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US4482386A Expired / Lapsed US ⏱️ 0.0 years remaining

Method of conditioning a water swellable hydrocolloid

Assignee: Warner Lambert Co LLC
•
Filing: 1983-04-29
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Granted: 1984-11-13
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Expires: 2003-04-29
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Abstract

Abstract Method to condition water-swellable hydrocolloids for use in mechanical forming processes such as die molding or injection molding. To avoid long conditioning times at high temperature, the hydrocolloids are conditioned to the predetermined water content at ambient temperature and then rapidly heated, just before processing, in a gaseous stream loaded with water to the equilibrium conditions needed to maintain the predetermined water content of the hydrocolloids at the high process temperature of the mechanical forming.

Inventors

  • 👤 Fritz Wittwer
  • 👤 Ivan Tomka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 03:14
CPC Classifications
C; C08; C08J; C08J3/00; C08J2300/00; C08J2300/10

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 137 words
A method by which a water-swellable hydrocolloid, for use in mechanical forming processes is conditioned to a given water content and is rapidly heated from a lower temperature to a higher temperature without virtually changing its water content, characterized by (a) slowly conditioning the hydrocolloid at the lower temperature to obtain an even distribution of water within every particle and through the bulk of the hydrocolloid, (b) transferring the hydrocolloid into a gaseous atmosphere of the desired higher temperature, said gaseous atmosphere is loaded with water to the proportion in equilibrium at the higher temperature with the predetermined water content of the hydrocolloid, and (c) removing the hydrocolloid from the said gaseous atmosphere within a short time sufficient to heat the hydrocolloid to the desired higher temperature but not sufficient to affect any substantial exchange of humidity.
Claim 2
Independent Claim 137 words
A method by which a water-swellable hydrocolloid, for use in mechanical forming processes is conditioned to a given water content and is rapidly heated from a lower temperature to a higher temperature without virtually changing its water content, characterized by (a) slowly conditioning the hydrocolloid at the lower temperature to obtain an even distribution of water within every particle and through the bulk of the hydrocolloid, (b) transferring the hydrocolloid into a gaseous atmosphere of the desired higher temperature, said gaseous atmosphere is loaded with water to the proportion in equilibrium at the higher temperature with the predetermined water content of the hydrocolloid, and (c) removing the hydrocolloid from the said gaseous atmosphere within a short time sufficient to heat the hydrocolloid to the desired higher temperature but not sufficient to affect any substantial exchange of humidity.
Claim 3
Dependent Claim 24 words
The method of claim 1 wherein the lower temperature is normal ambient temperature and the higher temperature is near the boiling point of water.
Claim 4
Dependent Claim 39 words
The method of claims 1 or 2, wherein the hydrocolloid has a glass-transition point above the lower temperature and below the higher temperature as defined in claim 1 and is able to be plastically deformed at the higher temperature.
Claim 5
Independent Claim 14 words
The method of claims 1 or 2, wherein the hydrocolloid is a plastifiable protein.
Claim 6
Independent Claim 14 words
The method as in any claims 1, 2, 4 or 6 wherein the plastifiable
Claim 7
Dependent Claim 22 words
The method of claim 5, wherein the gelatin is in granulated form with a mean particle size between 0,2 and 4 mm.
Claim 8
Independent Claim 60 words
The method of claims 1 to 6, wherein the gaseous atmosphere loaded with water is a gas stream preferably an air stream, of constant velocity, into which the hydrocolloid is fed at a constant rate at a first point, carried away with the gas stream, and removed from the gas stream at a second point after a predetermined elapsed time.
Claim 9
Dependent Claim 13 words
The method of claim 7 wherein the gas stream is an air stream.
Claim 10
Dependent Claim 20 words
The water-swellable hydrocolloid produced by the method of claim 1 for the feeding of die molding or injection molding machines.
Claim 11
Independent Claim 28 words
The method of claims 1 or 2 wherein the hydrocolloid is a natural hydrophilic polymer selected from a group consisting of casein, soya bean protein, or safflower protein.
Claim 12
Independent Claim 27 words
The method of claims 1 or 2 wherein the hydrocolloid is a modified natural hydrophilic polymer selected from a group consisting of phthalated gelatin and succinated gelatin.
Claim 13
Independent Claim 39 words
The method of claims 1 or 2 wherein the hudrocolloid is a synthetic hydrophilic polymer selected from a group consisting of cellulosephthalate-acetate, polyvinylacetate, polyvinylacetate-phthalate, and polymerisates of acrylic or methacrylic esters modified by hydrophilic groups to render them water-swellable.

References Cited (Backward Citations)

US1892599A Cited
US2051779A Cited
US3137592A Cited
US4256771A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-11-13 1988-05-14 1988-11-13 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-11-13 1992-05-14 1992-11-13 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-11-13 1996-05-14 1996-11-13 $7700.00 Window Closed / Lapsed

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