US4453981A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Direct preparation of slurries for ceramic board
Assignee: Corning Glass Works
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Filing: 1983-03-02
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Granted: 1984-06-12
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Expires: 2003-03-02
Abstract
Abstract There is disclosed a method of producing a slurry composed of ion-exchanged, synthetic mica crystals dispersed in a polar liquid. The method comprises providing a synthetic, lithium and/or sodium, water-swelling body of selected crystal type, and dispersing the mica body in the polar liquid while simultaneously effecting an exchange of larger cations from a contacting source with lithium and/or sodium ions from the mica crystals. The synthetic mica body may be vigorously mixed in a dilute solution of the exchangeable ion source. Alternatively, the mica body may be disintegrated in a mixer, the exchangeable ion source added to form a paste and more liquid added to dilute the paste.
Inventors
- 👤 Mark P. Taylor
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 07:17
CPC Classifications
C; C01; C01B; C01B3/00; C01B3/02; C01B3/32; C01B3/34; C01B3/38; C01B3/42; Y; Y10; Y10S; Y10S106/00; Y10S106/03
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
135 words
A method of producing a slurry composed of ion-exchanged, synthetic mica crystals dispersed in a polar liquid which comprises providing a synthetic, lithium and/or sodium, water-swelling mica body that is fully or predominantly cryastalline, the crystals being selected from the group of fluorhectorite, hydroxyl hectorite, boron fluorphlogopite, hydroxyl boron phlogopite, and solid solutions among those and between those and other structurally-compatible species selected from the group of talc, fluortalc, polylithionite, fluorpolylithionite, phlogopite, and fluorphlogopite, and high shear mixing the mica body in a polar liquid containing a contacting source of larger exchangeable cations to simultaneously disintegrate the mica and effect an exchange of larger cations from the contacting source with lithium and/or sodium ions from the mica crystals, said slurry consisting of very thin individual flakes aggregated together in a patchwork to form larger flocs.
Claim 2
Independent Claim
135 words
A method of producing a slurry composed of ion-exchanged, synthetic mica crystals dispersed in a polar liquid which comprises providing a synthetic, lithium and/or sodium, water-swelling mica body that is fully or predominantly cryastalline, the crystals being selected from the group of fluorhectorite, hydroxyl hectorite, boron fluorphlogopite, hydroxyl boron phlogopite, and solid solutions among those and between those and other structurally-compatible species selected from the group of talc, fluortalc, polylithionite, fluorpolylithionite, phlogopite, and fluorphlogopite, and high shear mixing the mica body in a polar liquid containing a contacting source of larger exchangeable cations to simultaneously disintegrate the mica and effect an exchange of larger cations from the contacting source with lithium and/or sodium ions from the mica crystals, said slurry consisting of very thin individual flakes aggregated together in a patchwork to form larger flocs.
Claim 3
Dependent Claim
15 words
A method in accordance with claim 1 wherein the synthetic mica is a lithium fluorhectorite.
Claim 4
Dependent Claim
17 words
A method in accordance with claim 1 wherein the source of exchangeable cations is a potassium salt.
Claim 5
Dependent Claim
34 words
A method in accordance with claim 1 wherein the polar liquid contains a predetermined amount of exchangeable cation sufficient to exchange with the lithium and/or sodium of the mica and to control ionic strength.
Claim 6
Dependent Claim
48 words
A method in accordance with claim 1 wherein the mica body is milled with a liquid in a mixer, the source of exchangeable cations is added to the mixer to form a paste, and further liquid is added to provide a desired level of solids in the slurry.
Claim 7
Dependent Claim
43 words
A method in accordance with claim 1 wherein the mica is a lithium and/or sodium fluorhectorite, the source of large cation is potassium chloride, and the latter is employed in an amount on the order of 200 millimoles per hundred grams of hectorite.
References Cited (Backward Citations)
US4239519A
Cited
US4339540A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-06-12 | 1987-12-12 | 1988-06-12 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-06-12 | 1991-12-12 | 1992-06-12 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-06-12 | 1995-12-12 | 1996-06-12 | $7700.00 | Window Closed / Lapsed |