Patent US4824238A successfully refreshed from Google Patents.
US4396378A
Expired / Lapsed
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Method for preparing cavities in teeth for restoration
Assignee: Scientific Pharmaceuticals Inc
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Filing: 1982-03-17
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Granted: 1983-08-02
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Expires: 2002-03-17
Abstract
Abstract A solid fatty polyamide dissolved in a volatile organic solvent has been found effective for preparing cavities of teeth for restoration. For example, when this solution is applied to a cavity in the form of a dental cavity varnish, the organic solvent may be evaporated to leave behind a continuous polyamide film which is compatible with methacrylate resin type restoratives. Solid fatty polyamides are generally derived from the reaction product of partially polymerized unsaturated fatty acids with aliphatic diamines. The present invention relates to methods for preparing cavities with these polyamides as well as to compositions containing these polyamides.
Inventors
- 👤 Jan A. Orlowski
- 👤 Marvin N. Stark
- 👤 David V. Butler
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 00:13
CPC Classifications
A; A61; A61K; A61K6/00; A61K6/20
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
127 words
A method for preparing a tooth having a cavity for restoration with a restorative material, said method comprising the steps of: (i) applying to the cavity at least one solution comprising at least one solid fatty polyamide dissolved in a volatile organic solvent; and (ii) forming a solid, hardened film of said polyamide in said cavity by evaporation of said solvent, said polyamide consisting essentially of the reaction product of at least one partially polymerized unsaturated fatty acid with at least one aliphatic diamine, said partially polymerized fatty acid having at least 32 carbon atoms and at least two carboxylic acid groups, said aliphatic diamine having 2-8 carbon atoms and two primary amino groups, and said polyamide having a molecular weight from about 6000 to about 9000.
Claim 2
Independent Claim
127 words
A method for preparing a tooth having a cavity for restoration with a restorative material, said method comprising the steps of: (i) applying to the cavity at least one solution comprising at least one solid fatty polyamide dissolved in a volatile organic solvent; and (ii) forming a solid, hardened film of said polyamide in said cavity by evaporation of said solvent, said polyamide consisting essentially of the reaction product of at least one partially polymerized unsaturated fatty acid with at least one aliphatic diamine, said partially polymerized fatty acid having at least 32 carbon atoms and at least two carboxylic acid groups, said aliphatic diamine having 2-8 carbon atoms and two primary amino groups, and said polyamide having a molecular weight from about 6000 to about 9000.
Claim 3
Dependent Claim
49 words
A method according to claim 1, wherein said partially polymerized unsaturated fatty acids consist of from about 40% to about 100% of dimers of at least one of said unsaturated fatty acids and from 0% to about 40% of trimers of at least one of said unsaturated fatty acids.
Claim 4
Dependent Claim
37 words
A method according to claim 1, wherein said organic solvent is selected from the group consisting of primary C 1 -C 4 alcohols, C 5 -C 8 hydrocarbons, methylenedichloride, chloroform, carbon tetrachloride and mixtures of said solvents.
Claim 5
Dependent Claim
20 words
A method according to claim 1, wherein said polyamide is the reaction product of dimerized linoleic acid with ethylene diamine.
Claim 6
Dependent Claim
26 words
A method according to claim 1, wherein said solution comprises from about 5 to about 35 grams of said polyamide per 100 ml of said solvent.
Claim 7
Dependent Claim
48 words
A method according to claim 1, wherein said step (i) comprises painting a solution which is a dental cavity varnish on the sides of said cavity, whereby when said polyamide film is formed in accordance with said step (ii) the exposed dental tubules of the tooth are sealed.
Claim 8
Dependent Claim
71 words
A method according to claim 1 wherein the composition employed consists essentially of: (i) at least one solid fatty polyamide; (ii) a volatile organic solvent, said polyamide (i) being dissolved in said solvent; and (iii) at least one non-volatile material suitable for preparing said tooth for restoration selected from the group consisting of antibacterial and antiseptic additives, antifungal additives, anesthetic additives, additives which stimulate secondary dentine formation and X-ray opaquing additives.
Claim 9
Dependent Claim
95 words
A method according to claim 7, wherein said non-volatile material (iii) is selected from the group consisting of: (a) antibacterial and antiseptic additives selected from the group consisting of benzalconium chloride, cetylpyridinium chloride, and camphorated pentachlorophenol; (b) anti-fungal agents selected from the group consisting of benzoic acid and salicylic acid; (c) anesthetic agents selected from the group consisting of benzocaine and benzyl alcohol; (d) an additive for stimulating secondary dentine formation which is calcium hydroxide; and (e) X-ray opaquing additives selected from the group consisting of barium sulphate, barium containing glass and strontium containing glass.
Claim 10
Dependent Claim
70 words
A method according to claim 7 wherein the solution is a dental cavity varnish and step (i) comprising painting said varnish on the sides of the cavity, whereby when said polyamide is formed in accordance with step (ii) the exposed dental tubules of the tooth are sealed and wherein said non-volatile material (iii) is fully dissolved in said volatile liquid (ii), and wherein said varnish is free of calcium hydroxide.
Claim 11
Dependent Claim
20 words
A process according to claim 7 wherein the composition includes calcium hydroxide as component (iii) for stimulating secondary dentine formation.
Claim 12
Dependent Claim
20 words
A process according to claim 1 wherein the composition includes calcium hydroxide as an additive for stimulating secondary dentine formation.
Claim 13
Dependent Claim
28 words
A process according to claim 1 wherein the composition contains an antibacterial and antiseptic additive selected from the group consisting of benzalconium chloride, cetylpyridinium chloride and camphorated pentachlorophenol.
Claim 14
Dependent Claim
23 words
A process according to claim 1 wherein the composition contains an anesthetic agent selected from the group consisting of benzocaine and benzyl alcohol.
Claim 15
Dependent Claim
29 words
A process according to claim 1 wherein the composition contains an x-ray opaquing additive selected from the group consisting of barium sulphate, barium containing glass and strontium containing glass.
Claim 16
Dependent Claim
15 words
A method according to claim 1 wherein the polyamide consists of the stated reaction product.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-08-01 | 1987-01-31 | 1987-08-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-08-01 | 1991-01-31 | 1991-08-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-08-01 | 1995-01-31 | 1995-08-02 | $7700.00 | Window Closed / Lapsed |