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US4423005A Expired / Lapsed US ⏱️ 0.0 years remaining

Determining quantitative degree of ethylene oxide exposure in sterilization processes

Assignee: Baxter International Inc
•
Filing: 1982-04-09
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Granted: 1983-12-27
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Expires: 2002-04-09
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Abstract

Abstract A method of quantitatively determining the amount of exposure of an object to ethylene oxide gas. A pre-weighed ethylene oxide-permeable container, which encloses a predetermined amount of catalyst for the reaction of the ethylene oxide gas to form a liquid, is placed adjacent to the object. The object and container are then exposed to ethylene oxide gas for controlled time and at a known humidity and temperature. The container is then reweighed. The weight gain of the container is a quantitative indication of the amount of exposure to ethylene oxide gas. The test system may be calibrated against its effect in known concentrations of ethylene oxide gas, so that the precise amount of exposure to ethylene oxide gas can be determined.

Inventors

  • 👤 J. Barry Murtaugh
  • 👤 Dean G. Laurin
  • 👤 John E. Kling
  • 👤 Archie G. Woodworth

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 05:49
CPC Classifications
G; G01; G01N; G01N33/00; G01N33/0004; G01N33/0009; G01N33/0027; G01N33/0036; G01N33/0047; Y; Y10; Y10S; Y10S436/00; Y10S436/908; Y10T; Y10T436/00; Y10T436/14; Y10T436/142222

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 58 words
A device for quantitatively determining the amount of exposure of an object to ethylene oxide gas, which comprises: a tube containing a catalyst for the hydrolysis of ethylene oxide, said tube being sealed at both ends thereof, the seal at at least one end being gas-permeable, but impermeable to said catalyst and liquid hydrolysis products of ethylene oxide.
Claim 2
Independent Claim 58 words
A device for quantitatively determining the amount of exposure of an object to ethylene oxide gas, which comprises: a tube containing a catalyst for the hydrolysis of ethylene oxide, said tube being sealed at both ends thereof, the seal at at least one end being gas-permeable, but impermeable to said catalyst and liquid hydrolysis products of ethylene oxide.
Claim 3
Dependent Claim 24 words
The device of claim 1 in which said catalyst is an ion exchange resin selected from the group consisting of acidic and basic resins.
Claim 4
Dependent Claim 17 words
The device of claim 2 in which said ion exchange resin is of a strongly acidic type.
Claim 5
Independent Claim 81 words
A device for quantitatively determining the amount of exposure of an object to ethylene oxide gas, which comprises: a container enclosing a predetermined amount of a catalyst for the reaction of ethylene oxide to form a liquid, said container including a porous gas-permeable member communicating between its interior and exterior, said member being impermeable to said catalyst and liquid, whereby ethylene oxide gas may pass into said container but liquid reaction products of ethylene oxide cannot pass out of said container.
Claim 6
Independent Claim 81 words
A device for quantitatively determining the amount of exposure of an object to ethylene oxide gas, which comprises: a container enclosing a predetermined amount of a catalyst for the reaction of ethylene oxide to form a liquid, said container including a porous gas-permeable member communicating between its interior and exterior, said member being impermeable to said catalyst and liquid, whereby ethylene oxide gas may pass into said container but liquid reaction products of ethylene oxide cannot pass out of said container.
Claim 7
Dependent Claim 33 words
The device of claim 4 in which said catalyst is an ion exchange resin selected from the group consisting of acidic and basic resins capable of causing hydrolysis and polymerization of ethylene oxide.
Claim 8
Dependent Claim 17 words
The device of claim 5 in which said ion exchange resin is of the strongly acidic type.

References Cited (Backward Citations)

US3028434A Cited
US2998306A Cited
US3851043A Cited
US3950980A Cited
US4277632A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-12-26 1987-06-27 1987-12-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-12-26 1991-06-27 1991-12-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-12-26 1995-06-27 1995-12-27 $7700.00 Window Closed / Lapsed

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