Process for drying pumpable suspensions

Claim 2

A process for drying pumpable suspensions or crystal solutions in which the liquid having a solids content of up to 50% by weight is evaporated during transport by the indirect application of heat accompanied by the release of pressure, characterised in that, in a multiphase flow tube, in which the ratio of circumference to cross-sectional area is from 0.05 to 1.5 [mm -1 ], and with a throughput of from 2 to 50 kg/h per square centimeter of cross-sectional area, any plug-like deposits in the tacky paste-to-solid transitional zone subjected to intense heating are sheared off from the wall of the flow tube by brief increases in pressure of from 0.5 to 10 bars beyond the system pressure of 5 to 20 bars, and in that the moisture still present in the solid particles is then removed by evaporation in the flow tube to a residue of 0.1% by weight.

Claim 3

A process as claimed in claim 1, characterised in that the increase in pressure is produced by vapour, including any propellent gas added, flowing at a rate of at least 100 m/s before reaching the transition zone.

Claim 4

A process as claimed in claim 1, characterised in that a vapour from an external source is added to said flow tube at certain time intervals to start off detachment of the solid.

Claim 5

A process as claimed in claims 1, 2 or 3, characterised in that the flow tube is coiled with a ratio of tube diameter to coil diameter of from 0.1 to 0.5.

Claim 6

A process for producing essentially dry material from pumpable suspensions or crystal solutions comprising (a) feeding said suspension or solution having a solids content of up to 50% by weight to a multiphase flow tube at a pressure of between 5 and 20 bars, wherein said flow tube has a ratio of circumference to cross-sectional area of between 0.05 and 1.5 mm -1 and has an unconstricted downstream terminus whereby the material being processed experiences a pressure drop during its transit of the tube; (b) maintaining a throughput in said flow tube of between 2 and 50 kg/h per square centimeter of cross-sectional area; (c) supplying sufficient indirect heat to said flow tube to affect evaporation to no more than 0.1 weight percent of liquid; and (d) applying pressure surges of between 0.5 and 10 bars to the material in the flow tube of sufficient magnitude duration and frequency to shear off the plug-like deposits which form in the portion of said tube in which the material being processed is undergoing a transition from a tacky paste to a solid and prevent blockage of the tube.

Claim 7

A process for producing essentially dry material from pumpable suspensions or crystal solutions comprising (a) feeding said suspension or solution having a solids content of up to 50% by weight to a multiphase flow tube at a pressure of between 5 and 20 bars, wherein said flow tube has a ratio of circumference to cross-sectional area of between 0.05 and 1.5 mm -1 and has an unconstricted downstream terminus whereby the material being processed experiences a pressure drop during its transit of the tube; (b) maintaining a throughput in said flow tube of between 2 and 50 kg/h per square centimeter of cross-sectional area; (c) supplying sufficient indirect heat to said flow tube to affect evaporation to no more than 0.1 weight percent of liquid; and (d) applying pressure surges of between 0.5 and 10 bars to the material in the flow tube of sufficient magnitude duration and frequency to shear off the plug-like deposits which form in the portion of said tube in which the material being processed is undergoing a transition from a tacky paste to a solid and prevent blockage of the tube.