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US4440800A Expired / Lapsed US ⏱️ 0.0 years remaining

Vapor coating of powders

Assignee: Commonwealth Scientific and Industrial Research Organisation
•
Filing: 1981-04-16
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Granted: 1984-04-03
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Expires: 2001-04-16
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Abstract

Abstract A liquid or powder material can be dispersed by the application of electrostatic fields. The phenomena, referred to as "electrodispersion" is the dispersion by an intense electric field of part of a static bed of liquid or powder into a stable cloud of rapidly moving particles, and the maintenance of a dynamic equilibrium between the static and dispersed phases. The density of the dispersed cloud of particles varies with a number of factors, including the field strength and the nature of the powder. The electrodeposition effect is employed to produce a uniform and durable coating of controlled thickness on the individual particles, by the generation of a vapor of the desired coating--typically a metal or semiconductor material--and allowing the vapor to permeate the dispersed particles. The electric field ensures that only the particles are coated, and the dispersed particles, having the same charge, repel each other, avoiding agglomeration. Potential applications include the manufacture of high performance catalysts wherein expensive metals like platinum are vapor-coated onto an inexpensive metal powder. Other possibilities include the production of graphite-coated metal particles for making self-lubricating metal components such as bearings and shafts, and the manufacture of slow dissolving coatings on pharmaceutical powders.

Inventors

  • 👤 David H. Morton
  • 👤 Stephen G. Szirmai
  • 👤 Edmund C. Potter

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 01:03
CPC Classifications
C; C23; C23C; C23C14/00; C23C14/22; C23C14/223; B; B22; B22F; B22F1/00; B22F1/17; B22F1/18; B22F9/00; B22F9/02; B22F9/12; Y; Y02; Y02E; Y02E60/00; Y02E60/30; Y02E60/32

Claims Analysis

Total Claims: 20
Claim 1
Independent Claim 38 words
A method of vapour coating of a particulate material, comprising dispersing said particulate material by the application of an electrostatic field and causing a vapour or dispersion of a coating material to permeate the dispersion of particulate material.
Claim 2
Independent Claim 38 words
A method of vapour coating of a particulate material, comprising dispersing said particulate material by the application of an electrostatic field and causing a vapour or dispersion of a coating material to permeate the dispersion of particulate material.
Claim 3
Dependent Claim 40 words
A method of vapour coating of a particulate material according to claim 1, wherein said vapour coating is conducted in a container with said vapour or dispersion of a coating material being supplied from a source external to said container.
Claim 4
Dependent Claim 35 words
A method of vapour coating of a particulate material according to claim 1, wherein dispersion of said particulate material and generation of said vapour or dispersion of a coating material are conducted in one container.
Claim 5
Independent Claim 24 words
A method of vapour coating of a particulate material according to any one of claims 1 to 3, carried out under conditions of vacuum.
Claim 6
Dependent Claim 23 words
A method of vapour coating of a particulate material according to claim 1, wherein the coating is in a gas other than air.
Claim 7
Dependent Claim 13 words
A method according to claim 5, wherein said gas is an inert gas.
Claim 8
Dependent Claim 12 words
A method according to claim 5, wherein said gas is sulphur dioxide.
Claim 9
Dependent Claim 24 words
A method according to claim 1, wherein said coating material is vaporized or dispersed from an electrode above a bed of said particulate material.
Claim 10
Dependent Claim 22 words
A method according to claim 1, wherein said coating material is vaporized or dispersed from an electrode which is at ground potential.
Claim 11
Dependent Claim 28 words
A method according to claim 1, wherein the thickness of the coating of the vapour-coated material is controlled by varying the rate of withdrawal of said vapour-coating material.
Claim 12
Independent Claim 95 words
A method of preparing discrete coated partilces having: (i) an inner core of a first material which is capable of being dispersed by the application of an electrostatic field, and (ii) an outer coating of a second material which is capable of being vaporized, said method comprising: (a) dispersing particles of said first material by the application of an electrostatic field; and (b) vaporizing or providing a dispersion of and subsequently depositing said second material as a vapor or dispersion onto the surface of said particles of the first material while said particles are dispersed.
Claim 13
Independent Claim 95 words
A method of preparing discrete coated partilces having: (i) an inner core of a first material which is capable of being dispersed by the application of an electrostatic field, and (ii) an outer coating of a second material which is capable of being vaporized, said method comprising: (a) dispersing particles of said first material by the application of an electrostatic field; and (b) vaporizing or providing a dispersion of and subsequently depositing said second material as a vapor or dispersion onto the surface of said particles of the first material while said particles are dispersed.
Claim 14
Dependent Claim 20 words
The method of claim 11, wherein said second material is deposited to form a continuous outer coating on said particles.
Claim 15
Dependent Claim 18 words
The method of claim 11 or 12, wherein said second material is deposited from the vapour phase thereof.
Claim 16
Dependent Claim 22 words
The method of claim 13, wherein said second material is provided with an electric charge of opposite polarity to the said particles.
Claim 17
Dependent Claim 26 words
The method of claim 11, wherein one electrode is placed in a bed of said first material and a second electrode is arranged above said bed.
Claim 18
Dependent Claim 37 words
The method of claim 11, wherein said step of dispersing particles by the application of an electrostatic field comprises providing electrostatic field generating means, generating an electrostatic field therefrom, and placing said particles in said electrostatic field.
Claim 19
Dependent Claim 18 words
The method of claim 11, wherein said dispersion is a suspension of at least some of said particles.
Claim 20
Dependent Claim 18 words
The method of claim 1, wherein said dispersion is a suspension of at least some of said particles.

References Cited (Backward Citations)

US3670699A Cited
US3978269A Cited
US4209550A Cited
US4150905A Cited
US4233387A Cited
US4233365A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-04-03 1987-10-03 1988-04-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-04-03 1991-10-03 1992-04-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-04-03 1995-10-03 1996-04-03 $7700.00 Window Closed / Lapsed

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