required of the fluidized particles for ensuring the agglomeration ability of said particles with respect to the particles produced in step (a), and wherein the amount of particles in the fluidized layer is adjusted corresponding to a pressure drop of 1.5-4.5 k Pas over the fluidized layer, (c) adjusting the amount of said liquid to the amount and drying capacity of the downward stream to ensure a moisture content of the particles reaching the fluidized layer between 2-16% and sufficient for agglomerating said particles by forming clusters thereof, but less than the moisture content which would cause formation of monogranules, and also to ensure that the downward gas stream still has a substantial drying capacity upon reaching the fluidized layer and sufficient kinetic energy for penetrating therein, thereby contributing to the drying process in the fluidized layer and promoting removal of particles and small agglomerates from the fluidized layer to the upper part of the drying chamber for agglomerate-forming contact with wet droplets and moist particles, (d) withdrawing a stream comprising the gas from said downward stream and the gas from said upward stream at a non-central location in the upper part of the drying chamber, (e) adjusting the amount of drying gas introduced as a central downward stream to be 2-4 times the amount of the upward stream of fluidizing gas, and (f) recovering agglomerated particles from said fluidized layer.
Claim 2
Dependent Claim
328 words
A process for producing an agglomerated powdery milk product, comprising the steps of (a) atomizing a liquid derived from milk, in the upper part of a conical downward tapering drying chamber by means of a nozzle into a central downward stream of drying gas at 200°-400° C. to produce particles, (b) maintaining in the lower part of said drying chamber a layer of particles fluidized in an upward stream of gas having a velocity of 0.3-1.5 m/sec, whereby the temperature of said upward stream of gas is adjusted between 10° and 150° C. to maintain the temperature required of the fluidized particles for ensuring the agglomeration ability of said particles with respect to the particles produced in step (a), and wherein the amount of particles in the fluidized layer is adjusted corresponding to a pressure drop of 1.5-4.5 k Pas over the fluidized layer, (c) adjusting the amount of said liquid to the amount and drying capacity of the downward stream to ensure a moisture content of the particles reaching the fluidized layer between 2-16% and sufficient for agglomerating said particles by forming clusters thereof, but less than the moisture content which would cause formation of monogranules, and also to ensure that the downward gas stream still has a substantial drying capacity upon reaching the fluidized layer and sufficient kinetic energy for penetrating therein, thereby contributing to the drying process in the fluidized layer and promoting removal of particles and small agglomerates from the fluidized layer to the upper part of the drying chamber for agglomerate-forming contact with wet droplets and moist particles, (d) withdrawing a stream comprising the gas from said downward stream and the gas from said upward stream at a non-central location in the upper part of the drying chamber, (e) adjusting the amount of drying gas introduced as a central downward stream to be 2-4 times the amount of the upward stream of fluidizing gas, and (f) recovering agglomerated particles from said fluidized layer.
Claim 3
Dependent Claim
34 words
The process of claim 1, wherein the ratio between the kinetic energy of the downward stream of gas and the kinetic energy of the upward stream of gas is in the range of 1000-15000.
Claim 4
Dependent Claim
22 words
The process of claim 1, wherein the mean residence time of the particles in the fluidized layer is at least 5 minutes.
Claim 5
Dependent Claim
20 words
The process of claim 1, wherein the agglomerated particles recovered in step (f) are further dried outside said drying chamber.
Claim 6
Dependent Claim
161 words
The process of claim 1 for producing agglomerated skim milk powder comprising (a) atomizing a skim milk concentrate of 45-52% by weight dry solids into a stream of air at 230°-350° C. having a downward velocity of 20-40 m/sec, whereby the amount of said concentrate is adjusted to produce particles of skim milk powder, which upon reaching the surface of said fluidized layer have a moisture content of 10-15%, (b) maintaining said layer of fluidized particles at a temperature of 60°-80° C. by introducing drying air at 70°-150° C. having an upward velocity of 0.3-1.5 m/sec in the lower part of said layer, (c) withdrawing from the upper part of the drying chamber a stream of air entraining fine particles of skim milk powder, (d) collecting said fine entrained particles, (e) recycling the collected fine particles to said fluidized layer in the drying chamber, (f) recovering agglomerated skim milk powder particles having a moisture content of 3.0-9% from the fluidized layer.
Claim 7
Dependent Claim
27 words
The process of claim 5, wherein the skim milk powder particles recovered in step (f) are dried outside the drying chamber to a moisture content of 2-5%.
Claim 8
Dependent Claim
161 words
The process of claim 1 for producing agglomerated whole milk powder comprising (a) atomizing a whole milk concentrate of 45-52% by weight dry solids into a stream of air at 200°-300° C. having a downward velocity of 20-40 m/sec, whereby the amount of said concentrate is adjusted to produce particles of whole milk powder, which upon reaching the surface of said fluidized layer have a moisture content of 8-16%, (b) maintaining said layer of fluidized particles at a temperature of 60°-80° C. by introducing drying air at 70°-150° C. having an upward velocity of 0.3-1.5 m/sec in the lower part of said layer, (c) withdrawing from the upper part of the drying chamber a stream of air entraining fine particles of whole milk powder, (d) collecting said fine entrained particles, (e) recycling the collected fine particles to said fluidized layer in the drying chamber, (f) recovering agglomerated whole milk powder particles having a moisture content of 4.5-9% from the fluidized layer.
Claim 9
Dependent Claim
27 words
The process of claim 7, wherein the particles recovered in step (f) are further dried and cooled outside the drying chamber to a moisture content of 2-4%.
Claim 10
Dependent Claim
165 words
The process of claim 1 for producing agglomerated whey powder comprising (a) atomizing a whey concentrate of 48-58% by weight dry solids into a stream of air at 230°-350° C. having a downward velocity of 20-40 m/sec, whereby the amount of said concentrate is adjusted to produce particles of whey powder, which upon reaching the surface of said fluidized layer have a moisture content of 2-6%, (b) maintaining said layer of fluidized particles at a temperature of 70°-90° C. by introducing drying air at 10°-80° C. having an upward velocity of 0.3-1.5 m/sec in the lower part of said layer, (c) withdrawing from the upper part of the drying chamber a stream of air entraining fine particles of whey powder, (d) collecting said fine entrained particles, (e) recycling the collected fine particles to said fluidized layer in the drying chamber, (f) recovering agglomerated whey powder particles from the fluidized layer, which particles have an average particle size of 200-700μ and a moisture content of 1-5%.
Claim 11
Dependent Claim
25 words
The process of claim 1, wherein the upward stream of gas in the lower part of said drying chamber has a velocity of 0.6-1.5 m/sec.
Claim 12
Dependent Claim
15 words
The process of claim 4, wherein the agglomerated particles are cooled outside said drying chamber.
Claim 13
Dependent Claim
27 words
The process of claim 4, in which the agglomerated particles from step (f) are further dried and cooled outside said drying chamber in a vibrated fuidized bed.
Claim 14
Dependent Claim
26 words
The process of claim 6, wherein the skim milk powder particles recovered in step (f) are dried outside the drying chamber in a vibrated fluidized bed.
Claim 15
Dependent Claim
25 words
The process of claim 8, wherein the particles recovered in step (f) are dried and cooled outside the drying chamber in a vibrated fluidized bed.
Claim 16
Dependent Claim
11 words
The process of claim 9, wherein the whey concentrate is precrystallized.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-12-25 | 1988-06-25 | 1988-12-25 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-12-25 | 1992-06-25 | 1992-12-25 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-12-25 | 1996-06-25 | 1996-12-25 | $7700.00 | Window Closed / Lapsed |