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US4393101A Expired / Lapsed US ⏱️ 0.0 years remaining

Diethynylbenzene-ethynylpyrene copolymers

Assignee: United States Department of the Air Force
•
Filing: 1982-06-11
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Granted: 1983-07-12
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Expires: 2002-06-11
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Abstract

Abstract A high char yielding matrix resin for use in fabricating carbon-carbon composites comprised of a polymerizable mixture of a diethynylbenzene monomer and an ethynylpyrene monomer.

Inventors

  • 👤 Norman Bilow

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 03:03
CPC Classifications
C; C08; C08F; C08F238/00; F; F02; F02K; F02K9/00; F02K9/97; F02K9/974

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 97 words
A method for the production of a resinous impregnated carbon-carbon composite ablative material which comprises the steps of (1) forming an interwoven graphite fiber structure, (2) impregnating said structure with a matrix resinous precursor composed of a polymerizable mixture of diethynylbenzene and ethynylpyrene, (3) heating said impregnated structure at a temperature and for a period of time sufficient to effect the copolymerization of said mixture (4) further heating said polymerized structure at a temperature, pressure and period of time sufficient to pyrolyze said structure (5) graphitizing said pyrolized structure and (6) recovering the resulting carbon-carbon composite structure.
Claim 2
Independent Claim 97 words
A method for the production of a resinous impregnated carbon-carbon composite ablative material which comprises the steps of (1) forming an interwoven graphite fiber structure, (2) impregnating said structure with a matrix resinous precursor composed of a polymerizable mixture of diethynylbenzene and ethynylpyrene, (3) heating said impregnated structure at a temperature and for a period of time sufficient to effect the copolymerization of said mixture (4) further heating said polymerized structure at a temperature, pressure and period of time sufficient to pyrolyze said structure (5) graphitizing said pyrolized structure and (6) recovering the resulting carbon-carbon composite structure.

References Cited (Backward Citations)

US3628984A Cited
US3705131A Cited
US3926897A Cited
US3926907A Cited
US3993711A Cited
US4215161A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-07-11 1987-01-10 1987-07-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-07-11 1991-01-10 1991-07-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-07-11 1995-01-10 1995-07-12 $7700.00 Window Closed / Lapsed

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