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US4381197A Expired / Lapsed US ⏱️ 0.0 years remaining

Warm consolidation of glassy metallic alloy filaments

Assignee: General Electric Co
•
Filing: 1980-07-24
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Granted: 1983-04-26
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Expires: 2000-07-24
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Abstract

Abstract Filaments of glassy metallic alloys prepared by chill block melt-spinning are consolidated under heat and pressure by uniaxial pressing to form discrete self-supporting glassy metallic alloy bodies of substantially uniform composition.

Inventors

  • 👤 Howard H. Liebermann

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-23 19:07
CPC Classifications
B; B22; B22F; B22F3/00; B22F3/006; B22F3/12; B22F3/14; B22F9/00; B22F9/002; B22F9/008; H; H01; H01F; H01F1/00; H01F1/01; H01F1/03; H01F1/12; H01F1/14; H01F1/147; H01F1/153; H01F1/15358

Claims Analysis

Total Claims: 19
Claim 1
Independent Claim 113 words
The method of producing a consolidated dense discrete metallic body comprising the steps of: (a) defining an open-ended compacting volume; (b) distributing a preselected amount of intertwined filamentary glassy metallic alloy substantially uniformly into said open-ended compacting volume, said filamentary alloy having a width-to-thickness ratio of less than about 600:1; and (c) uniaxially compressing said preselected amount of said filamentary alloy with a pressure for a period of time sufficient to produce thereby a consolidated dense discrete metallic body that is at least 50% glassy, with any remainder crystalline, while maintaining said filamentary alloy at a substantially uniform temperature throughout of at least its plastic transition temperature, but less than its crystallization temperature.
Claim 2
Independent Claim 113 words
The method of producing a consolidated dense discrete metallic body comprising the steps of: (a) defining an open-ended compacting volume; (b) distributing a preselected amount of intertwined filamentary glassy metallic alloy substantially uniformly into said open-ended compacting volume, said filamentary alloy having a width-to-thickness ratio of less than about 600:1; and (c) uniaxially compressing said preselected amount of said filamentary alloy with a pressure for a period of time sufficient to produce thereby a consolidated dense discrete metallic body that is at least 50% glassy, with any remainder crystalline, while maintaining said filamentary alloy at a substantially uniform temperature throughout of at least its plastic transition temperature, but less than its crystallization temperature.
Claim 3
Dependent Claim 17 words
The method of claim 1 wherein said open-ended compacting volume is formed in a partially assembled die.
Claim 4
Dependent Claim 44 words
The method of claim 2 further including the step of inserting a punch into said die to close said open-ended compacting volume prior to initiating the uniaxial compression step thereby completing the assembly of said die containing said preselected amount of said filamentary alloy.
Claim 5
Dependent Claim 71 words
The method of claim 1 wherein the distributing step is accomplished by repeatedly partially filling said open-ended compacting volume with a portion of said preselected amount of said filamentary alloy and partially compacting said portion of said filamentary alloy to a substantially uniform packing density of about at least 50% to no more than about 60% until said open-ended compacting volume is filled with said preselected amount of said filamentary alloy.
Claim 6
Dependent Claim 38 words
The method of claim 2 wherein an induction heating coil surrounding said die is used to rapidly heat said preselected amount of said filamentary alloy to the requisite substantially uniform temperature to be maintained during the compressing step.
Claim 7
Dependent Claim 33 words
A consolidated dense discrete self-supporting metallic body having an atomic structure that is at least 50% glassy with any remainder crystalline, said body being prepared in accordance with the method of claim 1.
Claim 8
Dependent Claim 13 words
The body of claim 6 in which the atomic structure is totally glassy.
Claim 9
Dependent Claim 13 words
The body of claim 6 in which the density is at least 80%.
Claim 10
Independent Claim 200 words
