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US4412936A Expired / Lapsed US ⏱️ 0.0 years remaining

Pigment for color-changing heat indicator

Assignee: ALMALYXKY GORNO-METALLURGICHESKY KOMBINAT 702400 ALMALYK TASHKENTSKOI OBLASTI
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Filing: 1981-05-07
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Granted: 1983-11-01
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Expires: 2001-05-07
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Abstract

Abstract A pigment for a color-changing heat indicator comprising a product obtained by interaction of an aqueous solution containing ions of copper and mercury with an aqueous solution of a nitrogen-containing organic compound: an amide of carbonic acid, an amide of thiocarbonic acid, a tertiary amine to give a reaction mixture which is reacted with an aqueous solution containing ions of iodine at an atomic ratio of copper:mercury:iodine equal to 2:1.5:3-5 and an amount of the nitrogen-containing organic compound equal to 0.8-8% of the total content of copper and mercury; the pigment has its critical temperature of from 38° to 70° C. and a heat-resistance of from 160° to 180° C.

Inventors

  • 👤 Stanislav F. Khmelkov
  • 👤 Mnaidar R. Ramazanov
  • 👤 Mikhail P. Soldatov
  • 👤 Vadim V. Beskaravainy
  • 👤 Viktor L. Aranovich
  • 👤 Lev K. Soldaev

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 19:28
CPC Classifications
G; G01; G01K; G01K11/00; G01K11/12; G01K11/14; C; C09; C09D; C09D5/00; C09D5/26; Y; Y10; Y10S; Y10S252/00; Y10S252/962

Claims Analysis

Total Claims: 8
Claim 1
Independent Claim 94 words
A method of producing a pigment for a color-changing heat indicator which comprises: (a) mixing an aqueous solution containing ions of bivalent copper and mercury with an aqueous solution of a nitrogen containing compound selected from the group consisting of an amide of carbonic or thiocarbonic acid, and a tertiary amine in an amount equal to 0.8-8.0% of the total content of copper and mercury, and (b) adding to the resulting mixture, an aqueous solution containing iodine ions to thereby form a pigment wherein the atomic ratio of Cu:Hg:I in said pigment is 2:1.5:3-5.
Claim 2
Independent Claim 94 words
A method of producing a pigment for a color-changing heat indicator which comprises: (a) mixing an aqueous solution containing ions of bivalent copper and mercury with an aqueous solution of a nitrogen containing compound selected from the group consisting of an amide of carbonic or thiocarbonic acid, and a tertiary amine in an amount equal to 0.8-8.0% of the total content of copper and mercury, and (b) adding to the resulting mixture, an aqueous solution containing iodine ions to thereby form a pigment wherein the atomic ratio of Cu:Hg:I in said pigment is 2:1.5:3-5.
Claim 3
Dependent Claim 20 words
The method according to claim 1, further comprising drying said pigment to a moisture content of between 2 and 4%.
Claim 4
Dependent Claim 21 words
The method according to claim 1 wherein said carbonic acid amide is selected from the group consisting of urea and thiourea.
Claim 5
Dependent Claim 12 words
The method according to claim 1 wherein said tertiary amine is hexamethylenetetramine.
Claim 6
Dependent Claim 13 words
The method according to claim 3, wherein the carbonic acid amide is urea.
Claim 7
Dependent Claim 13 words
The method according to claim 3, wherein the carbonic acid amide is thiourea.
Claim 8
Dependent Claim 15 words
The product produced by the process of claims 1, 2, 3, 4, 5 or 6.

References Cited (Backward Citations)

SU352922A1 Cited
US3219993A Cited
DE2611602A1 Cited
SU735620A1 Cited
JPS5370931A Cited
JPS54138546A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-10-31 1987-05-02 1987-11-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-10-31 1991-05-02 1991-11-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-10-31 1995-05-02 1995-11-01 $7700.00 Window Closed / Lapsed

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