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US4425378A Expired / Lapsed US ⏱️ 0.0 years remaining

Electroless nickel plating activator composition a method for using and a ceramic capacitor made therewith

Assignee: MRA Laboratories Inc
•
Filing: 1981-07-06
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Granted: 1984-01-10
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Expires: 2001-07-06
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Abstract

Abstract An activator composition paste includes a homogeneous dispersion of a palladium and commensurate amounts of silicon and of zinc. A screen printed layer of this paste is applied to a ceramic capacitor body to form electrodes, terminations or both. The body is heated to 615 DEG C. and subsequently electroless nickel plated providing excellent electrical and mechanical connection of the plated nickel to the ceramic.

Inventors

  • 👤 John P. Maher

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-07 11:30
CPC Classifications
C; C23; C23C; C23C18/00; C23C18/16; C23C18/18; C23C18/1851; C23C18/1862; C23C18/1865; C23C18/1872; C23C18/1886; C23C18/1889

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 51 words
An electroless plating activator composition for sensitizing a ceramic surface to be electroless nickel plated consisting essentially of palladium, at least half as much silicon as palladium and 1.3 times as much zinc as silicon, all by weight, said palladium, silicon and zinc being homogeneously dispersed in a liquid organic vehicle.
Claim 2
Dependent Claim 51 words
An electroless plating activator composition for sensitizing a ceramic surface to be electroless nickel plated consisting essentially of palladium, at least half as much silicon as palladium and 1.3 times as much zinc as silicon, all by weight, said palladium, silicon and zinc being homogeneously dispersed in a liquid organic vehicle.
Claim 3
Dependent Claim 27 words
The activator composition of claim 1 additionally comprising a liquid organic vehicle and an organic binder mixture in which said palladium, silicon and zinc are homogeneously dispersed.
Claim 4
Dependent Claim 18 words
The activator composition of claim 1 wherein said palladium is introduced in the form of a palladium resinate.
Claim 5
Dependent Claim 18 words
The activator composition of claim 1 wherein said silicon is introduced in the form of a silicon resinate.
Claim 6
Dependent Claim 18 words
The activator composition of claim 1 wherein said zinc is introduced in the form of a zinc resinate.
Claim 7
Dependent Claim 18 words
The activator composition of claim 1 wherein the silicon to palladium ratio by weight is less than 36.
Claim 8
Independent Claim 87 words
A method for making a ceramic capacitor comprising (a) selectively depositing on a ceramic body two films of an electroless nickel activator composition consisting essentially of palladium, at least half as much by weight of silicon as of palladium and 1.3 times as much zinc as silicon by weight said palladium, silicon, and zinc being homogeneously dispersed in a liquid organic vehicle; (b) heating said films to a peak temperature of from 500°-750° C.; and (c) electroless plating a layer of nickel over each of said films.
Claim 9
Independent Claim 87 words
A method for making a ceramic capacitor comprising (a) selectively depositing on a ceramic body two films of an electroless nickel activator composition consisting essentially of palladium, at least half as much by weight of silicon as of palladium and 1.3 times as much zinc as silicon by weight said palladium, silicon, and zinc being homogeneously dispersed in a liquid organic vehicle; (b) heating said films to a peak temperature of from 500°-750° C.; and (c) electroless plating a layer of nickel over each of said films.
Claim 10
Dependent Claim 48 words
The method of claim 7 wherein said electroless nickel activator composition is combined in a liquid organic vehicle to form a paste, said depositing consisting of screen printing said paste, whereby said heating drives off said organic vehicle and more securely bonds said activator films to said substrate.
Claim 11
Dependent Claim 20 words
The activator composition of claim 1 wherein the ratio of said zinc to said silicon is no greater than 2.9.

References Cited (Backward Citations)

US3207706A Cited
US3681261A Cited
US3741780A Cited
US4150995A Cited
US4243710A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-01-09 1987-07-11 1988-01-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-01-09 1991-07-11 1992-01-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-01-09 1995-07-11 1996-01-10 $7700.00 Window Closed / Lapsed

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