The method of producing a magnetically soft consolidated dense discrete body comprising the steps of: (a) defining an open-ended compacting volume; (b) distributing a preselected amount of intertwined magnetically soft filamentary glassy metallic alloy, preheated to a temperature of at least its plastic transition temperature, but less than its crystallization temperature, substantially uniformly into said open-ended compacting volume without exceeding the elastic limit of said alloy while maintaining said die at a substantially uniform temperature throughout of at least the plastic transition temperature, but less than the crystallization temperature of said alloy, said magnetically soft filamentary alloy having a width-to-thickness ratio of less than about 600:1; and (c) uniaxially compressing said preselected amount of magnetically soft filamentary glassy metallic alloy with a gradually applied pressure for a period of time sufficient to produce thereby a magnetically soft consolidated dense discrete metallic body that is at least 50% glassy, with any remainder crystalline, while maintaining said filamentary alloy at a substantially uniform temperature throughout of at least its plastic transition temperature, but less than its crystallization temperature; and (d) disassembling said die following completion of said uniaxial compression step recovering thereby a magnetically soft metallic body in a substantially strain-free condition.
Claim 11
Independent Claim 200 words
The method of producing a magnetically soft consolidated dense discrete body comprising the steps of: (a) defining an open-ended compacting volume; (b) distributing a preselected amount of intertwined magnetically soft filamentary glassy metallic alloy, preheated to a temperature of at least its plastic transition temperature, but less than its crystallization temperature, substantially uniformly into said open-ended compacting volume without exceeding the elastic limit of said alloy while maintaining said die at a substantially uniform temperature throughout of at least the plastic transition temperature, but less than the crystallization temperature of said alloy, said magnetically soft filamentary alloy having a width-to-thickness ratio of less than about 600:1; and (c) uniaxially compressing said preselected amount of magnetically soft filamentary glassy metallic alloy with a gradually applied pressure for a period of time sufficient to produce thereby a magnetically soft consolidated dense discrete metallic body that is at least 50% glassy, with any remainder crystalline, while maintaining said filamentary alloy at a substantially uniform temperature throughout of at least its plastic transition temperature, but less than its crystallization temperature; and (d) disassembling said die following completion of said uniaxial compression step recovering thereby a magnetically soft metallic body in a substantially strain-free condition.
Claim 12
Dependent Claim 17 words
The method of claim 9 wherein said open-ended compacting volume is formed in a partially assembled die.
Claim 13
Dependent Claim 71 words
The method of claim 10 further including the step of inserting a punch heated to a substantially uniform temperature throughout of at least the plastic transition temperature, but less than the crystallization temperature of said glassy metallic alloy, into said die to close said open-ended compacting volume prior to initiating the uniaxial compression step thereby completing the assembly of said die containing said preselected amount of said filamentary glassy metallic alloy.
Claim 14
Dependent Claim 26 words
The method of claim 9 further including the step of annealing the recovered substantially strain-free magnetically soft body at a temperature less than its crystallization temperature.
Claim 15
Dependent Claim 17 words
The method of claim 12 wherein said annealing is conducted in the presence of a magnetic field.
Claim 16
Dependent Claim 42 words
A magnetically soft consolidated dense discrete self-supporting body having a low coercive field, a high permeability and an atomic structure that is at least 50% glassy with any remainder crystalline, said body being prepared in accordance with the method of claim 9.
Claim 17
Dependent Claim 13 words
The body of claim 14 in which the atomic structure is totally glassy.
Claim 18
Dependent Claim 13 words
The body of claim 14 in which the density is at least 80%.
Claim 19
Dependent Claim 15 words
The body of claim 14 in which the coercive field is less than 250 millioersteds.

References Cited (Backward Citations)

US4079430A Cited
US4197146A Cited
US4201837A Cited
US4298382A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-04-25 1986-10-25 1987-04-26 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-04-25 1990-10-25 1991-04-26 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-04-25 1994-10-25 1995-04-26 $7700.00 Window Closed / Lapsed

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