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US4382101A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for increasing the peel strength of metal-clad polymers

Assignee: Honeywell UOP LLC
•
Filing: 1982-02-22
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Granted: 1983-05-03
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Expires: 2002-02-22
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Abstract

Abstract The peel strength of metal-clad polymers such as a polyimide polymer may be increased by treating said polymer with a gas plasma prior to the deposition of the metal thereon. The gas plasma is provided for by the introduction of a gas such as helium, argon, compositions of gases such as carbon tetrafluoride and oxygen over the surface of the polymer while said polymer is in an electrical field in which the power may range from about 3.8×10 -3 watts/cm 2 to about 100 watts/cm 2 .

Inventors

  • 👤 Anthony J. Polak

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 12:56
CPC Classifications
C; C08; C08J; C08J7/00; C08J7/12; C08J7/123; C23; C23C; C23C14/00; C23C14/02; C23C14/021; C23C14/022; C23C18/00; C23C18/16; C23C18/18; C23C18/20; C23C18/2006; H; H05; H05K; H05K3/00; H05K3/38; H05K3/381; H05K1/00; H05K1/02; H05K1/03; H05K1/0313; H05K1/032; H05K1/0333; H05K2201/00; H05K2201/01; H05K2201/0137; H05K2201/0154; H05K2203/00; H05K2203/09; H05K2203/095; H05K3/10; H05K3/18; H05K3/181; H05K3/388; Y; Y10; Y10T; Y10T428/00; Y10T428/31504; Y10T428/31721

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 114 words
A process for increasing the peel strength of a metal-clad polyimide polymer which comprises subjecting said polyimide polymer to a carbon tetrafluoride/oxygen gas plasma in an electrical field generated from an electrical power of from about 3.8×10 -3 watts/cm 2 to about 100 watts/cm 2 at a temperature of from about ambient to about the glass transition temperature of said polyimide polymer and a pressure in the range of from about 5 atmospheres to about 10 -6 torr for a period of time ranging from about 0.1 minutes to about 4 hours, thereafter depositing a conductive metal on the resultant treated polyimide polymer and recovering the resultant metal-clad polyimide polymer processing increased peel strength.
Claim 2
Dependent Claim 114 words
A process for increasing the peel strength of a metal-clad polyimide polymer which comprises subjecting said polyimide polymer to a carbon tetrafluoride/oxygen gas plasma in an electrical field generated from an electrical power of from about 3.8×10 -3 watts/cm 2 to about 100 watts/cm 2 at a temperature of from about ambient to about the glass transition temperature of said polyimide polymer and a pressure in the range of from about 5 atmospheres to about 10 -6 torr for a period of time ranging from about 0.1 minutes to about 4 hours, thereafter depositing a conductive metal on the resultant treated polyimide polymer and recovering the resultant metal-clad polyimide polymer processing increased peel strength.
Claim 3
Dependent Claim 15 words
The process as set forth in claim 1 in which said conductive metal is copper.
Claim 4
Dependent Claim 15 words
The process as set forth in claim 1 in which said conductive metal is nickel.
Claim 5
Dependent Claim 15 words
The process as set forth in claim 1 in which said conductive metal is aluminum.
Claim 6
Dependent Claim 15 words
The process as set forth in claim 1 in which said conductive metal is zinc.
Claim 7
Dependent Claim 15 words
The process as set froth in claim 1 in which said conductive metal is brass.

References Cited (Backward Citations)

US3801368A Cited
US3929604A Cited
US3914521A Cited
US4250225A Cited
US4165394A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-05-02 1986-11-01 1987-05-03 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-05-02 1990-11-01 1991-05-03 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-05-02 1994-11-01 1995-05-03 $7700.00 Window Closed / Lapsed

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