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US4477264A Expired / Lapsed US ⏱️ 0.0 years remaining

Pressure swing adsorption process for a medical oxygen generator for home use

Assignee: Air Products and Chemicals Inc
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Filing: 1983-03-30
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Granted: 1984-10-16
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Expires: 2003-03-30
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Abstract

Abstract A simplified low-cost system designed for home use in the direct administration of high purity oxygen to a patient, utilizes a single adsorption column containing successive layers of adsorbent. The first layer is composed of a molecular sieve adsorbent for removal of water and CO2 from the air feed stream. The second layer is a molecular sieve adsorbent which preferentially retains nitrogen. The sequence and conditions of the several steps of the operating cycle are designed to recover a therapeutic gas stream of about 90% oxygen content.

Inventors

  • 👤 Wilbur C. Kratz
  • 👤 Shivaji Sircar

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 03:47
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/02; B01D53/04; B01D53/047; A; A61; A61L; A61L9/00; A61L9/01; C; C01; C01B; C01B13/00; C01B13/02; C01B13/0229; C01B13/0248; C01B13/0259; B01D2253/00; B01D2253/10; B01D2253/106; B01D2253/11; B01D2256/00; B01D2256/12; B01D2257/00; B01D2257/10; B01D2257/102; B01D2257/50; B01D2257/504; B01D2257/80; B01D2259/00; B01D2259/40; B01D2259/40011; B01D2259/40058; B01D2259/4006; B01D2259/40064; B01D2259/40077; B01D2259/40079; B01D2259/40081; B01D2259/401; B01D2259/41; B01D2259/414; B01D2259/4141; B01D2259/4145; B01D2259/4146; B01D2259/45; B01D2259/4533; B01D2259/455; B01D53/0407; B01D53/0423; B01D53/053; C01B2210/00; C01B2210/0043; C01B2210/0046; C01B2210/0051; C01B2210/0062; Y; Y02; Y02C; Y02C20/00; Y02C20/40; Y02P; Y02P20/00; Y02P20/151

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 294 words
In the generation and recovery of high purity oxygen from an ambient air stream in a system employing a single adsorption column, the method which comprises the successive steps of: (a) introducing pressurized air into the column containing an adsorbent bed, said bed comprising in the direction of air flow thereinto a first shallow layer of an adsorbent effective in removal of water and CO 2 followed by a predominant second layer of an adsorbent selective in sorbing nitrogen from admixture with oxygen; said bed having been brought to adsorption pressure prior to said initial air introduction with a previously obtained product stream of high oxygen concentration to bring the same form subatmospheric to slightly above atmosphere pressure; (b) continuing said introduction of pressurized air into said bed without withdrawal of product therefrom until said bed is brought to a maximum pressure of several atmospheres; (c) then discontinuing said introduction of pressurized air and withdrawing from said bed, in the same direction as that in which the feed air was introduced, a part of the gas product contained therein and collecting said withdrawn part in a storage reservoir; (d) thereafter venting the bed to the atmosphere in a direction counter to air feed direction, thereby removing a portion of the contained nitrogen from said second adsorbent layer and part of the contained water and CO 2 from said first adsorbent layer; (e) next evacuating the bed in the same direction as in the preceding venting step (d) to remove remaining nitrogen, water and CO 2 from the respective adsorbent layer; followed by, (f) restoring the bed to slightly above atmospheric pressure for repetition of the defined sequence by introducing therein a portion of the product gas of high oxygen concentration from said storage reservoir.
Claim 2
Dependent Claim 294 words
In the generation and recovery of high purity oxygen from an ambient air stream in a system employing a single adsorption column, the method which comprises the successive steps of: (a) introducing pressurized air into the column containing an adsorbent bed, said bed comprising in the direction of air flow thereinto a first shallow layer of an adsorbent effective in removal of water and CO 2 followed by a predominant second layer of an adsorbent selective in sorbing nitrogen from admixture with oxygen; said bed having been brought to adsorption pressure prior to said initial air introduction with a previously obtained product stream of high oxygen concentration to bring the same form subatmospheric to slightly above atmosphere pressure; (b) continuing said introduction of pressurized air into said bed without withdrawal of product therefrom until said bed is brought to a maximum pressure of several atmospheres; (c) then discontinuing said introduction of pressurized air and withdrawing from said bed, in the same direction as that in which the feed air was introduced, a part of the gas product contained therein and collecting said withdrawn part in a storage reservoir; (d) thereafter venting the bed to the atmosphere in a direction counter to air feed direction, thereby removing a portion of the contained nitrogen from said second adsorbent layer and part of the contained water and CO 2 from said first adsorbent layer; (e) next evacuating the bed in the same direction as in the preceding venting step (d) to remove remaining nitrogen, water and CO 2 from the respective adsorbent layer; followed by, (f) restoring the bed to slightly above atmospheric pressure for repetition of the defined sequence by introducing therein a portion of the product gas of high oxygen concentration from said storage reservoir.
Claim 3
Dependent Claim 35 words
The method as defined in claim 1 wherein said evacuation in step (e) is carried out for a time to bring said bed to a pressure in the range of about 100 to 300 torr.
Claim 4
Dependent Claim 35 words
The method as definded in claim 1 wherein step (f) is carried out under conditions to repressure the evacuated bed from step (e) to superatmospheric pressure in the range of up to about 6 psig.
Claim 5
Dependent Claim 29 words
The method as defined in claim 1 wherein step (c) is continued to the point at which the pressures in the bed and in the storage reservoir are equalized.
Claim 6
Dependent Claim 20 words
The method as defined in claim 1 wherein the adsorbent in said second layer consists essentially of pelleted sodium mordenite.
Claim 7
Dependent Claim 22 words
The method as defined in claim 1 wherein said product gas recovered in step (c) has an oxygen concentration of about 90%.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-10-16 1988-04-16 1988-10-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-10-16 1992-04-16 1992-10-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-10-16 1996-04-16 1996-10-16 $7700.00 Window Closed / Lapsed

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