US4409078A
Expired / Lapsed
US
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Methods and apparatus for electrostatically resolving emulsions
Assignee: ExxonMobil Technology and Engineering Co
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Filing: 1981-04-20
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Granted: 1983-10-11
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Expires: 2001-04-20
Abstract
Abstract A new apparatus and methods are featured for electrostatically resolving emulsions. The apparatus comprises a flexible electrode carrying electrolytes, therein. Emulsions are resolved by passing current through the electrolyte at frequencies to or above 60 Hz.
Inventors
- 👤 John P. Wagner
- 👤 Edward C. Hsu
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 14:43
CPC Classifications
B; B01; B01D; B01D17/00; B01D17/06; B01D61/00; B01D61/38; B01D61/40; C; C10; C10G; C10G33/00; C10G33/02
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
141 words
A method of electrostatically resolving emulsions containing solids dispersed in liquid into corresponding liquid and solid phases, comprising the steps of: (a) placing a grounded electrode in an aqueous phase of said emulsion; (b) placing a current-carrying electrode adjacent an interface of said liquid and solid phases, said current-carrying electrode having an inner support member for supporting an outer flexible plastic tube, said outer flexible plastic tube surrounding said inner support member and being concentrically spaced therefrom so as to provide a space therebetween, and an electrolyte disposed within said space between said support member and said plastic tube; and (c) passing an alternating current through said current-carrying electrode, said current having a frequency above 60 Hz and a voltage in an approximate range of from 2 to 100 kV, sufficient to effect the separation of said emulsion into said phases.
Claim 2
Independent Claim
141 words
A method of electrostatically resolving emulsions containing solids dispersed in liquid into corresponding liquid and solid phases, comprising the steps of: (a) placing a grounded electrode in an aqueous phase of said emulsion; (b) placing a current-carrying electrode adjacent an interface of said liquid and solid phases, said current-carrying electrode having an inner support member for supporting an outer flexible plastic tube, said outer flexible plastic tube surrounding said inner support member and being concentrically spaced therefrom so as to provide a space therebetween, and an electrolyte disposed within said space between said support member and said plastic tube; and (c) passing an alternating current through said current-carrying electrode, said current having a frequency above 60 Hz and a voltage in an approximate range of from 2 to 100 kV, sufficient to effect the separation of said emulsion into said phases.
Claim 3
Dependent Claim
13 words
The method of claim 1, wherein said current frequency is approximately 400 Hz.
Claim 4
Independent Claim
166 words
A method of increasing the throughput of a coalescence apparatus which electrostatically resolves emulsions into their corresponding phases, comprising the steps of: (a) flowing said emulsion into a reaction vessel; (b) placing a grounded electrode in an aqueous phase of said emulsion; (c) placing a current-carrying electrode adjacent an interface of said phases, said current-carrying electrode having an inner support member for supporting an outer flexible plastic tube, said outer flexible plastic tube surrounding said inner support member and being concentrically spaced therefrom so as to provide a space therebetween, and an electrolyte disposed within said space between said support member and said plastic tube; (d) passing an alternating current through said current-carrying electrode, said current having a frequency above 60 Hz and a voltage in an approximate range of from 2 to 100 kV, sufficient to effect the separation of said emulsion into said phases, said throughput increasing with increasing frequency for a given voltage; and (e) removing the separated phases from said reaction vessel.
Claim 5
Independent Claim
166 words
A method of increasing the throughput of a coalescence apparatus which electrostatically resolves emulsions into their corresponding phases, comprising the steps of: (a) flowing said emulsion into a reaction vessel; (b) placing a grounded electrode in an aqueous phase of said emulsion; (c) placing a current-carrying electrode adjacent an interface of said phases, said current-carrying electrode having an inner support member for supporting an outer flexible plastic tube, said outer flexible plastic tube surrounding said inner support member and being concentrically spaced therefrom so as to provide a space therebetween, and an electrolyte disposed within said space between said support member and said plastic tube; (d) passing an alternating current through said current-carrying electrode, said current having a frequency above 60 Hz and a voltage in an approximate range of from 2 to 100 kV, sufficient to effect the separation of said emulsion into said phases, said throughput increasing with increasing frequency for a given voltage; and (e) removing the separated phases from said reaction vessel.
Claim 6
Dependent Claim
13 words
The method of claim 3, wherein said current frequency is approximately 400 Hz.
Claim 7
Independent Claim
149 words
A method of electrostatically resolving an emulsion having an approximate range of electrical conductivity of from 0.1 to 1×10 -12 ohm -1 cm -1 into its corresponding phases, comprising the steps of: (a) placing a grounded electrode in an aqueous phase of said emulsion; (b) placing a current-carrying electrode adjacent an interface of said phases, said current-carrying electrode having an inner support member for supporting an outer flexible plastic tube, said outer flexible plastic tube surrounding said inner support member and being concentrically spaced therefrom so as to provide a space therebetween, and an electrolyte disposed within said space between said support member and said plastic tube; and (c) passing an alternating current through said current-carrying electrode, said current having a frequency above 60 Hz and a voltage in an approximate range of from 2 to 100 kV, sufficient to effect the separation of said emulsion into said phases.
Claim 8
Independent Claim
149 words
A method of electrostatically resolving an emulsion having an approximate range of electrical conductivity of from 0.1 to 1×10 -12 ohm -1 cm -1 into its corresponding phases, comprising the steps of: (a) placing a grounded electrode in an aqueous phase of said emulsion; (b) placing a current-carrying electrode adjacent an interface of said phases, said current-carrying electrode having an inner support member for supporting an outer flexible plastic tube, said outer flexible plastic tube surrounding said inner support member and being concentrically spaced therefrom so as to provide a space therebetween, and an electrolyte disposed within said space between said support member and said plastic tube; and (c) passing an alternating current through said current-carrying electrode, said current having a frequency above 60 Hz and a voltage in an approximate range of from 2 to 100 kV, sufficient to effect the separation of said emulsion into said phases.
Claim 9
Dependent Claim
13 words
The method of claim 4, wherein said current frequency is approximately 400 Hz.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-10-10 | 1987-04-11 | 1987-10-11 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-10-10 | 1991-04-11 | 1991-10-11 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-10-10 | 1995-04-11 | 1995-10-11 | $7700.00 | Window Closed / Lapsed |