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US4469802A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing sintered body of boron nitride

Assignee: National Institute for Materials Science
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Filing: 1982-12-17
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Granted: 1984-09-04
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Expires: 2002-12-17
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Abstract

Abstract A process for producing a sintered body of cubic system boron nitride comprises steps of: (a) mixing raw material boron nitride selected from the group consisting of hexagonal system boron nitride, cubic system boron nitride, and a mixture thereof with Me 3 B 2 N 4 (where: Me represents an alkaline earth metal) in an amount of from 0.15 to 3.0 mol %; and (b) treating said mixed material at a temperature of 1350° C. and above under a thermodynamically stabilized pressure condition of the cubic system boron nitride.

Inventors

  • 👤 Tadashi Endo
  • 👤 Osamu Fukunaga
  • 👤 Tadao Sato

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 03:45
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/58; C04B35/583; C04B35/5831

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 90 words
A process for producing a sintered body of cubic system boron nitride which comprises steps of: (a) mixing raw material boron nitride selected from the group consisting of hexagonal system boron nitride, cubic system boron nitride, and a mixture thereof with Me 3 B 2 N 4 (where: Me represents an alkaline earth metal) in an amount of from 0.15 to 3.0 mol %; and (b) treating said mixed material at a temperature of 1350° C. and above under a thermodynamically stabilized pressure condition of the cubic system boron nitride.
Claim 2
Dependent Claim 90 words
A process for producing a sintered body of cubic system boron nitride which comprises steps of: (a) mixing raw material boron nitride selected from the group consisting of hexagonal system boron nitride, cubic system boron nitride, and a mixture thereof with Me 3 B 2 N 4 (where: Me represents an alkaline earth metal) in an amount of from 0.15 to 3.0 mol %; and (b) treating said mixed material at a temperature of 1350° C. and above under a thermodynamically stabilized pressure condition of the cubic system boron nitride.
Claim 3
Dependent Claim 34 words
The process according to claim 1, further comprising of treating the surface of the cubic system boron nitride to reversely transform the same into hexagonal system boron nitride at least in one part thereof.
Claim 4
Dependent Claim 27 words
The process according to claim 1, wherein said mixing ratio of Me 3 B 2 N 4 and boron nitride ranges from 0.15 to 1.8 mol %.
Claim 5
Dependent Claim 44 words
The process according to claim 1, wherein said Me 3 B 2 N 4 is one selected from the group consisting of Mg 3 B 2 N 4 , Ca 3 B 2 N 4 , and Sr 3 B 2 N 4 .

References Cited (Backward Citations)

JPS4940124B1 Cited
US3811899A Cited
US4188194A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-09-04 1988-03-05 1988-09-04 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-09-04 1992-03-05 1992-09-04 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-09-04 1996-03-05 1996-09-04 $7700.00 Window Closed / Lapsed

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