US4457892A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Biocidal gas sterilization and gas leakage determination
Assignee: American Sterilizer Co
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Filing: 1979-02-06
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Granted: 1984-07-03
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Expires: 1999-02-06
Abstract
Abstract Methods and apparatus for the timely determination of potentially harmful biocidal gas leakage from a pressurized chamber during sterilizing operations are disclosed. Biocidal gas make-up values are monitored during the sterilizing phase to provide prompt warning of biocidal gas leakage. In one embodiment, the timing of preselected pressure increment gas make-up charges are measured and compared to minimum acceptable gas make-up charge times. In addition, absorption of biocidal gas by the load can be compensated for in sterilizing operations where load absorption is a significant factor. Also, provision is made for predicting gas absorption by the load from steam absorption data obtained during pressure-controlled conditioning cycles.
Inventors
- 👤 Jack H. Young
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 16:20
CPC Classifications
A; A61; A61L; A61L2/00; A61L2/24; A61L2/16; A61L2/20; A61L2/206
Claims Analysis
Total Claims: 10
Claim 1
Independent Claim
136 words
Gas sterilization process utilizing a chemically biocidal gas and providing leakage determination of such biocidal gas from a sterilizing chamber comprising, after loading the sterilizing chamber with goods to be sterilized and sealing such chamber for operation at pressures other than atmospheric, the steps of charging chemically biocidal gas into the sterilizing chamber, establishing a desired concentration of such biocidal gas within the sterilizing chamber, providing a sterilization phase at a pressure above atmospheric to complete desired sterilization including make-up charging of the chemically biocidal gas as required to maintain such biocidal gas concentration for an extended time period, determining unacceptable leakage of the chemically biocidal gas from the chamber by quantitatively monitoring such make-up charging of the chemically biocidal gas, and interrupting charging of chemically biocidal gas in response to such determination of unacceptable leakage.
Claim 2
Dependent Claim
136 words
Gas sterilization process utilizing a chemically biocidal gas and providing leakage determination of such biocidal gas from a sterilizing chamber comprising, after loading the sterilizing chamber with goods to be sterilized and sealing such chamber for operation at pressures other than atmospheric, the steps of charging chemically biocidal gas into the sterilizing chamber, establishing a desired concentration of such biocidal gas within the sterilizing chamber, providing a sterilization phase at a pressure above atmospheric to complete desired sterilization including make-up charging of the chemically biocidal gas as required to maintain such biocidal gas concentration for an extended time period, determining unacceptable leakage of the chemically biocidal gas from the chamber by quantitatively monitoring such make-up charging of the chemically biocidal gas, and interrupting charging of chemically biocidal gas in response to such determination of unacceptable leakage.
Claim 3
Dependent Claim
54 words
The process of claim 1 in which maintaining biocidal gas concentration within the chamber includes sensing chamber pressure after establishing a desired pressure level above atmospheric pressure for the chemically biocidal gas in the chamber, and charging such biocidal gas under pressure when chamber pressure falls a predetermined increment below such established pressure level.
Claim 4
Dependent Claim
41 words
The process of claim 2 in which quantitatively monitoring make-up charging of the chemically biocidal gas comprises measuring time lapse between establishing such desired biocidal gas chamber pressure level and a predetermined pressure increment make-up charge of the chemically biocidal gas.
Claim 5
Dependent Claim
35 words
The process of claim 3 in which make-up charging of such biocidal gas is terminated when such time lapse falls below a predetermined value thereby indicating unacceptable leakage of such biocidal gas from said chamber.
Claim 6
Dependent Claim
49 words
The process of claim 1 in which quantitatively monitoring make-up charging of such biocidal gas comprises measuring decrease in concentration of the chemically biocidal gas in the chamber as an indication of unacceptable leakage of such biocidal gas from said chamber, and comparing such measurement with a predetermined standard.
Claim 7
Dependent Claim
42 words
The process of claims 1, 2, 3, or 5 further including the step of interrupting such sterilizing phase and exhausting the chemically biocidal gas from the chamber responsive to such determination which indicates unacceptable leakage of such biocidal gas from said chamber.
Claim 8
Dependent Claim
42 words
The process of claims 1, 2, 3, 4, or 5 in which such step of determining such unacceptable biocidal gas leakage from the sterilizing chamber further includes compensating for load absorption of the chemically biocidal gas by the goods to be sterilized.
Claim 9
Dependent Claim
92 words
The process of claims 2 or 3 further including the steps of compensating for load absorption of the chemically biocidal gas by providing a first make-up charge of such biocidal gas after establishing a desired biocidal gas pressure level in the sterilizing chamber, sugh first make-up charge providing for absorption of such biocidal gas by the goods to be sterilized, and measuring the interim between completion of such first make-up charge of such biocidal gas and a subsequent incremental decrease in sterilizing chamber pressure calling for make-up charging of such biocidal gas.
Claim 10
Dependent Claim
43 words
The process of claim 7 further including the steps of conditioning the goods to be sterilized by introducing a conditioning vapor into the chamber to heat and moisturize the goods, and evaluating load absorption characteristics during conditioning of the goods to be sterilized.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-07-03 | 1988-01-02 | 1988-07-03 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-07-03 | 1992-01-02 | 1992-07-03 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-07-03 | 1996-01-02 | 1996-07-03 | $7700.00 | Window Closed / Lapsed |