US4452624A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method for bonding insulator to insulator
Assignee: United States Department of the Navy
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Filing: 1982-12-21
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Granted: 1984-06-05
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Expires: 2002-12-21
Abstract
Abstract A method for making an airtight seal between a pair of insulator elements,uch as glass plates, without destroying any fine structure etched in the insulator elements. A thin metal film is deposited on one of the elements to be sealed and then placed in intimate contact with the other element to be sealed. The elements are then heated to a temperature well below their softening point, but high enough to significantly enhance the ion mobility in the insulator. A voltage is applied across the interface and the resulting anodic reaction consumes the film at the interface while producing a strong hermetic bond between the insulator elements.
Inventors
- 👤 Henry Wohltjen
- 👤 John F. Giuliani
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-26 21:13
CPC Classifications
C; C04; C04B; C04B37/00; C04B37/003; C04B37/006; C03; C03C; C03C27/00; C03C27/06; C03C27/08; C04B2237/00; C04B2237/02; C04B2237/12; C04B2237/121; C04B2237/30; C04B2237/32; C04B2237/50; C04B2237/52; C04B2237/70; C04B2237/708; C04B2237/86
Claims Analysis
Total Claims: 18
Claim 1
Independent Claim
121 words
A method for making an airtight seal between a pair of insulator elements without destroying any fine structures etched in the insulator elements, comprising the steps of: (a) coating one of the pair of insulator elements with a thin metal film; (b) placing the other insulator element and the thin metal film in close surface contact; (c) heating one of the insulator elements to a temperature below its softening point but high enough to render the heated insulator element sufficiently electrically conductive to pass a finite current; and (d) passing a finite positive current from the thin metal film to the heated insulator element to consume the thin metal film and produce an airtight seal between the pair of insulator elements.
Claim 2
Independent Claim
121 words
A method for making an airtight seal between a pair of insulator elements without destroying any fine structures etched in the insulator elements, comprising the steps of: (a) coating one of the pair of insulator elements with a thin metal film; (b) placing the other insulator element and the thin metal film in close surface contact; (c) heating one of the insulator elements to a temperature below its softening point but high enough to render the heated insulator element sufficiently electrically conductive to pass a finite current; and (d) passing a finite positive current from the thin metal film to the heated insulator element to consume the thin metal film and produce an airtight seal between the pair of insulator elements.
Claim 3
Dependent Claim
11 words
The method recited in claim 1 wherein: the insulator is glass.
Claim 4
Dependent Claim
13 words
The method recited in claim 2 wherein: the insulator is soda lime glass.
Claim 5
Dependent Claim
11 words
The method recited in claim 3 wherein: the metal is aluminum.
Claim 6
Dependent Claim
30 words
The method recited in claim 4 wherein: the one insulator element is coated with a thin metal film in the range of 400 to 2000 Angstroms thick in step (a).
Claim 7
Dependent Claim
27 words
The method recited in claim 5 wherein: the one insulator element is heated to a temperature in the range of 200° to 600° C. in step (c).
Claim 8
Dependent Claim
26 words
The method recited in claim 6 wherein step (d) includes the step of: applying a voltage between the thin metal film and the heated insulator element.
Claim 9
Independent Claim
174 words
A method for making an airtight seal between a pair of soda lime glass elements without destroying any fine structures etched in the soda lime glass elements, comprising the steps of: (a) coating one of the pair of soda lime glass elements with a thin aluminum film in the range of 400 to 2000 Angstroms thick; (b) placing the other soda lime glass element and the thin aluminum film in close surface contact; (c) heating one of the soda lime glass elements to a temperature in the range of 200° to 600° C. to render the heated soda lime glass element sufficiently electrically conductive to pass a finite current; and (d) passing a finite positive electric current from the thin aluminum film to the heated soda lime glass element to consume the thin aluminum film and produce an airtight seal between the pair of soda lime glass elements, step (d) including the step of applying a voltage of 200 to 1200 volts between the thin aluminum film and the heated soda lime glass element.
Claim 10
Independent Claim
174 words
A method for making an airtight seal between a pair of soda lime glass elements without destroying any fine structures etched in the soda lime glass elements, comprising the steps of: (a) coating one of the pair of soda lime glass elements with a thin aluminum film in the range of 400 to 2000 Angstroms thick; (b) placing the other soda lime glass element and the thin aluminum film in close surface contact; (c) heating one of the soda lime glass elements to a temperature in the range of 200° to 600° C. to render the heated soda lime glass element sufficiently electrically conductive to pass a finite current; and (d) passing a finite positive electric current from the thin aluminum film to the heated soda lime glass element to consume the thin aluminum film and produce an airtight seal between the pair of soda lime glass elements, step (d) including the step of applying a voltage of 200 to 1200 volts between the thin aluminum film and the heated soda lime glass element.
Claim 11
Dependent Claim
24 words
Themethod recited in claim 8 wherein: the voltage is applied for a time ranging from about 10 seconds to 10 minutes in step (d).
Claim 12
Dependent Claim
24 words
The method recited in claim 9 wherein: step (a) is accomplished by vapor-depositing the thin aluminum film on the one soda lime glass element.
Claim 13
Dependent Claim
21 words
The method recited in claim 10 wherein: step (b) is accomplished by clamping the pair of soda lime glass elements together.
Claim 14
Dependent Claim
23 words
The method recited in claim 11 wherein: step (c) is accomplished by placing the pair of soda lime glass elements in an oven.
Claim 15
Dependent Claim
32 words
The method recited in claim 12 wherein step (d) includes the step of: placing a removable thick metal electrode on the exposed end of the soda lime glass element that is heated.
Claim 16
Dependent Claim
35 words
The method recited in claim 13 wherein step (d) includes the step of: connecting the thick metal electrode and the thin aluminum film to the negative and positive terminals, respectively, of a voltage d.c. source.
Claim 17
Independent Claim
249 words
A method for making an airtight seal between a pair of soda lime glass elements without destroying any fine structures etched in the soda lime glass elements, comprising the steps of: (a) vapor-depositing a thin aluminum film in the range of 400 to 2000 Angstroms thick on one of the pair of soda lime glass elements; (b) clamping the pair of soda lime glass elements together to place the other soda lime glass element and the aluminum film in close surface contact; (c) heating one of the soda lime glass elements in an oven to a temperature in the range of 200° to 600° C. to render the heated soda lime glass element sufficiently electrically conductive to pass a finite current; and (d) passing a finite positive current from the thin aluminum film to the heated soda lime glass element to consume the thin aluminum film and produce an airtight seal between the pair of soda lime glass elements, step (d) including the steps of placing a removable thick metal electrode on the exposed end of the soda lime glass element that is heated; connecting the thick metal electrode and the thin aluminum film to the negative and positive terminals, respectively, of a 200 to 1200 volt d.c. source for a time ranging from about 10 seconds to 10 minutes; and removing the thick metal electrode from the exposed end of the heated insulator element after the airtight seal is formed between the pair of soda lime glass elements.
Claim 18
Independent Claim
249 words
A method for making an airtight seal between a pair of soda lime glass elements without destroying any fine structures etched in the soda lime glass elements, comprising the steps of: (a) vapor-depositing a thin aluminum film in the range of 400 to 2000 Angstroms thick on one of the pair of soda lime glass elements; (b) clamping the pair of soda lime glass elements together to place the other soda lime glass element and the aluminum film in close surface contact; (c) heating one of the soda lime glass elements in an oven to a temperature in the range of 200° to 600° C. to render the heated soda lime glass element sufficiently electrically conductive to pass a finite current; and (d) passing a finite positive current from the thin aluminum film to the heated soda lime glass element to consume the thin aluminum film and produce an airtight seal between the pair of soda lime glass elements, step (d) including the steps of placing a removable thick metal electrode on the exposed end of the soda lime glass element that is heated; connecting the thick metal electrode and the thin aluminum film to the negative and positive terminals, respectively, of a 200 to 1200 volt d.c. source for a time ranging from about 10 seconds to 10 minutes; and removing the thick metal electrode from the exposed end of the heated insulator element after the airtight seal is formed between the pair of soda lime glass elements.
References Cited (Backward Citations)
US3540957A
Cited
DE2301170A1
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-06-05 | 1987-12-05 | 1988-06-05 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-06-05 | 1991-12-05 | 1992-06-05 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-06-05 | 1995-12-05 | 1996-06-05 | $7700.00 | Window Closed / Lapsed |