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US4454064A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for preparing pentaerythritol phosphate

Assignee: Borg Warner Corp
•
Filing: 1982-10-29
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Granted: 1984-06-12
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Expires: 2002-10-29
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Abstract

Abstract A process involving the reaction of pentaerythritol with phosphorus oxychloride. A solvent is used in the process, but not catalyst or amine (as a hydrogen chloride acceptor) is required.

Inventors

  • 👤 Yuval Halpern
  • 👤 Ron H. Niswander

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 19:50
CPC Classifications
C; C07; C07F; C07F9/00; C07F9/02; C07F9/547; C07F9/6564; C07F9/6571; C07F9/6574; C07F9/65748

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 46 words
A process for the preparation of pentaerythritol phosphate comprising mixing approximately equimolar amounts of pentaerythritol and phosphorous oxychloride, in dioxane as a solvent, heating the mixture at a temperature within the range of from about 75° C. to about 125° C., and isolating said pentaerythritol phosphate.
Claim 2
Dependent Claim 46 words
A process for the preparation of pentaerythritol phosphate comprising mixing approximately equimolar amounts of pentaerythritol and phosphorous oxychloride, in dioxane as a solvent, heating the mixture at a temperature within the range of from about 75° C. to about 125° C., and isolating said pentaerythritol phosphate.
Claim 3
Dependent Claim 19 words
The process of claim 1 wherein the phosphorous oxychloride is added portionwise to the pentaerythritol at the reaction temperature.
Claim 4
Dependent Claim 13 words
The process of claim 1 wherein the pentaerythritol phosphate is isolated by filtration.
Claim 5
Dependent Claim 21 words
The process of claim 3 wherein the filtrate from the isolation step of a prior process is used as the solvent.

References Cited (Backward Citations)

US3293327A Cited
US3155703A Cited
US3189633A Cited
US3143662A Cited
US3168548A Cited
US3287448A Cited
US3342903A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-06-12 1987-12-12 1988-06-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-06-12 1991-12-12 1992-06-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-06-12 1995-12-12 1996-06-12 $7700.00 Window Closed / Lapsed

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