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US4424487A Expired / Lapsed US ⏱️ 0.0 years remaining

Dispersion coefficient determination

Assignee: Phillips Petroleum Co
•
Filing: 1981-06-02
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Granted: 1984-01-03
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Expires: 2001-06-02
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Abstract

Abstract Dispersion coefficients of fluids in porous media are determined by NMR spin echo techniques while the fluid is flowing through the porous medium.

Inventors

  • 👤 Donald E. Lauffer

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 03:36
CPC Classifications
G; G01; G01N; G01N15/00; G01N15/08; G01R; G01R33/00; G01R33/20; G01R33/44

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 93 words
A method for determining the dispersion coefficient of fluid in porous media comprising (a) positioning a sample representative of said porous media in an NMR spectrometer, (b) causing said fluid to flow through said so positioned sample, said fluid being capable of exhibiting a detectable response in an NMR spectrometer measurement, (c) carrying out an NMR spin echo measurement while said fluid is glowing and while said flowing fluid is subjected to a magnetic field gradient and obtaining a spin echo signal, (d) determining the dispersion coefficient from the spin echo signal obtained.
Claim 2
Independent Claim 93 words
A method for determining the dispersion coefficient of fluid in porous media comprising (a) positioning a sample representative of said porous media in an NMR spectrometer, (b) causing said fluid to flow through said so positioned sample, said fluid being capable of exhibiting a detectable response in an NMR spectrometer measurement, (c) carrying out an NMR spin echo measurement while said fluid is glowing and while said flowing fluid is subjected to a magnetic field gradient and obtaining a spin echo signal, (d) determining the dispersion coefficient from the spin echo signal obtained.
Claim 3
Dependent Claim 68 words
A method in accordance with claim 1 wherein said fluid is flowing through said sample in a main direction which is essentially 90° to the main constant magnetic field of the NMR spectrometer and wherein said sample during said spin echo measurement is subjected to a radio frequency electromagnetic pulse generated in a coil surrounding said sample and having a coil axis essentially parallel to said main direction.
Claim 4
Dependent Claim 50 words
A method in accordance with claim 2 wherein during said spin echo measurement said sample is subjected to a further magnetic field generating a gradient in magnetic field strength having a direction essentially parallel to the main magnetic field and wherein the transverse dispersion coefficient of the sample is determined.
Claim 5
Dependent Claim 57 words
A method in accordance with claim 2 wherein during said spin echo measurement said sample is subjected to a further magnetic field generating a gradient in the magnetic field strength having a direction essentially orthogonal to the main magnetic field and parallel to the coil axis and wherein the longitudinal dispersion coefficient of the sample is determined.
Claim 6
Dependent Claim 46 words
A method in accordance with claim 3 wherein a plurality of three 90° pulse spin echo measurements is carried out, wherein the spin echo signal is obtained as a function of the magnetic field gradient and wherein said transverse dispersion coefficient is determined from said function.
Claim 7
Dependent Claim 46 words
A method in accordance with claim 4 wherein a plurality of three 90° pulse spin echo measurements is carried out, wherein the spin echo signal is obtained as a function of said magnetic field gradient and wherein said longitudinal dispersion coefficient is determined from said function.
Claim 8
Independent Claim 105 words
A method for determining the dispersion coefficient of fluid in porous media comprising (a) positioning a sample representative of said porous media in an NMR spectrometer, (b) causing said fluid to flow through said so positioned sample, said fluid being capable of exhibiting a detectable response in an NMR spectrometer measurement, (c) carrying out an NMR spin echo measurement while said fluid is flowing and while said flowing fluid is subjected to a magnetic field gradient and obtaining a spin echo signal, (d) obtaining the spin echo signal as a function of said magnetic field gradient, and (e) determining the dispersion coefficient from said function.
Claim 9
Independent Claim 105 words
A method for determining the dispersion coefficient of fluid in porous media comprising (a) positioning a sample representative of said porous media in an NMR spectrometer, (b) causing said fluid to flow through said so positioned sample, said fluid being capable of exhibiting a detectable response in an NMR spectrometer measurement, (c) carrying out an NMR spin echo measurement while said fluid is flowing and while said flowing fluid is subjected to a magnetic field gradient and obtaining a spin echo signal, (d) obtaining the spin echo signal as a function of said magnetic field gradient, and (e) determining the dispersion coefficient from said function.
Claim 10
Independent Claim 111 words
A method for determining the dispersion coefficient of fluid in porous media comprising (a) positioning a sample representative of said porous media in an NMR spectrometer, (b) causing said fluid to flow through said so positioned sample, said fluid being capable of exhibiting a detectable response in an NMR spectrometer measurement, (c) carrying out an NMR spin echo measurement while said fluid is flowing and while said flowing fluid is subjected to a magnetic field having a constant magnetic field gradient applied and obtaining a spin echo signal, (d) obtaining the spin echo signal as a function of said magnetic field gradient, and (e) determining the dispersion coefficient from said function.
Claim 11
Independent Claim 111 words
A method for determining the dispersion coefficient of fluid in porous media comprising (a) positioning a sample representative of said porous media in an NMR spectrometer, (b) causing said fluid to flow through said so positioned sample, said fluid being capable of exhibiting a detectable response in an NMR spectrometer measurement, (c) carrying out an NMR spin echo measurement while said fluid is flowing and while said flowing fluid is subjected to a magnetic field having a constant magnetic field gradient applied and obtaining a spin echo signal, (d) obtaining the spin echo signal as a function of said magnetic field gradient, and (e) determining the dispersion coefficient from said function.

References Cited (Backward Citations)

US3213355A Cited
US4022276A Cited
SU754280A1 Cited
US4318044A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-01-02 1987-07-04 1988-01-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-01-02 1991-07-04 1992-01-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-01-02 1995-07-04 1996-01-03 $7700.00 Window Closed / Lapsed

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