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US4447725A Expired / Lapsed US ⏱️ 0.0 years remaining

Quantitative measurement of fat, protein and lactose in dairy products

Assignee: MULTISPEC Ltd
•
Filing: 1981-06-15
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Granted: 1984-05-08
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Expires: 2001-06-15
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Abstract

Abstract Electro-optical apparatus for measurement of fat, protein, lactose and solids in milk wherein a milk sample in a test cell is irradiated with reference and measurement beams at differing wavelengths for fat, protein and lactose, and signals are stored indicative of uncorrected concentrations. A scaling and correction circuit includes cross-correction circuitry for compensating the effects on each reading caused by the other constituents. The signals so corrected are then provided in percentage by weight or weight over volume on suitable digital displays. For enhanced accuracy of fat concentration, infrared absorption is measured at both the carbon-hydrogen stretching wavelength (3.48 microns) and the wavelength of absorption at the ester linkages (5.72 microns), and the resulting readings are combined in a predetermined function for obtaining a reading of fat concentration.

Inventors

  • 👤 Delmar A. Biggs
  • 👤 John Shields

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 13:26
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/17; G01N21/25; G01N21/31; G01N21/314; G01N33/00; G01N33/02; G01N33/04; G01N33/06; G01N2021/3129; Y; Y10; Y10S; Y10S250/00; Y10S250/91

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 77 words
Apparatus for measuring fat concentration in fat emulsions such as natural and synthetic dairy products comprising means for holding a product sample, means for irradiating said sample with energy in the infrared spectrum at a first wavelength characteristic of ester linkages and a second wavelength characteristic of saturated carbon-hydrogen bonds, and means for assessing fat concentration in the sample as a predetermined conjoint function of energy absorbed by said sample at both said first and second wavelengths.
Claim 2
Dependent Claim 77 words
Apparatus for measuring fat concentration in fat emulsions such as natural and synthetic dairy products comprising means for holding a product sample, means for irradiating said sample with energy in the infrared spectrum at a first wavelength characteristic of ester linkages and a second wavelength characteristic of saturated carbon-hydrogen bonds, and means for assessing fat concentration in the sample as a predetermined conjoint function of energy absorbed by said sample at both said first and second wavelengths.
Claim 3
Dependent Claim 24 words
The apparatus set forth in claim 1 wherein said irradiating means includes means for successively irradiating said sample at said first and second wavelengths.
Claim 4
Dependent Claim 78 words
The apparatus set forth in claim 1 or 2 further comprising means for irradiating said sample with energy at a third wavelength characteristic of peptide linkages and a fourth wavelength characteristic of hydroxy groups in the sample, and means coupled to said assessing means and responsive to absorption of energy at said third and fourth wavelengths for correcting said predetermined conjoint function for absorption due to said peptide linkages and hydroxy groups at said first and second wavelengths.
Claim 5
Dependent Claim 32 words
The apparatus set forth in claim 3 further comprising means for indicating protein and lactose concentrations in said sample as a function of absorption of energy at said third and fourth wavelengths.
Claim 6
Independent Claim 65 words
A method of measuring fat concentration in dairy products comprising the steps of irradiating a test sample with infrared energy, determining infrared absorption of said sample at a first wavelength characteristic of carbon-hydrogen bonds and a second wavelength characteristic of ester linkages, and then quantitatively assessing the fat concentration of said sample as a predetermined function of absorption at both said first and second wavelengths.
Claim 7
Independent Claim 65 words
A method of measuring fat concentration in dairy products comprising the steps of irradiating a test sample with infrared energy, determining infrared absorption of said sample at a first wavelength characteristic of carbon-hydrogen bonds and a second wavelength characteristic of ester linkages, and then quantitatively assessing the fat concentration of said sample as a predetermined function of absorption at both said first and second wavelengths.
Claim 8
Dependent Claim 55 words
The method set forth in claim 5 comprising the additional steps of determining infrared absorption of said sample at a third wavelength characteristic of peptide linkages and a fourth wavelength characteristic of hydroxy groups, and assessing said fat concentration as a predetermined function of absorption at all of said first, second, third and fourth wavelengths.
Claim 9
Dependent Claim 29 words
The method set forth in claim 6 comprising the additional step of assessing solids concentration in said sample as a predetermined function of absorption at all of said wavelengths.

References Cited (Backward Citations)

US3161768A Cited
US3803384A Cited
US4076983A Cited
JPS5252694A Cited
US4247773A Cited
US4247773B1 Cited
US4310763A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-05-08 1987-11-07 1988-05-08 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-05-08 1991-11-07 1992-05-08 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-05-08 1995-11-07 1996-05-08 $7700.00 Window Closed / Lapsed

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