← Back to Patent Explorer
US4425291A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for the production of more water-resistant foamed elements from waterglass containing natural latex dispersion

Assignee: KUPFER MANFRED MEYERHOLZ 1 D-2833 DUENSEN GERMANY
•
Filing: 1981-11-27
•
Granted: 1984-01-10
•
Expires: 2001-11-27
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract A method for the production of a more water-resistant foamed element from waterglass consisting essentially of the steps of mixing together a major amount of an alkali metal silicate solution, with inorganic fillers, at least one alkali-resistant wetting agent in an amount sufficient to form a stable foam, at least one compound capable of hardening a waterglass foam in an amount sufficient to cause said alkali metal silicate to harden, and sufficient natural latex dispersion to cause the foamed element to have a greater water resistance, mechanically foaming said mixture by the incorporation of an inert gas thereon, filling the resultant foam into an element form capable of disassembly, curing said foam in said form, and recovering a more water-resistant foamed and cured element. Preferably the natural latex dispersion is employed in a 50% dispersion in an amount of from 0.2% to 30% by weight, preferably from 0.2% to 10% by weight, based on the total mixture. The alkali metal silicate solution used has, in the case of sodium silicate, a solids content of about 27% to 43% by weight at an SiO 2 /Na 2 O molar ratio of about 4 : 1 to 3 : 1 and in the case of potassium silicate a solids content of about 20% to 36% by weight at an SiO 2 /K 2 O molar ratio of about 4 : 1 to 3.4 : 1, it being possible to use any desired mixture ratios of the mentioned alkali metal silicates. The mixture may optionally contain an addition of 0.1% to 2.5% by weight, preferably from 1% to 2% by weight of B 2 O 3 . Preferably the wetting agent added to the mixture is an anionic tenside, such as a sodium C 14-16 alkylsulfonate, in an amount of from 0.1% to 10% by weight, preferably from 4% to 6% by weight in the form of a 30% aqueous solution. The fillers to be added to the mixture are inorganic compounds of light specific gravity in a grain size up to 0.1 mm and in an amount of up to 50% by weight, preferably from 10% to 20% by weight. The hardeners are preferably proportioned into the mixture during foaming in amounts of from 1% to 10% by weight, preferably from 2% to 6% by weight. The preferred hardener is glycerine triacetate.

Inventors

  • 👤 Gunter Beer
  • 👤 Wolfgang Pesch
  • 👤 Wolfgang Friedemann
  • 👤 Manfred Kupfer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 20:34
CPC Classifications
C; C04; C04B; C04B28/00; C04B28/24; C04B28/26

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 115 words
A method for the production of a more water-resistant foamed element from waterglass consisting essentially of the steps of mixing together a major amount of an alkali metal silicate solution, with inorganic fillers, at least one alkali-resistant wetting agent in an amount sufficient to form a stable foam, at least one compound capable of hardening a waterglass foam in an amount sufficient to cause said alkali metal silicate to harden, and sufficient natural latex dispersion to cause the foamed element to have a greater water resistance, mechanically foaming said mixture by the incorporation of an inert gas thereon, molding the resultant foam, curing said molded foam, and recovering a more water-resistant foamed and cured element.
Claim 2
Independent Claim 115 words
A method for the production of a more water-resistant foamed element from waterglass consisting essentially of the steps of mixing together a major amount of an alkali metal silicate solution, with inorganic fillers, at least one alkali-resistant wetting agent in an amount sufficient to form a stable foam, at least one compound capable of hardening a waterglass foam in an amount sufficient to cause said alkali metal silicate to harden, and sufficient natural latex dispersion to cause the foamed element to have a greater water resistance, mechanically foaming said mixture by the incorporation of an inert gas thereon, molding the resultant foam, curing said molded foam, and recovering a more water-resistant foamed and cured element.
Claim 3
Dependent Claim 29 words
The method of claim 1 wherein a 50% aqueous natural latex dispersion is used in an amount of from 0.2% to 30% by weight, based on the total mixture.
Claim 4
Dependent Claim 25 words
The method of claim 2 wherein said dispersion is used in an amount of from 0.2% to 10% by weight, based on the total mixture.
Claim 5
Dependent Claim 81 words
The method of claim 1 or 2 or 3 wherein said alkali metal silicate solution is selected from the group consisting of sodium silicate solution having a solids content of about 27% to 43% by weight and a SiO 2 /Na 2 O molar ratio of about 4:1 to 3:1, potassium silicate solution having a solids content of about 20% to 36% by weight and a SiO 2 /K 2 O molar ratio of about 4:1 to 3.4:1, and mixtures thereof.
Claim 6
Dependent Claim 28 words
The method of claim 1 or 2 or 3 wherein said alkali metal silicate solution contains from 0.1% to 2.5% by weight of B 2 O 3 .
Claim 7
Dependent Claim 24 words
The method of claim 4 wherein said alkali metal silicate solution contains from 0.1% to 2.5% by weight of B 2 O 3 .
Claim 8
Dependent Claim 24 words
The method of claim 5 wherein said alkali metal silicate solution contains from 1% to 2% by weight of B 2 O 3 .
Claim 9
Dependent Claim 24 words
The method of claim 6 wherein said alkali metal silicate solution contains from 1% to 2% by weight of B 2 O 3 .
Claim 10
Dependent Claim 29 words
The method of claim 1 or 2 or 3 wherein said alkali-stable wetting agent is anionic and is present in an amount of from 0.1% to 10% by weight.
Claim 11
Dependent Claim 39 words
The method of claim 9 wherein said anionic wetting agent is Na 14 -C 16 alkylsulfonate present as a 30% aqueous solution and employed in an amount of from 4% to 6% by weight, based on the total mixture.
Claim 12
Dependent Claim 28 words
The method of claim 1 or 2 or 3 wherein said inorganic fillers are of light specific gravity and have a particle size of up to 0.1 mm.
Claim 13
Dependent Claim 22 words
The method of claim 11 wherein said light inorganic fillers are present in an amount of from 1% to 50% by weight.
Claim 14
Dependent Claim 22 words
The method of claim 12 wherein said light inorganic fillers are present in an amount of from 10% to 20% by weight.
Claim 15
Dependent Claim 39 words
The method of claim 1 or 2 or 3 wherein said at least one compound capable of hardening a waterglass foam is an acid-splitting ester or acid anhydride present in an amount of from 1% to 10% by weight.
Claim 16
Dependent Claim 26 words
The method of claim 14 wherein said acid-splitting ester or acid anhydride is glycerine triacetate present in an amount of from 2% to 6% by weight.

References Cited (Backward Citations)

DE1905340U Cited
US3508940A Cited
US3707385A Cited
US3782982A Cited
US3719510A Cited
DE2165912A1 Cited
US3850650A Cited
US3864137A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-01-09 1987-07-11 1988-01-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-01-09 1991-07-11 1992-01-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-01-09 1995-07-11 1996-01-10 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag