← Back to Patent Explorer
US4472265A Expired / Lapsed US ⏱️ 0.0 years remaining

Dormant mesophase pitch

Assignee: Fuji Standard Research Inc
•
Filing: 1981-12-10
•
Granted: 1984-09-18
•
Expires: 2001-12-10
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A novel carbonaceous pitch which is optically isotropic in nature and which turns into optically anisotropic when shear forces are applied thereto. The carbonaceous pitch may be obtained by hydrogenating the mesophase of a mesophase pitch to the extent that the mesophase is rendered soluble in quinoline. The carbonaceous pitch is useful as a binder and an impregnator and as a precursor material for a highly oriented, high-strength and high-modulus carbon fiber, needle coke or the like carbonaceous materials.

Inventors

  • 👤 Sugio Otani

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 18:21
CPC Classifications
C; C10; C10C; C10C3/00; D; D01; D01F; D01F9/00; D01F9/08; D01F9/12; D01F9/14; D01F9/145

Claims Analysis

Total Claims: 22
Claim 1
Independent Claim 60 words
A carbonaceous pitch comprising dormant anisotropic components which are partially hydrogenated, polycyclic polycondensed ring aromatic hydrocarbons derived from the mesophase of a mesophase pitch by hydrogenation of said mesophase and which are soluble in quinoline, said carbonaceous pitch being optically isotropic in nature but, upon being subjected to shear forces in one direction, capable of being oriented in said direction.
Claim 2
Dependent Claim 60 words
A carbonaceous pitch comprising dormant anisotropic components which are partially hydrogenated, polycyclic polycondensed ring aromatic hydrocarbons derived from the mesophase of a mesophase pitch by hydrogenation of said mesophase and which are soluble in quinoline, said carbonaceous pitch being optically isotropic in nature but, upon being subjected to shear forces in one direction, capable of being oriented in said direction.
Claim 3
Dependent Claim 18 words
A carbonaceous pitch as claimed in claim 1, and having a H/C atomic ratio of 0.55 to 1.2.
Claim 4
Dependent Claim 22 words
A carbonaceous pitch as claimed in claim 1, wherein said mesophase pitch has a mesophase content of 1 to 90 wt %.
Claim 5
Dependent Claim 22 words
A carbonaceous pitch as claimed in claim 1, wherein said mesophase pitch has a mesophase content of 5 to 70 wt %.
Claim 6
Dependent Claim 19 words
A carbonaceous pitch as claimed in claim 1, and being a homogeneous liquid when heated above its melting point.
Claim 7
Dependent Claim 19 words
A carbonaceous pitch as claimed in claim 1, and having a melting point of about 150° to 300° C.
Claim 8
Dependent Claim 23 words
A carbonaceous pitch as claimed in claim 1, and exhibiting a viscosity of about 100 poises when heated to 200° to 300° C.
Claim 9
Dependent Claim 54 words
A process for the preparation of a carbonaceous pitch which is optically isotropic in nature but is capable of being oriented in one direction when subjected to shear forces in said direction, comprising providing a mesophase pitch, and hydrogenating the mesophase of said mesophase pitch so that the mesophase is rendered soluble in quinoline.
Claim 10
Dependent Claim 54 words
A process for the preparation of a carbonaceous pitch which is optically isotropic in nature but is capable of being oriented in one direction when subjected to shear forces in said direction, comprising providing a mesophase pitch, and hydrogenating the mesophase of said mesophase pitch so that the mesophase is rendered soluble in quinoline.
Claim 11
Dependent Claim 31 words
A process as claimed in claim 8, wherein said hydrogenation comprises subjecting said mesophase pitch to hydrogenating conditions, so that substantially all the mesophase contained therein is rendered soluble in quinoline.
Claim 12
Dependent Claim 20 words
A process as claimed in claim 8, wherein said mesophase pitch has a H/C atomic ratio of 0.43 to 0.75.
Claim 13
Dependent Claim 20 words
A process as claimed in claim 10, wherein said mesophase pitch has a H/C atomic ratio of 0.45 to 0.65.
Claim 14
Dependent Claim 32 words
A process as claimed in claim 8, wherein the product of said hydrogenation is heated above its melting point for a period of time sufficient to remove low boiling point components therefrom.
Claim 15
Dependent Claim 24 words
A process as claimed in claim 12, wherein the product of said hydrogenation is heated to a temperature of about 450° C. or less.
Claim 16
Dependent Claim 24 words
A process as claimed in claim 13, wherein the product of said hydrogenation is heated to a temperature of about 280° to 430° C.
Claim 17
Dependent Claim 21 words
A process as claimed in claim 8, wherein said mesophase pitch has a mesophase component of 1 to 90 wt %.
Claim 18
Dependent Claim 21 words
A process as claimed in claim 8, wherein said mesophase pitch has a mesophase component of 5 to 70 wt %.
Claim 19
Dependent Claim 116 words
A process for the production of a carbon fiber comprising the steps of: providing a carbonaceous pitch comprising dormant anisotropic components which are partially hydrogenated, polycyclic polycondensed ring aromatic hydrocarbons derived from the mesophase of a mesophase pitch by hydrogenation of said mesophase and which are soluble in quinoline, said carbonaceous pitch being optically isotropic in nature but, upon being subjected to shear forces in one direction, capable of being oriented in said direction; heating said carbonaceous pitch above its melting point; spinning a carbonaceous fiber from said molten pitch; exposing said spun fiber to an oxygen-containing atmosphere so that said spun fiber is rendered infusible; and heat-treating said infusible fiber at temperatures above 800° C.
Claim 20
Dependent Claim 116 words
A process for the production of a carbon fiber comprising the steps of: providing a carbonaceous pitch comprising dormant anisotropic components which are partially hydrogenated, polycyclic polycondensed ring aromatic hydrocarbons derived from the mesophase of a mesophase pitch by hydrogenation of said mesophase and which are soluble in quinoline, said carbonaceous pitch being optically isotropic in nature but, upon being subjected to shear forces in one direction, capable of being oriented in said direction; heating said carbonaceous pitch above its melting point; spinning a carbonaceous fiber from said molten pitch; exposing said spun fiber to an oxygen-containing atmosphere so that said spun fiber is rendered infusible; and heat-treating said infusible fiber at temperatures above 800° C.
Claim 21
Dependent Claim 44 words
A carbonaceous pitch obtained by hydrogenating the mesophase of a mesophase pitch to render said mesophase soluble in quinoline, said carbonaceous pitch being optically isotropic in nature but being capable of being oriented in one direction when subjected to shear forces in said direction.
Claim 22
Dependent Claim 44 words
A carbonaceous pitch obtained by hydrogenating the mesophase of a mesophase pitch to render said mesophase soluble in quinoline, said carbonaceous pitch being optically isotropic in nature but being capable of being oriented in one direction when subjected to shear forces in said direction.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-09-18 1988-03-19 1988-09-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-09-18 1992-03-19 1992-09-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-09-18 1996-03-19 1996-09-18 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag