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US4397797A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for extrusion coating of a pipe with a foamed cover layer having three integrally formed cellular sub-layers

Assignee: Furukawa Metals Co Ltd
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Filing: 1980-07-25
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Granted: 1983-08-09
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Expires: 2000-07-25
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Abstract

Abstract A method for manufacturing a heat insulating pipe having a foamed insulating layer around the outer surface of said pipe. The foamed insulating layer has an expansion ratio of at least 4. It has three integral sub-layers, said sub-layers including a cellular middle foamed sub-layer which is integral with a cellular inner foamed sub-layer and a cellular outer foamed sub-layer, said inner and outer sub-layer being on opposite sides of said middle sub-layer, said cellular inner foamed sub-layer being the innermost sub-layer with respect to said pipe and surrounding the outer surface of said pipe. The cells of said inner and outer sub-layers are smaller than the cells of said middle cellular sub-layer, the ratio mu 1/ mu 2 of the cell dimensions of said cellular middle sub-layer are between 0.3 and 0.9, wherein mu 1 is the average cell dimension measured in the radial direction of said pipe and mu 2 is the average cell dimension measured in the axial direction of said pipe. The method for producing said 3 sub-layered foamed insulating layer comprises passing a pipe heated to a temperature of between 60 DEG C. and 120 DEG C. through the nipple of a cross-head die and simultaneously extruding a mixture of a propylene-ethylene block polymer having an ethylene content of between 1 and 20% by weight and a Melt Index of between 0.1 and 4 together with a foaming agent over the outer surface of said pipe to cause said mixture to expand and form said 3 sub-layered foamed insulating layer on said pipe, the relationship between the overall thickness t of the 3 sub-layered foamed insulating layer, the expansion ratio M of the 3 sub-layered foamed insulating layer, and the die-nipple distance d of a cross-head die being <IMAGE> wherein K=0.75 to 0.20.

Inventors

  • 👤 Akio Nojiri
  • 👤 Toshio Koreeda
  • 👤 Masao Horiguch

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 07:59
CPC Classifications
C; C08; C08J; C08J9/00; C08J9/34; B; B29; B29C; B29C44/00; B29C44/20; B29C44/22; B29C44/32; B29C44/322; F; F16; F16L; F16L59/00; F16L59/04; F16L59/14; C08J2323/00; C08J2323/02; C08J2323/10; Y; Y10; Y10S; Y10S138/00; Y10S138/09; Y10T; Y10T428/00; Y10T428/13; Y10T428/1352; Y10T428/1376; Y10T428/249921; Y10T428/249953; Y10T428/249961; Y10T428/249976; Y10T428/249977

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 301 words
A method for manufacturing a heat insulating pipe comprising a pipe having a foamed insulating layer around the outer surface of said pipe, said foamed insulating layer having an expansion ratio of at least 4 and comprising three integrally formed sub-layers, said sub-layers including a cellular middle foamed sub-layer which is integral with a cellular inner foamed sub-layer and a cellular outer foamed sub-layer, said inner and outer sub-layer being on opposite sides of said middle sub-layer, said cellular inner foamed sub-layer being the innermost sub-layer with respect to said pipe and surrounding the outer surface of said pipe, the cells of said inner and outer cellular sub-layers being smaller than the cells of said middle cellular sub-layer, the ratio μ 1 /μ 2 of the cell dimensions of said cellular middle sub-layer being between 0.3 and 0.9, wherein μ 1 is the average cell dimension measured in the radial direction of said pipe and μ 2 is the average cell dimension measured in the axial direction of said pipe; the method for producing said 3 sub-layered foamed insulating layer comprising: passing a pipe heated to a temperature of between 60° C. and 120° C. through the nipple of a cross-head die and simultaneously extruding a mixture of a propylene-ethylene block polymer having an ethylene content of between 1 and 20% by weight and a Melt Index of between 0.1 and 4 together with a foaming agent over the outer surface of said pipe to cause said mixture to expand and form said 3 sub-layered foamed insulating layer on said pipe, the relationship between the overall thickness t of the 3 sub-layered foamed insulating layer, the expansion ratio M of the 3 sub-layered foamed insulating layer, and the die-nipple distance d of the cross-head die being ##EQU3## wherein K=0.75 to 0.20.
Claim 2
Independent Claim 301 words
A method for manufacturing a heat insulating pipe comprising a pipe having a foamed insulating layer around the outer surface of said pipe, said foamed insulating layer having an expansion ratio of at least 4 and comprising three integrally formed sub-layers, said sub-layers including a cellular middle foamed sub-layer which is integral with a cellular inner foamed sub-layer and a cellular outer foamed sub-layer, said inner and outer sub-layer being on opposite sides of said middle sub-layer, said cellular inner foamed sub-layer being the innermost sub-layer with respect to said pipe and surrounding the outer surface of said pipe, the cells of said inner and outer cellular sub-layers being smaller than the cells of said middle cellular sub-layer, the ratio μ 1 /μ 2 of the cell dimensions of said cellular middle sub-layer being between 0.3 and 0.9, wherein μ 1 is the average cell dimension measured in the radial direction of said pipe and μ 2 is the average cell dimension measured in the axial direction of said pipe; the method for producing said 3 sub-layered foamed insulating layer comprising: passing a pipe heated to a temperature of between 60° C. and 120° C. through the nipple of a cross-head die and simultaneously extruding a mixture of a propylene-ethylene block polymer having an ethylene content of between 1 and 20% by weight and a Melt Index of between 0.1 and 4 together with a foaming agent over the outer surface of said pipe to cause said mixture to expand and form said 3 sub-layered foamed insulating layer on said pipe, the relationship between the overall thickness t of the 3 sub-layered foamed insulating layer, the expansion ratio M of the 3 sub-layered foamed insulating layer, and the die-nipple distance d of the cross-head die being ##EQU3## wherein K=0.75 to 0.20.
Claim 3
Dependent Claim 9 words
The method of claim 1 wherein K is 0.3-0.4.
Claim 4
Dependent Claim 27 words
The method of claim 1 or 2 wherein said propylene-ethylene block copolymer is a powder having a Melt Index of 0.1-2 and an ethylene content of 7-20%.
Claim 5
Dependent Claim 22 words
The method of claim 3 wherein said propylene-ethylene block copolymer has admixed therewith up to 40% by weight of an ethylene-propylene rubber.
Claim 6
Dependent Claim 24 words
The method of claim 1 or 2 wherein said propylene-ethylene block copolymer has admixed therewith up to 40% by weight of an ethylene-propylene rubber.
Claim 7
Dependent Claim 19 words
The method of claim 1 wherein said foaming agent has a decomposition temperature of between 120° and 170° C.
Claim 8
Dependent Claim 19 words
The method of claim 4 wherein said foaming agent has a decomposition temperature of between 120° and 170° C.
Claim 9
Dependent Claim 20 words
The method of claim 1 or 2 wherein said pipe is a copper pipe which has been precoated with resin.
Claim 10
Dependent Claim 31 words
The method of claim 6 wherein said pipe is a copper pipe which has been precoated with resin applied from an aqueous resin-containing emulsion or an aqueous-containing solution and then baked.
Claim 11
Dependent Claim 20 words
The method of claim 1 wherein said middle sub-layer comprises 40-90% of the total thickness of said formed insulated layer.

References Cited (Backward Citations)

GB1217729A Cited
US3649730A Cited
US3528458A Cited
FR2033555A5 Cited
JPS4824822B1 Cited
JPS484869U Cited
DE2420608A1 Cited
US4146562A Cited
US4130976A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-08-08 1987-02-07 1987-08-09 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-08-08 1991-02-07 1991-08-09 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-08-08 1995-02-07 1995-08-09 $7700.00 Window Closed / Lapsed

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